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alkaline etching

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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0046227
EISBN: 978-1-62708-217-4
... milled section of the floor. An alkaline etch-type cleaner was used on the panels before chemical milling and before painting. Various tests and measurements indicated that the aluminum alloy used for the fuel-tank floors conformed to the specifications for 7178-T6. Low power magnification, fractographs...
Image
Published: 01 June 2019
Fig. 3 a). Structure of a sliver, etch: alkaline sodium picramate. View. 100× unetched: steel etched: alloy. b). Structure of a sliver, etch: alkaline sodium picramate. Alloy. 500× More
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001785
EISBN: 978-1-62708-241-9
..., and metallurgical analyses. SEM imaging revealed microvoid coalescence within the fracture zone. The microvoids were flat and smooth edged indicating insufficient bonding. In addition, a cross sectional sample, mounted and etched using alkaline chromate, revealed an oxygen-rich zone in the jaw. It was concluded...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c9001183
EISBN: 978-1-62708-223-5
... ( Fig. 2 ). During treatment with sodium hydroxide or alkaline sodium picrate solution the alloy zone was etched ( Figs. 3 ) and the metal completely dissolved. Fig. 1 Section through a sliver. 10× a). Etch: Nital. Section through a sliver. 10×. b). Etch: Sodium hydroxide 1:10. Fig. 2...
Image
Published: 01 January 2002
Fig. 37 Failure caused by a forging lap in a sledge-hammer head. (a) Cracks on the striking face soon after the hammer was first used. (b) A hot alkaline chromate etch revealed oxygen enrichment (white region) adjacent to the crack. 65× More
Image
Published: 30 August 2021
Fig. 37 Failure caused by a forging lap in a sledgehammer head. (a) Cracks on the striking face soon after the hammer was first used. (b) A hot alkaline chromate etch revealed oxygen enrichment (white region) adjacent to the crack. Original magnification: 65× More
Image
Published: 01 January 2002
Fig. 36 Metallographic samples from the ring forging shown in Fig. 35 . (a) Macroetching (10% aqueous nitric acid) of a disk cut through the ring forging revealed decarburization around the cracks. 0.75×. (b) Etching of a polished section with a hot alkaline chromate solution revealed oxygen More
Image
Published: 30 August 2021
Fig. 36 Metallographic samples from the ring forging shown in Fig. 35 . (a) Macroetching (10% aqueous nitric acid) of a disk cut through the ring forging revealed decarburization around the cracks. Original magnification: 0.75×. (b) Etching of a polished section with a hot alkaline chromate More
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001321
EISBN: 978-1-62708-215-0
... on the crown of the top tubes and located in an area near the upward bend of the tube. The inside of all the tubes were covered with a loosely adherent, black, alkaline, powdery deposit comprised mainly of magnetite. The corroded areas, however, had relatively less deposit. The morphology of the corrosion...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.rail.c9001175
EISBN: 978-1-62708-231-0
... of the boiler was polished and etched with Fry-solution, which revealed parallel striations formed due to the cold bending of the plate. The zones of slip were concentrated around the rivet holes. The cracks were formed here. The structure examination proved that the cracks had taken an exactly intercrystalline...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0048665
EISBN: 978-1-62708-217-4
... confirmed that neither carburization nor decarburization had occurred on the surface of either pin. Alkaline chromate etching confirmed that no intergranular oxidation products were present. The microstructure was typical of tempered martensite and was satisfactory. Conclusions Overdriving...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001814
EISBN: 978-1-62708-180-1
.... Macrostructural examination, either by cold etching (more common) or hot etching, is very useful for detecting gross problems. Prior-austenite grain size is frequently evaluated by the Shepherd fracture grain size technique, a simple but accurate approach. X-ray diffraction can be used to determine the amount...
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006818
EISBN: 978-1-62708-329-4
.... Macrostructural examination, either by cold etching (more common) or hot etching, is very useful for detecting gross problems. Prior-austenite grain size is frequently evaluated by the Shepherd fracture grain size technique, a simple but accurate approach. X-ray diffraction can be used to determine the amount...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001335
EISBN: 978-1-62708-215-0
... the height of the problem in an attempt to eliminate the tube embrittlement, including the alkaline dip, pickling operation, furnace atmosphere, drawing lubricant, and temperature control during hot drawing and annealing. Furthermore, tube embrittlement was not always observed, but when present was typically...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001109
EISBN: 978-1-62708-214-3
..., and probably not protective. Typical unetched and etched microstructures near the top surface of the grate bar are shown in Fig. 3 , respectively. Upon etching, the internal microstructure showed coalescence of carbide particles outlining the cored cast structure, as well as the presence of a lamellar...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001396
EISBN: 978-1-62708-229-7
... to this solution at 300°/400°C. showed an increase in weight in contrast to the reduction which occurred in alkaline solutions, and the black oxide film that was formed was of a much greater thickness. Other specimens, treated in a stainless, as opposed to a mild, steel vessel, showed consistently high weight...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001773
EISBN: 978-1-62708-241-9
... Specimen at leak location, designations ( a )–( d ) identify locations of photomicrographs shown in Fig. 11 (etched with 10% oxalic acid) Fig. 11 ( a ) Parent microstructure, Plate A; equiaxed austenitic grain structure characteristic of Grade 316L; indication of cold work (typical Plates...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001818
EISBN: 978-1-62708-180-1
... the carbon content of the base metal. This high hardness is consistent with the carbon content and indicates a high susceptibility to cracking upon cooling or deformation. Fig. 5 Section through arc-gouged drain groove showing thin layer of dendritic structure containing cracks. Etched with nital. 55...
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006825
EISBN: 978-1-62708-329-4
... and polished-and-etched samples by optical and electron microscopy forms a significant part of the failure investigation. Besides providing information on various microstructural features, such as cracks, porosity, inclusions, segregation, phase distribution, and others, it also reveals the effect...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001813
EISBN: 978-1-62708-180-1
.... These pits are readily visible in Fig. 4(b) , a close-up view of one rivet hole, because their surfaces were covered with nickel plating that was not removed during grinding and etching of the specimen. The pits as well as other defects found at the rivet holes and at the bottom end of the spring were...