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chemical polishing

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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001162
EISBN: 978-1-62708-220-4
...Abstract Abstract Some 99.90 pure tin tubes (0.15 mm thick) used for packaging a chemical compound cracked on bending and underwent brittle fracture prior to filling, while others remained ductile and showed no sign of failure. Examination showed that specimens prepared by mechanical methods...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001160
EISBN: 978-1-62708-220-4
...Abstract Abstract A corrosion resistant chromium nickel steel (X 2 Cr-Ni-Mo 18 10) worm drive used in a chemical plant at 80 deg C and 100 to 200 atm pressure to transport media containing chloride failed during normal operation. Visual inspections showed that the entire surface of the gear...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0059924
EISBN: 978-1-62708-235-8
... to reveal detectable indications. The indications were not considered serious enough to reject the forgings. A few small indications in the areas tested were revealed by magnetic particle inspection. The area was conditioned by grinding and polishing to obtain an additional inspection at a greater depth...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047192
EISBN: 978-1-62708-235-8
... displayed very flat fracture surfaces with no apparent yielding, but the two large segments did show evidence of bending (yielding) near the fractures. In addition, some segments contained fine radial cracks. Analysis (visual inspection, optical microscopy on polished-and-etched specimens, hardness testing...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0046870
EISBN: 978-1-62708-217-4
... of the hollow shaft was exposed to hydraulic oil at temperatures of 0 to 80 deg C (30 to 180 deg F). Analysis (visual inspection, 15-30x low magnification examination, 4x light fractograph, chemical analysis, hardness testing) supported the conclusions that the shaft cracked in a region subjected to severe...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001489
EISBN: 978-1-62708-217-4
... 17.9 3.6 4.5 1.9 2.1 0.5 0.2 — 1.4 Ca — — — — 18.9 16.5 1.0 1.2 — — — 1.5 Fe balance The chemical compositions of the inclusions observed on the polished surfaces of specimens A and B are given in Tables 2 and 3 , respectively. Almost all the inclusions in rings...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.pulp.c0089567
EISBN: 978-1-62708-230-3
..., chemical analysis, mechanical testing, as-polished 54x magnification, etched with nital 33x/54x/215x/230x magnification) supported the conclusions that the NDE indications were the consequence of a cold-shut condition in the casting. The cold shut served as a stress-concentration site and was therefore...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001845
EISBN: 978-1-62708-241-9
... grinding emery papers up to #2000 grit. Chemical polishing was performed with diamond paste and FeCl3 solution (2 g FeCl 3 + 500 ml deionized water). Etch solution (5 g FeCl 3 + 50 ml HCl + 500 ml deionized water) was applied to reveal the microstructure. Cleaning was performed using ethanol followed...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001108
EISBN: 978-1-62708-214-3
... tubing. Fig. 4 Polished, nonetched transverse section of the straight specimen of the pigtail tubing. Examination of etched samples was performed after chemical etching of the previously polished surfaces with 50 vol% HCI, 16 vol% H 2 O 2 , and 34 vol% H 2 O. The etched microstructure...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001753
EISBN: 978-1-62708-241-9
... defects. Chemical analysis to determine the component’s chemical composition was conducted via certified optical emission spectroscopy (OES). Axial and transverse sections from the right-side fork leg were cold mounted in resin for metallographic inspection. The metallographic mounts were polished...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
... that the failure analyst usually considers, but they do occur from time to time. Such materials can be identified both microscopically and chemically, and careful documentation and continuity of evidence is very important in such circumstances. A special case of wear is fretting, in which contacting surfaces...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006757
EISBN: 978-1-62708-295-2
..., the mount should be of a material that is not chemically attacked. The grinding and polishing procedure is best carried out on an automatic or semiautomatic machine. The structure of each and every ceramic product has been specifically adjusted to exhibit the required properties and thus shows a unique...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001667
EISBN: 978-1-62708-235-8
... been chemically milled, a procedure common to the surface preparation and machining of titanium alloys, which produced a superior surface finish. All of the grinding and polishing performed on the weldment was done with the Di-Profiler using various PSA-backed grinding papers and polishing cloths...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001059
EISBN: 978-1-62708-214-3
... or replacement, was recommended to prevent chloride buildup. Painting of the steel surface with an epoxy-phenolic or epoxy-coal tar was also suggested. Chemical processing industry Columns (process) Marine environments 316 UNS S31600 Stress-corrosion cracking Pitting corrosion Background Visual...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001839
EISBN: 978-1-62708-241-9
... cracking of the coil material. To address the problem through appropriate process intervention to prevent its recurrence in low nickel stainless steel hot rolled coils. The chemical composition of the steel samples was analyzed using an optical emission spectrometer (OES), ARL Model 3460...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0089456
EISBN: 978-1-62708-223-5
.... The polished specimen was then etched with 5% nital. A marked banded structure was evident even macroscopically ( Fig. 1b ). Microscopic examination revealed that the pattern was due to severe chemical segregation or banding ( Fig. 1c ). Hardness measurements were then conducted across the face...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001754
EISBN: 978-1-62708-241-9
... subsequently led to the discovery of overlooked debris in an engine chip detector, and thus resulted in a review of several maintenance practices. aircraft bearings operating overload inadequate maintenance and inspection M50 alloy steel bulk deformation energy dispersive spectrometry chemical...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001704
EISBN: 978-1-62708-218-1
...Abstract Abstract Several type 304 stainless steel fire truck water tanks developed through-wall leaks after being in service for approximately two years. One representative tank underwent a comprehensive laboratory analysis, which included metallographic examinations and chemical analyses...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001180
EISBN: 978-1-62708-219-8
...Abstract Abstract A T-piece from a copper hot water system failed. Microscopic examination of a polished section revealed a main crack and branching transcrystalline cracks running from the outer surface of the pipe into the pipe wall. The crack appearance indicated disintegration by stress...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001362
EISBN: 978-1-62708-215-0
... in Fig. 1 , was visually examined. Multiple cracks were observed over much of the surface of the damaged disc. Fig. 1 The rotor disc segment is shown as received for analysis Nondestructive Evaluation Surface Examination Metallography Chemical Analysis/Identification Mechanical...