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X-ray diffraction

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Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006768
EISBN: 978-1-62708-295-2
...) Micrograph. Source: Ref 53 Fig. 20 Applied bending load and number of cycles to failure, R = −1, for Waspaloy specimen. Source: Ref 53 Fig. 26 Comparison of residual stress on the inner diameter of shot-peened coil springs in new and used conditions using x-ray diffraction...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003528
EISBN: 978-1-62708-180-1
... of distance from the maximum stress concentration in the radius of a tiedown socket Fig. 9 X-ray diffraction stress versus applied stress on (a) as-received and (b) electropolished surfaces Fig. 27 Plot of the change in the compressive residual stress due to heat treatment Fig. 28...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0090639
EISBN: 978-1-62708-227-3
... due to the cold-working coining process, and high residual stresses created by welding. Recommendations included the removal of the brittle, carbon-rich transformed martensite layer introduced by flame cutting and the application of a localized stress-relief heat treatment process. X-ray diffraction...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001616
EISBN: 978-1-62708-229-7
... from Stage 2 (where corrosion was low) and Stage 3 (severe corrosion) were taken and subjected to visual inspection, SEM, x-ray diffraction, microhardness measurement, and chemical and microstructural analysis. It was determined that extended non-operation of the plant resulted in the settlement...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001560
EISBN: 978-1-62708-217-4
... both combustion products from the cartridges and corrosion products from the chamber, were analyzed using elemental analysis and x-ray diffraction techniques. Electrochemical polarization techniques were also utilized to estimate corrosion rates. Aerospace engines Aircraft components Breech...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0046512
EISBN: 978-1-62708-234-1
... of deposits scraped from the aluminum spacer and the vellum gasket were identified by x-ray diffraction as molybdenum disulfide. Deposits taken from the nickel-plated steel housing were not completely identified. Analysis indicated, however, that nickel formate dihydrate was one of the constituents...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001674
EISBN: 978-1-62708-234-1
... a preferential attack of the gold. To investigate the problem, a matrix of test units was produced and analyzed. Scanning electron microscopy, EDX analysis, and x-ray diffraction techniques were used to determine the extent of the corrosion and identify the corrosion products. The results indicated...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c0091897
EISBN: 978-1-62708-236-5
... the spacer sleeve, roller bearing, and lockwasher were identified by x-ray diffraction as ferric oxide (α-Fe 2 O 3 ) with minor constituents of metallic iron and copper. Discoloration of the deposit was caused by the grease lubricant and mishandling during disassembly. Spectrochemical analysis...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.rail.c9001665
EISBN: 978-1-62708-231-0
..., scanning electron microscopy, EDXA, and x-ray mapping were used to study the steel in the vicinity of this part of the fracture surface. It was found to be contaminated with copper. Debye-Scherrer x-ray diffraction patterns obtained from the scale showed that it consisted of magnetite and hematite...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001286
EISBN: 978-1-62708-215-0
... measured by x-ray diffraction. The results indicated that the stamped brake discs had failed by fatigue caused by a tensile residual stress pattern in the fillet. The residual stress pattern was attributed to the change in manufacturing process from casting to stamping. Use of a manufacturing process...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001107
EISBN: 978-1-62708-214-3
... analysis of the liner material was performed using scanning electron rricroscopy/energy-dispersive spectroscopy Results indicated that the alloy composition was representative of alloy 800. Corrosion or Wear Deposits X-ray diffraction analysis indicated that the carbides were primarily chromium...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001109
EISBN: 978-1-62708-214-3
... years to approximately 9 months. Several corroded grate bars were examined metallographically and by electron microscopy to determine the causes of the accelerated corrosion. Chemical and X-ray diffraction analyses were also conducted, along with simulation tests to assess the role of alkali chlorides...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001119
EISBN: 978-1-62708-214-3
.... Failure initiated from the spring inside coil surface. Examination of the fracture surface using scanning electron microscopy showed no evidence of fatigue. Final fracture occurred in torsion. X-ray diffraction analysis revealed high inner-diameter residual stresses, indicating inadequate stress relief...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001807
EISBN: 978-1-62708-241-9
... was conducted to assess the role of friction in subsurface fatigue cracking in rolling-sliding contact applications. Based on the results of stress calculations and x-ray diffraction testing of steel samples, friction contributes to subsurface damage primary through its effect on the distribution of orthogonal...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001811
EISBN: 978-1-62708-241-9
... to be homogenous and had no banded structure. However, x-ray diffraction analysis confirmed the presence of up to 6% retained austenite which likely caused the tube to buckle during the 910 °C heat treating procedure. tube buckling retained austenite bainitic steel distortion x-ray diffraction analysis...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001829
EISBN: 978-1-62708-241-9
..., and x-ray diffraction. It was shown that degradation is driven by chemical and mechanical differences, oxide growth, depletion, and recrystallization, the combined effect of which results in exfoliation, spallation, and mechanical thinning. turbine vanes thermal degradation high-temperature...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001843
EISBN: 978-1-62708-241-9
... pest, a type of degradation that occurs at low temperatures. Based on the results of the investigation, which included SEM/EDS analysis, inductively coupled plasma spectroscopy, and x-ray diffraction, the metal surfaces contained less than 0.1% Bi and thus were not adequately protected against tin pest...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0046044
EISBN: 978-1-62708-235-8
.... Chemical analysis of the cracked metal showed a slightly higher level of carbon than in the component that did not crack. X-ray diffraction studies of material from the fractured dome showed a very low level of retained austenite, and chemical analysis showed a slightly higher content of carbon...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
...) spectroscopy Chemical shift of nuclei Mass spectroscopy Mass/charge of ions produced X-ray diffraction analysis (XRD) Crystalline polymer component Small-angle x-ray diffraction X-ray scattering at low angle Scanning electron microscopy (SEM) Surface and particle morphology Transmission...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c9001698
EISBN: 978-1-62708-222-8
... lists the composition of the corrosion products as obtained from one pipe sample. X-ray Diffraction Analysis Table 1 X-ray Diffraction Analysis Compound Approx. wt% Cu 2 0 50± CuCO 3 ·Cu(OH) 2 40 Amorphous Balance X-ray Fluorescence Analysis Table 2 X-ray...