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A. Ray, D. Mukherjee, B. Sarkar, S. Mishra
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George Goodrich, Ilya Divinsky
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Michael E. Finn, John M. Tartaglia
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George F. Vander Voort
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Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001814
EISBN: 978-1-62708-180-1
... temperature chosen as a compromise between the recommended temperatures for the grades. Excessively high austenitizing temperatures promote grain growth and excessive retained austenite. Most tool steel grades have high carbon contents and rely on the undissolved portion of the carbides to control grain...
Abstract
This article describes the characteristics of tools and dies and the causes of their failures. It discusses the failure mechanisms in tool and die materials that are important to nearly all manufacturing processes, but is primarily devoted to failures of tool steels used in cold-working and hot-working applications. It reviews problems introduced during mechanical design, materials selection, machining, heat treating, finish grinding, and tool and die operation. The brittle fracture of rehardened high-speed steels is also considered. Finally, failures due to seams or laps, unconsolidated interiors, and carbide segregation and poor carbide morphology are reviewed with illustrations.
Book Chapter
Brittle Failure of a Titanium Nitride-Coated High Speed Steel Hob
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001269
EISBN: 978-1-62708-215-0
... homogenization of the carbides in the resultant hob, and lower sulfur content. Carbides Coatings Hobbing cutters Microstructural effects Sulfur Wear M2 UNS T11302 Brittle fracture Background A gear manufacturer reported recurring premature failures of titanium nitrided M2 tool steel gear...
Abstract
Recurring, premature failures occurred in TiN-coated M2 gear hobs used to produce carbon steel ring gears. Fractographic and metallographic examination, microhardness testing, and chemical analysis by means of EDS revealed that the primary cause of failure was a coarse cellular carbide network, which created a brittle path for fracture to occur longitudinally. As the cellular carbide network must be dispersed and refined during hot working of the original bar of material, the hobs were not salvageable. Minor factors contributing to the hob failures were premature wear resulting from lower matrix hardness and high sulfur content of the material, which contributed to lower ductility through increased nucleation sites. It was recommended that the hob manufacturer specify a minimum amount of required reduction for the original bar of tool steel material, to provide for sufficient homogenization of the carbides in the resultant hob, and lower sulfur content.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0047840
EISBN: 978-1-62708-223-5
... Abstract The A2 tool steel mandrel, part of a rolling tool used for mechanically joining two tubes was fractured after making five rolled joints. A 6.4 mm diam hole was drilled by EDM through the square end of the hardened mandrel due to difficulty was experienced in withdrawing the tool...
Abstract
The A2 tool steel mandrel, part of a rolling tool used for mechanically joining two tubes was fractured after making five rolled joints. A 6.4 mm diam hole was drilled by EDM through the square end of the hardened mandrel due to difficulty was experienced in withdrawing the tool. The fracture progressed into the threaded section and formed a pyramid-shape fragment after it was initiated at approximately 45 deg through the hole in the square end. An irregular zone of untempered martensite with cracks radiating from the surface of the hole (result of melting around hole) was revealed by metallographic examination. A microstructure of fine tempered martensite containing some carbide particles was exhibited by the core material away from the hole. Brittle fracture characteristics with beach marks were exhibited by the fracture surfaces which is characteristic of a torsional fatigue fracture. As a corrective measure, the hole through the square end of the mandrel was incorporated into the design of the tool and was drilled and reamed before heat treatment and specified hardness of the threaded portion and square end of the mandrel was reduced.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006818
EISBN: 978-1-62708-329-4
.... Most tool steel grades have high carbon contents and rely on the undissolved portion of the carbides to control grain growth. An excessive austenitizing temperature puts more carbon in solution, thus permitting grain growth as well as excess retained austenite due to suppression of the martensite start...
Abstract
This article discusses failure mechanisms in tool and die materials that are very important to nearly all manufacturing processes. It is primarily devoted to failures of tool steels used in cold working and hot working applications. The processes involved in the analysis of tool and die failures are also covered. In addition, the article focuses on a number of factors that are responsible for tool and die failures, including mechanical design, grade selection, steel quality, machining processes, heat treatment operation, and tool and die setup.
Book Chapter
Influence of Microstructure on the Premature Failure of a Second-Intermediate Sendzimir Mill Drive Roll
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001535
EISBN: 978-1-62708-232-7
... to that in the MC-type isolated carbides, reinforces the fact that carbide inhomogeneity in tool steels is higher in the presence of tungsten ( Ref 8 ). 5. Conclusion Although the average carbide content (3.065 vol%) is apparently normal for this grade of steel, field-to-field variations of carbide volume...
Abstract
Although a precise understanding of roll failure genesis is complex, the microstructure of a broken roll can often unravel intrinsic deficiencies in material quality responsible for its failure. This is especially relevant in circumstances when, even under a similar mill-operating environment, the failure involves a particular roll or a specific batch of rolls. This paper provides a microstructural insight into the cause of premature breakage of a second-intermediate Sendzimir mill drive roll used at a stainless steel sheet rolling plant under the Steel Authority of India Limited. Microstructural issues influencing roll quality, such as characteristics of carbides, tempered martensite, retained austenite, etc., have been extensively studied through optical and scanning electron microscopy, electron-probe microanalysis, image analysis, and x-ray diffractometry. These are discussed to elucidate specific microstructural inadequacies that accentuated the failure. The study reveals that even through retained austenite content is low (6.29 vol%) and martensite is non-acicular, the roll breakage is a consequence of intergranular cracking caused by improper carbide morphology and distribution.
Image
Fracture in a thin medical device manufactured from type D 2 tool steel. (a...
Available to PurchasePublished: 01 January 2002
Fig. 9 Fracture in a thin medical device manufactured from type D 2 tool steel. (a) View showing a fractured massive carbide and associated matrix crack. Scanning electron micrograph. 1187× (b) Cross section through a cracked region in a similar part showing brittle fracture in the carbides
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Image
(a) Flange edge of a roll made from AISI D2 tool steel that chipped off dur...
Available to PurchasePublished: 30 August 2021
Fig. 41 (a) Flange edge of a roll made from AISI D2 tool steel that chipped off during its initial use. Failure was due to poor carbide distribution and morphology, which embrittled the material. (b) Micrograph showing the poor carbide distribution and morphology in the roll. The grain size
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Image
Fracture in a thin medical device manufactured from type D2 tool steel. (a)...
Available to PurchasePublished: 15 January 2021
Fig. 9 Fracture in a thin medical device manufactured from type D2 tool steel. (a) View showing a fractured massive carbide and associated matrix crack. Scanning electron micrograph. Original magnification: 1187×. (b) Cross section through a cracked region in a similar part showing brittle
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Image
A properly heat treated tool of manganese oil-hardening steel has a martens...
Available to PurchasePublished: 01 January 2002
Fig. 4 A properly heat treated tool of manganese oil-hardening steel has a martensitic structure (left) containing fine tempered martensite and carbides. An overheated tool material has an acicular martensitic structure (right) that cracks easily (see Fig. 5 ). Etchant, Nital; 700X.
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Image
(a) Optical microscopy observation of the worn surface of a steel after sli...
Available to PurchasePublished: 15 January 2021
Fig. 4 (a) Optical microscopy observation of the worn surface of a steel after sliding against a tool steel. The presence of parallel grooves due to the action of hard carbides in the tool steel microstructure can be observed. (b) Scanning electron micrograph showing abrasive wear
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Book Chapter
Failure of an ASTM A681-89 H13 Die Segment for Die Casting of Aluminum
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001120
EISBN: 978-1-62708-214-3
... Abstract A segment from a premium-quality H13 tool steel die for die casting of aluminum failed after only 700 shots. The segment was subjected to visual, macroscopic, hardness, and metallographic testing. The investigation revealed that failure occurred as a result of fatigue at an electrical...
Abstract
A segment from a premium-quality H13 tool steel die for die casting of aluminum failed after only 700 shots. The segment was subjected to visual, macroscopic, hardness, and metallographic testing. The investigation revealed that failure occurred as a result of fatigue at an electrical-discharge-machined surface where the resulting rehardened layer had not been removed. This rehardened layer had cracked, providing a source for fatigue initiation.
Book Chapter
Prevention of Machining-Related Failures
Available to PurchaseSeries: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006826
EISBN: 978-1-62708-329-4
... pockets in the machined part that damage the workpiece by increasing the surface roughness and becoming stress raisers. The presence of carbides in cast iron can increase chipping of the cutting tool and have a deleterious effect on surface roughness ( Ref 7 ). Using polished or coated cutting tools...
Abstract
The first part of this article focuses on two major forms of machining-related failures, namely machining workpiece (in-process) failures and machined part (in-service) failures. Discussion centers on machining conditions and metallurgical factors contributing to (in-process) workpiece failures, and undesired surface layers and metallurgical factors contributing to (in-service) machined part failures. The second part of the article discusses the effects of microstructure on machining failures and their preventive measures.
Book Chapter
Thermal Exposure Assessment by Quantitative Microscopy and Selective Etching
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001571
EISBN: 978-1-62708-229-7
... Abstract The accident at Three Mile Island Unit No. 2 on 28 March 1979 was the worst nuclear accident in US history. By Jan 1990, it was possible to electrochemically machine coupons from the lower head using a specially designed tool. The specimens contained the ER308L stainless steel cladding...
Abstract
The accident at Three Mile Island Unit No. 2 on 28 March 1979 was the worst nuclear accident in US history. By Jan 1990, it was possible to electrochemically machine coupons from the lower head using a specially designed tool. The specimens contained the ER308L stainless steel cladding and the A533 Grade B plate material to a depth of about mid-wall. The microstructures of these specimens were compared to that of specimens cut from the Midland, Michigan reactor vessel, made from the same grade and thickness but never placed in service. These specimens were subjected to known thermal treatments between 800 and 1100 deg C for periods of 1 to 100 min. Microstructural parameters in the control specimens and in those from TMI-2 were quantified. Selective etchants were used to better discriminate desired microstructural features, particularly in the cladding. This report is a progress report on the quantification of changes in both the degree of carbide precipitation and delta ferrite content and shape in the cladding as a function of temperature and time to refine the estimates of the maximum temperatures experienced.
Book Chapter
Unidirectional-Bending Fatigue Failure of an A6 Tool Steel Shaft
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0047779
EISBN: 978-1-62708-223-5
... Abstract Two A6 tool steel (free machining grade) shafts, parts of a clamping device used for bending 5.7 cm OD tubing on an 8.6 cm radius, failed simultaneously under a maximum clamping force of 54,430 kg. The shaft was imposed with cyclic tensile stresses due to the clamping force...
Abstract
Two A6 tool steel (free machining grade) shafts, parts of a clamping device used for bending 5.7 cm OD tubing on an 8.6 cm radius, failed simultaneously under a maximum clamping force of 54,430 kg. The shaft was imposed with cyclic tensile stresses due to the clamping force and unidirectional bending stresses resulting from the nature of operation. Nonmetallic oxide-sulfide segregation was indicated by microscopic examination of the edge of the fracture surface. Both smooth and granular areas were revealed on visual examination of the fracture. The shaft was subjected to a low overstress as the smooth-textured fatigue zone was relatively large compared with the crystalline textured coarse final-fracture zone. The fatigue crack was nucleated by the nonmetallic inclusion that intersected the surface and initiated in the 0.25 mm radius fillet at a change in section due to stress concentration. To minimize this stress concentration, a larger radius fillet shaft at the critical change in section was suggested as corrective measure.
Image
The flange edge of a roll made from AISI D2 tool steel that chipped off dur...
Available to PurchasePublished: 01 January 2002
Fig. 41(a) The flange edge of a roll made from AISI D2 tool steel that chipped off during its initial use. Failure was due to poor carbide distribution and morphology, which embrittled the material. See also Fig. 41(b) .
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Image
AISI M2 roughing tool that cracked just after heat treatment. (a) Cracks ac...
Available to PurchasePublished: 01 January 2002
Fig. 17 AISI M2 roughing tool that cracked just after heat treatment. (a) Cracks accentuated with magnetic particles. (b) Microstructural examination revealed a badly overaustenitized condition with a heavy grain-boundary carbide film, coarse plate martensite, and unstable retained austenite
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Image
AISI M2 roughing tool that cracked just after heat treatment. (a) Cracks ac...
Available to PurchasePublished: 30 August 2021
Fig. 17 AISI M2 roughing tool that cracked just after heat treatment. (a) Cracks accentuated with magnetic particles. (b) Microstructural examination revealed a badly overaustenitized condition with a heavy grain-boundary carbide film, coarse plate martensite, and unstable retained austenite
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Book Chapter
Corrosion-Fatigue Fracture of an H21 Tool Steel Safety-Valve Spring in Moist Air
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c0046874
EISBN: 978-1-62708-229-7
... (625 to 750 deg F). Because the spring was enclosed and mounted above the valve, its temperature was probably slightly lower. The 195 mm (7 in.) OD x 305 mm (12 in.) long spring was made from a 35 mm (1 in.) diam rod of H21 hot-work tool steel. It had been in service for about four years and had been...
Abstract
The safety valve on a steam turbogenerator was set to open when the steam pressure reaches 2400 kPa (348 psi). The pressure had not exceeded 1790 kPa (260 psi) when the safety-valve spring shattered into 12 pieces. The steam temperature in the line varied from about 330 to 400 deg C (625 to 750 deg F). Because the spring was enclosed and mounted above the valve, its temperature was probably slightly lower. The 195 mm (7 in.) OD x 305 mm (12 in.) long spring was made from a 35 mm (1 in.) diam rod of H21 hot-work tool steel. It had been in service for about four years and had been subjected to mildly fluctuating stresses. Analysis (visual inspection, 0.3x photographs, 0.7x light fractographs, and metallographic examination) supported the conclusions that the spring failed by corrosion fatigue that resulted from application of a fluctuating load in the presence of a moisture-laden atmosphere. Recommendations included replacing all safety valves in the system with new open-top valves that had shot-peened and galvanized steel springs. Alternatively, the valve springs could be made from a corrosion-resistant metal-for example, a 300 series austenitic stainless steel or a nickel-base alloy, such as Hastelloy B or C.
Book Chapter
Service Failure of a Die Insert Made From AISI D2 Tool Steel
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001121
EISBN: 978-1-62708-214-3
... Abstract An AISI D2 tool steel insert from a forming die used in the manufacture of automotive components failed prematurely during production. Results of various analyses and simulation tests indicated fatigue failure resulting from improper heat treatment. The fatigue fracture originated...
Abstract
An AISI D2 tool steel insert from a forming die used in the manufacture of automotive components failed prematurely during production. Results of various analyses and simulation tests indicated fatigue failure resulting from improper heat treatment. The fatigue fracture originated because of a highly stressed condition produced by a sharp corner combined with low toughness from ineffective tempering. It was recommended that 25 other inserts that belonged to the same die be double tempered.
Book Chapter
Brittle Fracture of a Roll-Assembly Sleeve Due to Improper Microstructure
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0047140
EISBN: 978-1-62708-234-1
... that superficial working of the metal, probably insufficient hot working, produced a microstructure in which the carbide particles were not broken up and evenly distributed. As a result, the grains were totally surrounded with brittle carbide particles. This facilitated the formation of a crack at a fillet...
Abstract
A roll assembly consisting of a forged AISI type 440A stainless steel sleeve shrink fitted over a 4340 steel shaft and further secured with tapered keys on opposite ends was crated and shipped by air. Upon arrival, the sleeve was found to have cracked longitudinally between the keyways. A roll manufacturer had successfully used the above procedure for many years to make them. Analysis (visual inspection; 150x micrograph of sections etched with a mixture of 2 parts HNO3, 2 parts acetic acid, and 3 parts HCI; electron microscopy; and stress testing) supported the conclusion that superficial working of the metal, probably insufficient hot working, produced a microstructure in which the carbide particles were not broken up and evenly distributed. As a result, the grains were totally surrounded with brittle carbide particles. This facilitated the formation of a crack at a fillet in the keyway. Crack growth was rapid once the crack had initiated, causing brittle fracture to occur.
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