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A new supplier for aluminum die castings was being evaluated, and the castings failed to meet the durability test requirements. Specifically, the fatigue life of the castings was low. Initial inspection of the fatigue fracture surfaces revealed large-scale porosity visible to the naked eye. New castings with reduced porosity also failed the durability tests. The fatigue fracture surfaces of additional casting fragments were very rough and contained multiple ratchet marks along the inner fillet. These observations indicated the fatigue process was heavily influenced by the presence of surface imperfections. Improving the surface finish or choosing a stronger alloy, were more likely to improve part durability than reducing the porosity.

A ‘worn-out’ spiral bevel gear and pinion set was submitted for examination and evaluation. This was a spiral bevel drive set with the gear attached to a differential. The assembled unit was driving a new, large, experimental farm tractor in normal plowing and tilling operations. The primary failure was associated with the 4820H NiMo alloy steel pinion, and thus the gear was not examined. The mode of failure was rolling contact fatigue, and the cause of failure improper engineering design. The pattern of continual overload was restricted to a specific concentrated area situated diagonally across the profile of the loaded side, which was consistent on every tooth.

A plant had manufactured and heat treated their product in house for years. As time went on, the special steel that they had been using became more expensive, and a switch was made to a more common and less highly alloyed material. However, no change in hardness specifications were made, because calculations of ideal critical diameter and analysis of available hardenability data indicated that the original hardness specification could be met. There was, however, less room for process variation. The parts ended up containing temper carbides, developed heavy decarburization, and experienced excessive distortion because they were left in the furnace for extended and varying periods with the temperature “turned down a couple hundred degrees.”

Tube failures occurred in quick succession in two boiler units from a bank of six boilers in a refinery. The failures were confined to the SAE 192 carbon steel horizontal support tubes of the superheater pack. In both cases, the failure was by perforation adjacent to the welded fin on the crown of the top tubes and located in an area near the upward bend of the tube. The inside of all the tubes were covered with a loosely adherent, black, alkaline, powdery deposit comprised mainly of magnetite. The corroded areas, however, had relatively less deposit. The morphology of the corrosion damage was typical of alkaline corrosion and confirmed that the boiler tubes failed as a result of steam blanketing that concentrated phosphate salts. The severe alkaline conditions developed most probably because of the decomposition of trisodium phosphate, which was used as a water treatment chemical for the boiler feed water.

A failed tapered-ring sprocket locking device consisted of an assembly of four tapered rings that are retained by a series of cap screws. The middle wedge-shaped rings were pulled closer as the screws were tightened forcing the split inner ring to clamp tightly onto the shaft. One of the wedge-shaped middle rings fractured prior to having been fully torqued, preventing the sprocket from being locked to the shaft. “Woody” fracture features, as a result of decohesion between a high volume fractions of manganese sulfide stringers and the matrix, was revealed during examination. The material was revealed by chemical analysis to be resulfurized grade of carbon steel (SAE type 1144, UNS G11440) which has enhanced longitudinal tensile properties but low transverse properties. It was observed that when the fastening screws were torqued, a significant hoop stress was placed on the middle rings and it caused the failure at the large inclusion present at the minimum section thickness zone of the middle ring. It was concluded that since the material contained a high volume fraction of these inclusions, the material choice was not appropriate for this application. A nonresulfurized grade of low-alloy steel was suggested as recommendation.

Near-surface porosity in zinc die castings that were subsequently plated with copper, nickel, and bright chromium was causing blemishes in the plating. Identifying die casting turbulence and hot spots were keys to process modifications that subsequently allowed porosity to be greatly minimized.

This article presents tools, techniques, and procedures that engineers and material scientists can use to investigate plastic part failures. It also provides a brief survey of polymer systems and the key properties that need to be measured during failure analysis. It describes the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy, differential scanning calorimetry, differential thermal analysis, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses the use of X-ray diffraction for analyzing crystal phases and structures in solid materials.

Engineering plastics, as a general class of materials, are prone to the development of internal stresses which arise during processing or during servicing when parts are exposed to environments that impose deformation and/or temperature extremes. Thermal stresses are largely a consequence of high coefficients of thermal expansion and low thermal diffusivities. Although time-consuming techniques can be used to analyze thermal stresses, several useful qualitative tests are described in this article. The classification of internal stresses in plastic parts is covered. The article describes the effects of low thermal diffusivity and high thermal expansion properties, and the variation of mechanical properties with temperature. It discusses the combined effects of thermal stresses and orientation that result from processing conditions. The article also describes the effect of aging on properties of plastics. It explains the use of high-modulus graphite fibers in amorphous polymers.

A failure analysis investigation was conducted on a fractured aluminum tailwheel fork which failed moments after the landing of a privately owned, 1955 twin-engine airplane. Nondestructive evaluation via dye-penetrant inspection revealed no discernible surface cracks. The chemical composition of the sand-cast component was identified via optical emission spectroscopy and is comparable to an aluminum sand-cast alloy, AA 712.0. Metallographic evaluation via optical microscopy and scanning electron microscopy revealed a high degree of porosity in the microstructure as well as the presence of deleterious intermetallic compounds within interdendritic regions. Macrohardness testing produced hardness values which are noticeably higher than standard hardness values for 712.0. The primary fracture surfaces indicate evidence of mixed-mode fracture, via intergranular cracking, cleaved intermetallic particles, and dimpled cellular regions in the matrix. The secondary fracture surface demonstrates similar features of intergranular fracture.

A microstructural analysis has been made of a burner nozzle removed from service in a coal gasification plant. The nozzle was a casting of a Co-29wt%Cr-19wt%Fe alloy. Extensive hot corrosion had occurred on the surface. There was penetration along grain boundaries, and corrosion products in these regions were particularly rich in S, and also contained Al, Si, O, and Cl. The grain boundaries contained Cr-rich particles which were probably Cr23-C6 type carbides. In the matrix, corrosion occurred between the Widmanstatten plates. Particles were found between these plates, most of which were rich in Cr and O, and probably were Cr2-O3 oxides. Other matrix particles were found which were rich in Al, O, and S. The corrosion was related to these grain boundary and matrix particles, which either produced a Cr-depleted zone around them or were themselves attacked.

Plastics or polymers are used in a variety of engineering and nonengineering applications where they are subjected to surface damage and wear. This article discusses the classification of polymer wear mechanisms based on the methodologies of defining the types of wear. The first classification is based on the two-term model that divides wear mechanisms into interfacial and bulk or cohesive. The second is based on the perceived wear mechanism. The third classification is specific to polymers and draws the distinction based on mechanical properties of polymers. In this classification, wear study is separated as elastomers, thermosets, glassy thermoplastics, and semicrystalline thermoplastics. The article describes the effects of environment and lubricant on the wear failures of polymers. It presents a case study on nylon as a tribological material. The article explains the wear failure of an antifriction bearing, a nylon driving gear, and a polyoxymethylene gear wheel.

This article focuses on the types of activities required for the resolution of wear problems. These include examining and characterizing the tribosystem; characterizing and modeling the wear process; obtaining and evaluating wear data; and evaluating and verifying the solution.

A 127 cu m (4,480 cu ft) pressurized railroad tank car burst catastrophically. The railroad tank was approximately 18 m (59 ft) long (from 2:1 elliptical heads), 3 m (10 ft) in OD, and 16 mm (0.63 in.) thick. The chemical and material properties of the tank were to comply with AAR M-128 Grade B. As a result of the explosive failure of the tank car, fragments were ejected from the central region of the car between the support trucks from ground zero to a maximum of approximately 195 m (640 ft). The mode of failure was a brittle fracture originating at a preexisting lamination and crack in the tank wall adjacent to the tank nozzle. The mechanism of failure was overpressurization of the railroad tank car caused by a chemical reaction of the butadiene contents. The interrelationship of the mode, mechanism, and consequences of failure is reviewed to reconstruct the sequence of events that led up to the breach of the railroad tank car. Means to prevent similar reoccurrences are discussed.

Failures of four different 300-series austenitic stainless steel biomedical fixation implants were examined. The device fractures were observed optically, and their surfaces were examined by scanning electron microscopy. Fractography identified fatigue to be the failure mode for all four of the implants. In every instance, the fatigue cracks initiated from the attachment screw holes at the reduced cross sections of the implants. Two fixation implant designs were analyzed using finite-element modeling. This analysis confirmed the presence of severe stress concentrations adjacent to the attachment screw holes, the fatigue crack initiation sites. Conclusions were reached regarding the design of these types of implant fixation devices, particularly the location of the attachment screw holes. The use of austenitic stainless steel for these biomedical implant devices is also addressed. Recommendations to improve the fixation implant design are suggested, and the potential benefits of the substitution of titanium or a titanium alloy for the stainless steel are discussed.

Several large-diameter type 304L stainless steel impeller/propeller blades in a circulating water pump failed after approximately 8 months of operation. The impeller was a single casting that had been modified with a fillet weld buildup at the blade root. Visual examination indicated that the fracture originated near the blade-to-hub attachment in the area of the weld buildup. Specimens from four failed castings and from an impeller that had developed cracks prior to design modification were subjected to a complete analysis. A number of finite-element-method computer models were also constructed. It was determined that the blades failed by fatigue that had been accelerated by stress-corrosion cracking. The mechanism of failure was flow-induced vibration, in which the vortex-shedding frequencies of the blades were attuned to the natural frequency of the blade/hub configuration. A number of solutions involving material selection and impeller redesign were recommended.

The fatigue failure of a wire rope used on a skip hoist in an underground mine has been studied as part of the ongoing research by the Bureau of Mines into haulage and materials handling hazards in mines. Macroscopic correlation of individual wire failures with wear patterns, fractography, and microhardness testing were used to gain an understanding of the failure mechanism. Wire failures occurred predominantly at characteristic wear sites between strands. These wear sites are identifiable by a large reduction in diameter; however, reduction in area was not responsible for the location of failure. Fractography revealed multiple crack initiation sites to be located at other less noticeable wear sites or opposite the characteristic wear site. Microhardness testing revealed hardening, and some softening, at wear sites.

With any polymeric material, chemical exposure may have one or more different effects. Some chemicals act as plasticizers, changing the polymer from one that is hard, stiff, and brittle to one which is softer, more flexible, and sometimes tougher. Often these chemicals can dissolve the polymer if they are present in large enough quantity and if the polymer is not crosslinked. Other chemicals can induce environmental stress cracking (ESC), an effect in which brittle fracture of a polymer will occur at a level of stress well below that required to cause failure in the absence of the ESC reagent. Finally, there are some chemicals that cause actual degradation of the polymer, breaking the macromolecular chains, reducing molecular weight, and diminishing polymer properties as a result. This article examines each of these effects. The discussion also covers the effects of surface embrittlement and temperature on polymer performance.

The purpose of this article is to assist the reader in understanding the role that an engineering expert witness plays in evaluating incidents related to product liability, so that he or she may become better acquainted with the role that an engineer plays in such litigation. The topics covered are admissibility of expert opinions, how to evaluate data, factual evidence, mandatory and voluntary standards, physical evidence, medical records, scientific literature, design decisions evaluation, environment of use, user's contribution, reports of opposing experts, report of findings, and deposition and trial testimonies.

The susceptibility of plastics to environmental failure, when exposed to organic chemicals, can limit their use in many applications. A combination of chemical and physical factors, along with stress, usually leads to a serious deterioration in properties, even if stress or the chemical environment alone may not appreciably weaken a material. This phenomenon is referred to as environmental stress cracking (ESC). The ESC failure mechanism for a particular plastics-chemical environment combination can be quite complex and, in many cases, is not yet fully understood. This article focuses on two environmental factors that contribute to failure of plastics, namely chemical and physical effects.

The circumstances surrounding the in-service failure of a cast Ni-base superalloy (Alloy 713LC) second stage turbine blade and a cast and coated Co-base superalloy (MAR-M302) first stage air-cooled vane in two turbine engines used for marine application are described. An overview of a systematic approach, analyzing the nature of degeneration and failure of the failed components, utilizing conventional metallurgical techniques, is presented. The topographical features of the turbine blade fracture surface revealed a fatigue-induced crack growth pattern, where crack initiation had taken place in the blade trailing edge. An estimate of the crack-growth rate for the stage II fatigue fracture region coupled with the metallographic results helped to identify the final mode of the turbine blade failure. A detailed metallographic and fractographic examination of the air-cooled vane revealed that coating erosion in conjunction with severe hot-corrosion was responsible for crack initiation in the leading edge area.