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Tito Luiz da Silveira, Francisco Solano Moreira, Miriam Conçeicão Garcia Chavez, Iain Le May
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Sara Fernandez, María José Quintana, José Ovidio García, Luis Felipe Verdeja, Roberto González ...
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in Failure of Supports in a Petrochemical Product Transfer Line
> ASM Failure Analysis Case Histories: Chemical Processing Equipment
Published: 01 June 2019
Fig. 2 Showing creep damage in the pipe in the form of grain boundary sliding and cracking. Unetched.
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001687
EISBN: 978-1-62708-220-4
... properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube. Grain boundary sliding Plastic deformation Spalling Voids HK UNS J94224 Creep fracture/stress rupture The petrochemical...
Abstract
Microstructural examinations on transverse cross sections of a steam reformer tube, showed the presence of large macrovoids elongated in the radial direction and emanating from the internal surface of the tube. The macrovoids were located at the interdendritic regions, and were partially filled by a Mn-Fe bearing chromium oxide film. The areas adjacent to the oxide film were chemically depleted in C, Cr and Mn and rich in Fe and Ni. Associated with this depletion were a large concentration of microvoids. It was suggested that the dissolution of carbides in areas surrounding the macrovoids and the concentration of stresses at their tips, caused extensive localized plastic deformation which led to the formation of microvoids and subsequently to the spalling of the oxide film. The non-protective character of the film induced a progressive deterioration of the grain boundaries properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001736
EISBN: 978-1-62708-220-4
... mechanism, namely grain boundary sliding, relating to the periodic nature of the loading, with high residual stresses being present. Grain boundary sliding Petrochemical equipment Transfer piping Welded joints 316 UNS S31600 Creep fracture/stress rupture Leakage was detected at the welds...
Abstract
Leakage was detected at the welds between stiffening plates and the pipe in a transfer line carrying butane and related petrochemical compounds. The line and reinforcing rings were of AISI 316 stainless steel, the pipe being of 508 mm diam and 6.25 mm wall thickness. The design temperature and pressure were 621 deg C and 2.75 kPa, respectively, while the operating conditions were 579 deg C and 1.03 kPa. The line was insulated. Failure occurred after approximately 90,000 h of operation, shutdowns being approximately two per annum. The cracking occurred at the toe of welds between the plates and the pipe. The creep damage failure was attributed to repeated relaxation cycles of very high thermal stresses of resulting from the periodic shutdowns, temperature fluctuations during service, or both. This failure emphasized the information available from an evaluation of the operative creep mechanism, namely grain boundary sliding, relating to the periodic nature of the loading, with high residual stresses being present.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001011
EISBN: 978-1-62708-229-7
... transfer zone of the coil. It showed that many damage mechanisms may combine in the transition from fracture initiation to final failure. The presence of grain boundary sliding as an indication of creep damage was useful in the characterization of the stress level as high and showed that the process...
Abstract
After some 87,000 h of operation, failure took place in the bend of a steam pipe connecting a coil of the third superheater of a steam generator to the outlet steam collector. The unit operated at 538 deg C and 135 kPa, producing 400 t/h of steam. The 2.25Cr-1Mo steel pipe in which failure took place was 50.8 mm in diam with a nominal wall thickness of 8 mm. It connected to the AISI 321 superheater tube by means of a butt weld and was one of 46 such parallel connecting tubes. The Cr-Mo tubing was situated outside the heat transfer zone of the superheater. The overall sequence of failure involved overheating of the Cr-Mo outlet tubes, heavy oxidation, oxide cracking on thermal cycling, thermal fatigue cracking plus oxidation, creep-controlled crack growth, and rapid plastic deformation and rupture. This failure was indicative of excess temperature of the steam coming from the heat transfer zone of the coil. It showed that many damage mechanisms may combine in the transition from fracture initiation to final failure. The presence of grain boundary sliding as an indication of creep damage was useful in the characterization of the stress level as high and showed that the process of creep was not operative throughout the life of the equipment.
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in Metallographic Studies of a Reformer Tube Failure Due to Thermal Fatigue
> ASM Failure Analysis Case Histories: Chemical Processing Equipment
Published: 01 June 2019
Fig. 6 Details (three views at increasing magnification) of remnant external cracks adjacent to the repair weld (unetched material). The grain boundary creep pore was formed by grain boundary sliding.
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Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001675
EISBN: 978-1-62708-220-4
... removal of the external cracks by grinding. Fig. 6 Details (three views at increasing magnification) of remnant external cracks adjacent to the repair weld (unetched material). The grain boundary creep pore was formed by grain boundary sliding. Fig. 7 Details of cracking shown...
Abstract
The failure of a reformer tube furnace manifold has been examined using metallography. It has been shown that the cause of failure was thermal fatigue; the damage was characterized by the presence of voids produced by creep mechanisms operating during the high temperature cycle under high local stress. The study indicates that standard metallographic procedures can be used to identify failure modes in high temperature petrochemical plants.
Image
in Metallographic Studies of a Reformer Tube Failure Due to Thermal Fatigue
> ASM Failure Analysis Case Histories: Chemical Processing Equipment
Published: 01 June 2019
Fig. 7 Details of cracking shown in Figure 5 with the SEM (unetched). The damage was produced by grain boundary sliding in alternate directions following reversal of the local stress. Figures 7e and 7f show, respectively, the distribution of chromium and nickel in the area of 7d .
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001598
EISBN: 978-1-62708-232-7
... uses single crystal turbine blades. Obtaining a single crystal in the drain tube is highly unlikely. Therefore, the high temperature weaknesses of the grain boundaries and the tendency of grain boundary sliding and void formation need to be addressed. One possible solution to the tendency for creep...
Abstract
The metallurgical condition of a cylindrical induction melter (CIM) vessel was evaluated after approximately 375 h of operation over a two-year span at temperatures between 1400 to 1500 deg C. Wall thinning and significant grain growth was observed in the lower portion of the conical section and the drain tube. No through-wall penetrations were found in the cylindrical and conical sections of the CIM vessel and only one leak site was identified in the drain tube. Failure of the drain tube was associated with localized overheating and creep. The observed degradation resulted from cumulative service at elevated temperature. A recommendation was made to implement a support for the conical section of the CIM and to increase the wall thickness of the drain tube. Thus, the possibility of drain tube misalignment in the induction coils and localized over heating will be minimized. In addition, the use of grain stabilized Pt/Rh alloy should be evaluated as a method to prevent grain growth.
Book Chapter
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001816
EISBN: 978-1-62708-241-9
... components superplastic deformation boundary sliding dislocation creep high-strength low alloy steel decohesions traction testing grain size elongation Ti-Nb microalloyed ultrafine-grained steel (UGS steel, general) high-strength low-alloy steel (HSLA steel, general) Introduction A material...
Abstract
This paper describes the superplastic characteristics of shipbuilding steel deformed at 800 °C and a strain rate less than 0.001/s. After the superplastic deformation, the steel presents mixed fractures: by decohesion of the hard (pearlite and carbides) and ductile (ferrite) phases and by intergranular sliding of ferrite/ferrite and ferrite/pearlite, just as it occurs in stage III creep behavior. The behavior is confirmed through the Ashby-Verrall model, according to which the dislocation creep (power-law creep) and diffusion creep (linear-viscous creep) occur simultaneously.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006806
EISBN: 978-1-62708-329-4
... (chemical-bonded boundary lubricant, lamellar solid lubricant) or lubricated with available moisture or applied lubricant. Fig. 2 Configurations of various sliding bearings The bearings meant for more severe duty must be designed and fabricated more precisely, and they more likely require...
Abstract
A mechanical part, which supports the moving part, is termed a mechanical bearing and can be classified into rolling (ball or roller) bearings and sliding bearings. This article discusses the failures of sliding bearings. It first describes the geometry of sliding bearings, next provides an overview of bearing materials, and then presents the various lubrication mechanisms: hydrostatic, hydrodynamic, boundary lubrication, elastohydrodynamic, and squeeze-film lubrication. The article describes the effect of debris and contaminant particles in bearings. The steps involved in failure analysis of sliding bearings are also covered. Finally, the article discusses wear-damage mechanisms from the standpoint of bearing design.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001188
EISBN: 978-1-62708-235-8
... Abstract A short fracture section of a forged and normalized Ck 35 (DIN 17200) steel slide showed three distinct zones: a dark colored crystalline area, an incipient crack propagating into a far advanced, rubbed fracture surface, and a fine crystalline final break. Metallographic examination...
Abstract
A short fracture section of a forged and normalized Ck 35 (DIN 17200) steel slide showed three distinct zones: a dark colored crystalline area, an incipient crack propagating into a far advanced, rubbed fracture surface, and a fine crystalline final break. Metallographic examination showed the dark incipient crack was present before the last heat treatment and was oxidized and decarburized prior to the conclusion of the annealing process. The crack ran perpendicular to the fiber, so it was not formed before or during forging. It was a thermal stress crack produced during flame cutting of the middle section of the slide. The initial crack acted as a sharp notch favoring the formation of the fatigue fracture which lead to the failure of the slide.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006911
EISBN: 978-1-62708-395-9
... from boundary sliding on asperity contacts to fully sliding on fluid films can be described using the Stribeck curve ( Fig. 4 ), which displays how increasing fluid film thickness ratio λ affects the friction coefficient μ . The fluid film thickness ratio is the ratio of fluid film thickness...
Abstract
Tribology is the study of contacting materials in relative motion and more specifically the study of friction, wear, and lubrication. This article discusses the classification and the mechanisms of friction, wear, and lubrication of polymers. It describes the tribological applications of polymers and the tribometers and instrumentation used to measure the tribological properties of polymers. The article discusses the processes involved in calculating the wear rate of polymers and the methods of characterization of the sliding interface. It provides information on the pressure and velocity limit of polymer composites and polymer testing best practices.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006789
EISBN: 978-1-62708-295-2
... is to adopt a suitable lubrication, if possible. If the Λ-factor is high (typically in excess of 1), wear is negligible, because the asperities do not touch each other during sliding. In boundary lubrication, adhesion wear takes place but is 1 to 3 orders of magnitude less than in the corresponding dry...
Abstract
This article considers the main characteristics of wear mechanisms and how they can be identified. Some identification examples are reported, with the warning that this task can be difficult because of the presence of disturbing factors such as contaminants or possible additional damage of the worn products after the tribological process. Then, the article describes some examples of wear processes, considering possible transitions and/or interactions of the mechanism of fretting wear, rolling-sliding wear, abrasive wear, and solid-particle erosion wear. The role of tribological parameters on the material response is presented using the wear map concept, which is very useful and informative in several respects. The article concludes with guidelines for the selection of suitable surface treatments to avoid wear failures.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001004
EISBN: 978-1-62708-229-7
...) fracture, viz., in low temperature RTE fracture, initiation and propagation of microcracks are rate controlling while at high temperatures the nucleation and growth of creep cavitation, dislocation mobility and grain boundary sliding are important. Wilkinson et al ( 6 ) observed that the ductility of P...
Abstract
The results of a failure analysis of a series of Cr-Mo-V steel turbine studs which had experienced a service lifetime of some 50,000 h are described. It was observed that certain studs suffered complete fracture while others showed significant defects located at the first stress bearing thread. Crack extension was the result of marked creep embrittlement and reverse temper embrittlement (RTE). Selected approaches were examined to assess the effects of RTE on the material toughness of selected studs. It was observed that Auger electron microscopy results which indicated the extent of grain boundary phosphorus segregation exhibited a good relationship with ambient temperature Charpy data. The electrochemical polarization kinetic reactivation, EPR, approach, however, proved disappointing in that the overlapping scatter in the minimum current density, Ir, for an embrittled and a non-embrittled material was such that no clear decision of the toughness properties was possible by this approach. The initial results obtained from small punch testing showed good agreement with other reported data and could be related to the FATT. Indeed, this small punch test, combined with a miniature sample sampling method, represents an attractive approach to the toughness assessment of critical power plant components.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001291
EISBN: 978-1-62708-215-0
... Abstract Examination of several fighter aircraft main landing gear legs revealed unusual cracking in the hard chromium plating that covered the sliding section of the inner strut. The cracking was associated with cracks in the 35 NCD 16 steel beneath the plating. A detailed investigation...
Abstract
Examination of several fighter aircraft main landing gear legs revealed unusual cracking in the hard chromium plating that covered the sliding section of the inner strut. The cracking was associated with cracks in the 35 NCD 16 steel beneath the plating. A detailed investigation revealed that the cracking was caused by the combination of incorrect grinding procedure, the presence of hydrogen, and fatigue. The grinding damage generated tensile stresses in the steel, which caused intergranular cracking during the plating cycle. The intergranular cracks were initiation sites for fatigue crack growth during service. It was recommended that the damaged undercarriage struts be withdrawn from service pending further analysis and development of a repair technique.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006781
EISBN: 978-1-62708-295-2
... of creep may manifest as grain-boundary movement or sliding, dislocation glide, dislocation glide plus climb, and/or the diffusion of chemical species within the lattice. The rate equation that governs most forms of crystalline creep may be simplified to the following functional form ( Ref 2 ): (Eq 2...
Abstract
Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material, temperature-assisted grain-boundary evolution, and temperature-driven surface oxidation, among other things. This article discusses some of the major aspects and challenges of dealing with TMF life prediction. It describes the damage mechanisms of TMF and covers various experimental techniques to promote TMF damage mechanisms and elucidate mechanism coupling interactions. In addition, life modeling in TMF conditions and a practical application of TMF life prediction are presented.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006780
EISBN: 978-1-62708-295-2
... enough, dislocations rearrange and annihilate through recovery events. On a more macroscopic scale, creep deformation also produces microstructural changes, such as slip bands, grain-boundary sliding, cavity formation and growth, and cracking (grain boundary, interphase boundary, and transgranular...
Abstract
The principal types of elevated-temperature mechanical failure are creep and stress rupture, stress relaxation, low- and high-cycle fatigue, thermal fatigue, tension overload, and combinations of these, as modified by environment. This article briefly reviews the applied aspects of creep-related failures, where the mechanical strength of a material becomes limited by creep rather than by its elastic limit. The majority of information provided is applicable to metallic materials, and only general information regarding creep-related failures of polymeric materials is given. The article also reviews various factors related to creep behavior and associated failures of materials used in high-temperature applications. The complex effects of creep-fatigue interaction, microstructural changes during classical creep, and nondestructive creep damage assessment of metallic materials are also discussed. The article describes the fracture characteristics of stress rupture. Information on various metallurgical instabilities is also provided. The article presents a description of thermal-fatigue cracks, as distinguished from creep-rupture cracks.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006794
EISBN: 978-1-62708-295-2
... Corrosive wear can occur in different forms, depending on the wearing condition. A few typical forms of corrosive wear encountered in industry are discussed here. Abrasion-Corrosion This form of deterioration is the material removal caused by sliding of a harder, rough counterface across the target...
Abstract
Corrosive wear is defined as surface damage caused by wear in a corrosive environment, involving combined attacks from wear and corrosion. This article begins with a discussion on several typical forms of corrosive wear encountered in industry, followed by a discussion on mechanisms for corrosive wear. Next, the article explains testing methods and characterization of corrosive wear. Various factors that influence corrosive wear are then covered. The article concludes with general guidelines for material selection against corrosive wear.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003546
EISBN: 978-1-62708-180-1
... the grain-boundary sliding Grain-boundary carbides (in polycrystalline materials) to reduce the creep rate by inhibiting grain-boundary sliding The way in which cracking occurs could be envisioned as oxidation of a grain boundary at high temperatures and cracking by slip-band impingement at low...
Abstract
Thermomechanical fatigue (TMF) refers to the process of fatigue damage under simultaneous changes in temperature and mechanical strain. This article reviews the process of TMF with a practical example of life assessment. It describes TMF damages caused due to two possible types of loading: in-phase and out-of-phase cycling. The article illustrates the ways in which damage can interact at high and low temperatures and the development of microstructurally based models in parametric form. It presents a case study of the prediction of residual life in a turbine casing of a ship through stress analysis and fracture mechanics analyses of the casing.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003565
EISBN: 978-1-62708-180-1
... from the dry case. Thus, a boundary-lubricated, normal-impact contact is essentially quasi-dry. Wear is, therefore, not likely to be reduced with lubrication of a normal contact. In a lubricated compound-impact contact, due to the tendency for a full film to form, a superimposed sliding speed...
Abstract
This article discusses the generic features of impact wear on metals, ceramics, and polymers. It describes normal impact wear and compound impact wear, as well as the features of impact wear testing apparatus such as ballistic impact wear apparatus and pivotal hammer impact wear apparatus. Most mechanical components continue to be functional beyond the zero wear limit, and their usefulness is normally connected with the loss of a specific depth of material. The article reviews the zero impact wear model and some measurable impact wear models. It presents a case study illustrating the impact of wear failure on automotive engine inlet valves and seat inserts.
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