The center portions of two adjacent low-carbon steel boiler tubes (made to ASME SA-192 specifications) ruptured during a start-up period after seven months in service. It was indicated by reports that there had been sufficient water in the boiler two hours before start-up. The microstructure near the rupture edge was revealed by metallographic examination to consist of ferrite and acicular martensite or bainite. The microstructure and the observed lack of cold work indicated a temperature above the transformation temperature of 727 deg C had been reached. Swelling of the tubes was disclosed by the wall thickness and OD of the tubing. The tubes were concluded to have failed due to rapid overheating.

A recuperator used for preheating the combustion air for a rolling mill furnace failed after a relatively short service time because of leakage of the pipes in the colder part. The 6 % chrome steel pipes used for the warmer part connected by means of welding with austenitic electrodes to the unalloyed mild steel pipe of larger diam. Visual inspection showed corrosion and deep, trench-like erosion over the entire circumference of the seam on the side of the thicker mild steel pipe. Examination using the V2-A solution for picral etch showed the microstructure of the unalloyed pipe had become coarse-grained and acicular, and the microstructure of the welding seam had become predominantly martensitic as a result of the mixing of the weld metal with the fused pipe material. The chrome steel pipe had become partially transformed to martensite or bainite at the transition to the weld. Thus, the failure occurred due to typical contact corrosion wherein the alloyed welding seam represented the less noble electrode. The martensitic structure may have contributed to the failure as well. Due to the typical nature of the failure, no recommendations were made.

A deformed steel tube was received for failure analysis after buckling during a heat-treat operation. The tube was subjected to various metallurgical tests as well as nondestructive testing to confirm the presence of residual stresses. The microstructure of the tube was found to be homogenous and had no banded structure. However, x-ray diffraction analysis confirmed the presence of up to 6% retained austenite which likely caused the tube to buckle during the 910 °C heat treating procedure.

This article provides an overview of the effects of various material- and process-related parameters on residual stress, distortion control, cracking, and microstructure/property relationships as they relate to various types of failure. It discusses phase transformations that occur during heat treating and describes the metallurgical sources of stress and distortion during heating and cooling. The article summarizes the effect of materials and the quench-process design on distortion and cracking and details the effect of cooling characteristics on residual stress and distortion. It also provides information on the methods of minimizing distortion and tempering. The article concludes with a discussion on the effect of heat treatment processes on microstructure/property-related failures.

A steel socket pipe conduit NW 150 cracked open during pressure testing next to the weld seam almost along the entire circumference. The crack occurred in part in the penetration notch and in part immediately adjacent to it. While the uncracked pipe showed the light etch shading of a low-carbon steel in which the zone heated during welding was delineated only slightly next to the seam, the other pipe was etched much darker, i.e., higher in carbon, and the heated zone appeared to stand out darkly against the basic material. The overlapping weld was defect-free and dense. The uncracked pipe consisted of soft steel that obviously was made for this purpose, while the cracked pipe consisted of a strongly-hardenable steel which contained not only more carbon and manganese than customary but also a considerable amount of chromium. Therefore, the damage was caused by a mix-up of materials that allowed an unsuitable steel to be used for the weldment.

A pipe in the lateral wall of a boiler powering an aircraft carrier flat-top boat failed during a test at sea. The pipe was made from ASTM 192 steel, an adequate material for the application. Microstructural analysis along with equipment operating records provided valuable insight into what caused the pipe to rupture. Although the pipe had been replaced just 50 h before the accident, the analysis revealed incrustations and corrosion pits on the inner walls and oxidation on the outer walls. Microstructural changes were also observed, indicating that the steel was exposed to high temperatures. The combined effect of pitting, incrustations, and phase transformations caused the pipe to rupture.

Textile-machine crankshafts forged from 4140 steel fractured transversely on one cheek during one to three years of service. The cause of failure for two forgings (one complete fractured forging and second a section that contained the shorter shaft fracture cheek) was determined. Indication of fatigue failure was revealed by visual examination of the fracture surfaces. Rough grooves from hot trimming of the flash were visible on the surface of the cheeks. The outer face of one cheek of the throw on the forging contained shallow surface folds. Slightly decarburized forged surface was identified around one of the folds and a fatigue crack initiated in the fold and propagated across the cheek. Properties representative of 4140 steel, quenched and tempered to a hardness of 20 to 22 HRC, were observed. Tempered bainite was revealed in the general microstructure. As a corrective measure, the forgings were normalized, hardened and tempered to 28 to 32 HRC before being machined to increase fatigue strength and extremely rough surfaces were removed by careful grinding.

Examples of metallic inclusions in steels of various types are presented. The structure of an inclusion in an annealed Fe-1C-1.5Cr steel consisted of ferrite with lamellar pearlite. The carbon content of the inclusion was therefore considerably lower than that of the chromium steel and was adapted to the latter by diffusion only at the periphery of the inclusion. In another section of a hardened piece of the same chromium steel, the steel in this case had a structure of martensite with hypereutectic carbide, while the inclusions consisted of a very fine laminated eutectoid of the lower pearlite range (Troostite). In a pipe of 18-8 austenitic stainless steel a weakly magnetizable spot of limited size was found. This inclusion too was probably more alloy-deficient than the austenitic steel, similar to the ones described above. All three cases were casting defects.

A 13/16-in. hex socket failed while in use. Analysis (hardness testing, optical and scanning electron microscopy, and EDS) revealed that the socket was made of low carbon steel formed in a powder metallurgy process. A number of flaws were found including nonuniform wall thickness, poor geometric design with sharp corners as stress raisers, and incomplete sintering evidenced by unsintered particles. These were determined to be the primary cause of failure, although inclusions on the fracture surface containing S and Al may have played a role as well.

Failures of 10Cr-Mo9-10 and X 20Cr-Mo-V12-1 superheated pipes during service in steam power generation plants are described. Through micrographic and fractographic analysis, creep and overheating were identified as the cause of failure. The Larson-Miller parameter is computed, as a function of oxidation thickness, temperature and time, confirming the creep failure diagnostic.

A large pressure vessel designed for use in an ammonia plant failed during hydrostatic testing. It was fabricated from ten Mn-Cr-Ni-Mo-V steel plates which were rolled and welded to form ten cylindrical shell sections and three forgings of similar composition. The fracture surfaces were metallographically examined to be typical for brittle steel fracture and associated with the circumferential weld that joined the flange forging to the first shell section. Featureless facets in the HAZ were observed and were revealed to be the fracture-initiation sites. Pronounced banding in the structure of the flange forging was revealed by examination. A greater susceptibility to cracking was interpreted from the higher hardenability found within the bands. Stress relief was concluded to have not been performed at the specified temperature level (by hardness and impact tests) which caused the formation of hard spots. The mode of crack propagation was established by microstructural examination to be transgranular cleavage. It was concluded that failure of the pressure vessel stemmed from the formation of transverse fabrication cracks in the HAZ fostered by the presence of hard spots. It was recommended that normalizing and tempering temperatures be modified and a revised forging practice explored.

This article introduces some of the general sources of heat treating problems with particular emphasis on problems caused by the actual heat treating process and the significant thermal and transformation stresses within a heat treated part. It addresses the design and material factors that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated with nonferrous heat treatments. The processes involved in cold working of certain ferrous and nonferrous alloys are also covered.

A steam-pressurized Yankee dryer shell ruptured during normal operation. Cracking had occurred around much of the circumference at the drive end of the shell, which measured 3.7 m (12 ft) in diameter by 3.4 m (11 ft) long with a head bolted to each end. The crack initiated at a 90 deg corner in contact with the edge of the head. The material was a hardened gray cast iron containing 2.8% Ni and 1.2% Mo. Based on the results of visual, nondestructive, metallographic, and chemical analyses, it was concluded that failure occurred after corrosion fatigue cracking had weakened the shell. An ultrasonic examination of all Yankee dryers of the same type was recommended to look for cracking at the edge of the shell. Modification of the head-to-shell joint was recommended as well.

Two identical “D” tube package boilers, installed at separate plants, experienced a number of tube ruptures after relatively short operating times. The tubes, which are joined by membranes, experienced localized bulging and circumferential cracking along the fireside crown as a result of overheating and thermal fatigue. It was recommended that recent alterations to the steam-drum baffling be remodified to improve circulation in the boiler and prevent further overheating. Several thermocouples were attached to tubes in problem areas of the boiler to monitor the effects of the steam-drum modifications on tube wall temperatures.

The first part of this article focuses on two major forms of machining-related failures, namely machining workpiece (in-process) failures and machined part (in-service) failures. Discussion centers on machining conditions and metallurgical factors contributing to (in-process) workpiece failures, and undesired surface layers and metallurgical factors contributing to (in-service) machined part failures. The second part of the article discusses the effects of microstructure on machining failures and their preventive measures.

An anchorage plate which fractured was one of a pair used as intermediate members through which the boom suspension ropes were attached to the jury-mast of an excavator. Failure of the plate released the ropes on one side of the boom, resulting in extensive damage to the latter and also bending of the other anchorage plate. The anchorage plates were 23 x 9 in. and had been flame-cut from mild steel plate. Collars were fillet-welded on each side at both ends to provide extra bearing area for the pins. Holes had then been flame-cut slightly under size and bored to final dimensions. The plates were given a slight set after flame-cutting to provide a more direct line of pull for the ropes. The fracture surface was bounded by narrow lips, indicative of shear failure. Failure of the anchorage plate was attributed to cracks present at the junctions of the fillet welds, and deficient notch-ductility of the material from which the plates were made.

Sucker-rod pumps are operating in very aggressive environments in oil well production. The combined effect of a corrosive environment and significant mechanical loads contribute to frequent cases of failure of the rod string during operation. Standards and recommendations have been developed to control and avoid those failures. This study presents various failure cases of sucker rods in different applications. The heat treatment of the steel material and the resulting microstructure are an important factor in the behavior of the sucker rod. A spheroidized microstructure presents a weaker resistance to corrosion affecting the rod life. Non-metallic inclusions are a pitting preferential site leading to fatigue crack initiation. Heterogeneous microstructure as banded martensite and ferrite/pearlite decreases the ductility of the material affecting the fatigue propagation resistance.

A fire in a storage yard engulfed several propane delivery trucks, causing one of them to explode. A series of elevated-temperature stress-rupture tears developed along the top of the truck-mounted tank as it was heated by the fire. Unstable fracture then occurred suddenly along the length of the tank and around both end caps, following the girth welds that connect them to the center portion of the tank. The remaining contents of the tank were suddenly released, aerosolized, and combusted, creating a powerful boiling liquid expanding vapor explosion (BLEVE). Based on the metallography of the tank pieces, the approximate tank temperature at the onset of explosion was determined. Metallurgical analysis provided additional insights as well as a framework for making tanks less susceptible to this destructive failure mechanism.

Rolling-contact fatigue (RCF) is a common failure mode in components subjected to rolling or rolling-sliding contact. This article provides a basic understanding of RCF and a broad overview of materials and manufacturing techniques commonly used in industry to improve component life. A brief discussion on coatings to improve surface-initiated fatigue and wear is included, due to the similarity to RCF and the increasing criticality of this failure mode. The article presents a working knowledge of Hertzian contact theory, describes the life prediction of rolling-element bearings, and provides information on physics and testing of rolling-contact fatigue. Processes commonly used to produce bearings for demanding applications are also covered.

Hardenability evaluation is typically applied to heat treatment process control, but can also augment standard metallurgical failure analysis techniques for steel components. A comprehensive understanding of steel hardenability is an essential complement to the skills of the metallurgical failure analyst. The empirical information supplied by hardenability analysis can provide additional processing and service insight to the investigator. The intent of this paper is to describe some applications of steel thermal response concepts in failure analysis, and several case studies are included to illustrate these applications.