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K. Mogami, S. Saito, H. Makishita, K. Ando, N. Ogura
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Friedrich Karl Naumann, Ferdinand Spies
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Vickers hardness
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Image
Low load Vickers hardness test with test load of 500 gf in the segregation ...
Available to Purchase
in A Broken Cross-Recessed Die Made from High Speed Tool Steel
> ASM Failure Analysis Case Histories: Machine Tools and Manufacturing Equipment
Published: 01 June 2019
Fig. 4 Low load Vickers hardness test with test load of 500 gf in the segregation region shown in Fig. 3 weaker etch than in Fig. 3 ). 200 ×
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Image
Distribution of vickers hardness near the fractured surface. In the symbol ...
Available to Purchase
in Failure Analysis of Liquid Propane Gas Cylinder
> ASM Failure Analysis Case Histories: Oil and Gas Production Equipment
Published: 01 June 2019
Fig. 9 Distribution of vickers hardness near the fractured surface. In the symbol I, the middle black point is the mean value of vickers hardness and standard deviation is indicated by the bar enclosed lines.
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Image
Shell position relative to the running surface in rail 5. Vicker's hardness...
Available to Purchase
in An Investigation of Shell and Detail Cracking in Railroad Rails
> ASM Failure Analysis Case Histories: Rail and Rolling Stock
Published: 01 June 2019
Fig. 14 Shell position relative to the running surface in rail 5. Vicker's hardness readings show that shell forms at the interface of cold worked and soft material.
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Image
a). Proximity of blade end. Eroded inlet edge with hardened region and Vick...
Available to PurchasePublished: 01 June 2019
Fig. 8 a). Proximity of blade end. Eroded inlet edge with hardened region and Vickers hardness indentations, transverse section, etch: V2A-solution. 10× b). Center of blade. Eroded inlet edge with hardened region and Vickers hardness indentations, transverse section, etch: V2A-solution. 10×
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Effect of austenitizing temperature on structure of 1% C steel. (a) Quenche...
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in Problems Associated with Heat Treated Parts
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 12 Effect of austenitizing temperature on structure of 1% C steel. (a) Quenched from 1000 °C (1830 °F). Coarse martensite plates (gray) and retained austenite (white). Vickers hardness of 745. (b) Quenched from 750 °C (1380 °F). Spheroidized carbides (white) in a fine martensite matrix
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Stress-strain plots for samples of Ti-6Al-4V, with sample axes aligned in t...
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in Mechanisms and Appearances of Ductile and Brittle Fracture in Metals
> Failure Analysis and Prevention
Published: 01 January 2002
Fig. 76 Stress-strain plots for samples of Ti-6Al-4V, with sample axes aligned in the three principal directions of the material. Vickers hardness values appear in the schematic of a block of material. Source: Ref 81
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Stress-strain plots for samples of Ti-6Al-4V titanium alloy with sample axe...
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in Mechanisms and Appearances of Ductile and Brittle Fracture in Metals
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 76 Stress-strain plots for samples of Ti-6Al-4V titanium alloy with sample axes aligned in the three principal directions of the material. Vickers hardness values appear in the schematic of a block of material. Source: Ref 80
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Book Chapter
Fractured Turbine Blades
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001228
EISBN: 978-1-62708-229-7
..., transverse section, etch: V2A-solution. Fig. 8 a). Proximity of blade end. Eroded inlet edge with hardened region and Vickers hardness indentations, transverse section, etch: V2A-solution. 10× b). Center of blade. Eroded inlet edge with hardened region and Vickers hardness indentations, transverse...
Abstract
In an electric power station, seven turbine blades out of 112 broke or cracked within 8 to 14 months after commencement of operation. The blades in question were all located on the last running wheel in the low pressure section of a 35,000 kW high pressure condensing turbine. They were milled blades without binding wires and cover band. They did not fracture at the fastening, i.e. the location of highest bending stress, but in a central region which was 165 to 225 mm away from the gripped end. The blades were fabricated from a stainless heat-treatable chromium steel containing 0.2C and 13.9Cr. Microstructural examination showed the blades were destroyed by flexural vibrations which evidently reached their maximum amplitude at the location of fracture. Erosion of the inlet edge, possibly in connection with vibration-induced corrosion cracking, contributed to fracture.
Book Chapter
Mechanical Testing in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006761
EISBN: 978-1-62708-295-2
... surface finish, flat surface, and parallel sides Sample must fit within the machine and be balanced on the pedestal Vickers hardness Hardness Test is slow Careful surface preparation of the specimen is necessary Measurement of indentation is operator dependent and results in variation...
Abstract
Mechanical testing is an evaluative tool used by the failure analyst to collect data regarding the macro- and micromechanical properties of the materials being examined. This article provides information on a few important considerations regarding mechanical testing that the failure analyst must keep in mind. These considerations include the test location and orientation, the use of raw material certifications, the certifications potentially not representing the hardware, and the determination of valid test results. The article introduces the concepts of various mechanical testing techniques and discusses the advantages and limitations of each technique when used in failure analysis. The focus is on various types of static load testing, hardness testing, and impact testing. The testing types covered include uniaxial tension testing, uniaxial compression testing, bend testing, hardness testing, macroindentation hardness, microindentation hardness, and the impact toughness test.
Book Chapter
Failure Analysis of a Gas Turbine Marriage Bolt
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001830
EISBN: 978-1-62708-241-9
... 0.2–0.35 0–0.04 0–0.04 0.45–0.7 0.8–1.15 0.5–0.65 0.25–0.35 Hardness and Microhardness Measurement To determine the hardness of the alloy, Vickers hardness measurements were carried out on several points from the outer surface to the central zone of the polished surface of the bolt...
Abstract
An 18-MW gas turbine exploded unexpectedly after three hours of normal operation. The catastrophic failure caused extensive damage to the rotor, casing, and nearly all turbo-compressor components. Based on their initial review, investigators believed that the failure originated at the interface between two shaft sections held together by 24 marriage bolts. Visual and SEM examination of several bolts revealed extensive deterioration of the coating layer and the presence of deep corrosion pits. It was also learned that the bolts were nearing the end of their operating life, suggesting that the effects of fatigue-assisted corrosion had advanced to the point where one of the bolts fractured and broke free. The inertial unbalance produced excessive vibration, subjecting the remaining bolts to overload failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001212
EISBN: 978-1-62708-235-8
... magnification. Fig. 1 Handle etched with 10% nital to show the flame hardened zone (dark). 1 × Fig. 2 Cracks running across the indentations caused by the tool during alignment. (Photographed with the TESSOVAR, Carl Zeiss. Oberkochen). 37 × The Vickers hardness was determined at a load...
Abstract
Operation handles produced from C45 steel showed many fine cracks at the flame hardened noses. The cracks ran from the corners of indentations caused by the tool during alignment. Metallographic investigation showed the nose was overheated during flame hardening. It was concluded that the numerous hardening cracks were caused by abrupt quenching from over-heating temperature and by local stress concentrations due to indentations of the tool caused during alignment.
Book Chapter
Failure Analysis of Liquid Propane Gas Cylinder
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001142
EISBN: 978-1-62708-228-0
... structure of the fractured LPG cylinder, near the fracture (A), the opposite side of the fractured position (B). Fig. 8 Metallographic section of the flaw near the fracture. 4. Hardness Micro Vickers hardness was measured at the positions where the microstructure was investigated...
Abstract
Several newly developed liquid propane gas (LPG) cylinders made from Fe-0.13C-0.42Mn steel failed, each fracturing in the longitudinal direction. One of the cylinders was thoroughly analyzed to determine the cause. Deep-drawing flaws were observed on the inner wall of the cylinder, oriented in the direction of the fracture and roughly equal in length. Flaws about 1.3 mm deep, steps, and a chevron pattern were observed on the fractured surface as were cleavage facets, revealed by SEM. Hardness was relatively high and the microstructure near the fracture surface appeared elongated. In addition, the stress intensity factor KI calculated from the value of the internal pressure was lower than that estimated by the fracture toughness test. All of this suggests that the tanks were not sufficiently annealed and prone to brittle fracture. The analysis thus proves that cracks initiated by deep-drawing flaws were the primary cause of failure.
Book Chapter
A Broken Cross-Recessed Die Made from High Speed Tool Steel
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c9001250
EISBN: 978-1-62708-223-5
... on hardening (coarse grain hardness cracks). The graphic representation of the results of low load hardness tests in Fig. 5 shows the differences in hardness between the segregation zone and the neighbouring fine acicular structure in Fig. 4 . Fig. 4 Low load Vickers hardness test with test load...
Abstract
A broken cross-recessed die was examined. Examination of the unetched, polished section for impurities revealed several coarse streaks of slag. The purity did not therefore correspond to the requirements set for a high speed tool steel of the given theoretical quality DMo 5. After etching with 5% nital the polished surface exhibited a pronounced, easily-visible, fibrous structure. Microscopic examination revealed that this etch pattern was produced by marked segregation bands. The very unfavorable structure for a high speed steel tool of these dimensions and subject to such stresses together with the low purity favored the fracture of the tool.
Book Chapter
Fatigue Fracture of a Type 316L Stainless Steel Angled Plate
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c0048413
EISBN: 978-1-62708-226-6
... of the plate had a high degree of cleanliness ( Fig. 1d ). The deformation structure showed that the material was in the cold-worked condition, which was confirmed by Vickers hardness tests. Energy-dispersive x-ray analysis indicated a chemical composition corresponding to a type 316 stainless steel...
Abstract
A type 316L stainless steel angled plate failed. The fatigue fracture was found to have occurred at a plate hole. Symmetric cyclic bending forces were revealed by the fatigue damage at the fracture edge at the top surface of the plate. Fatigue striations and slip bands produced on the surface during cyclic loading were observed. The material was showed by the deformation structure to be in the cold-worked condition and was termed to not be the cause of the implant failure.
Book Chapter
Failure of a Thick-Wall Alloy Steel Pressure Vessel Caused by Cracks in Weld HAZ
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0048795
EISBN: 978-1-62708-220-4
... martensite. A Vickers hardness traverse (1-kg load) across a band showed average values of 507 on one side of the band, 549 within the band, and 488 on the other side. A microprobe scan across the banded area showed the following differences in chemical composition: 1.56% Mn outside the band, 1.94% within...
Abstract
A large pressure vessel designed for use in an ammonia plant failed during hydrostatic testing. It was fabricated from ten Mn-Cr-Ni-Mo-V steel plates which were rolled and welded to form ten cylindrical shell sections and three forgings of similar composition. The fracture surfaces were metallographically examined to be typical for brittle steel fracture and associated with the circumferential weld that joined the flange forging to the first shell section. Featureless facets in the HAZ were observed and were revealed to be the fracture-initiation sites. Pronounced banding in the structure of the flange forging was revealed by examination. A greater susceptibility to cracking was interpreted from the higher hardenability found within the bands. Stress relief was concluded to have not been performed at the specified temperature level (by hardness and impact tests) which caused the formation of hard spots. The mode of crack propagation was established by microstructural examination to be transgranular cleavage. It was concluded that failure of the pressure vessel stemmed from the formation of transverse fabrication cracks in the HAZ fostered by the presence of hard spots. It was recommended that normalizing and tempering temperatures be modified and a revised forging practice explored.
Book Chapter
Fracture of Tempered Leaf Springs
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001185
EISBN: 978-1-62708-228-0
... structure ( Fig. 4 ). The transformed structure had a Vickers hardness (HV 0.2) of 733 to 773, compared with values of 447 to 463 for the unchanged tempered structure (cf. the hardness impressions in Fig. 4 ). Fig. 4 Microstructure in a cross-section through the origin of a crack, etched...
Abstract
U-shaped leaf springs, intended to serve as spacers between oil tank floats and the inner walls of the containers, broke while being fitted, or after a short time in use, in the bend of the U. The springs were made of tempered strip steel of type C 88 with 0.84 % C, bent at room temperature, and electroplated with cadmium for protection against corrosion. Each fracture showed seven or eight kidney-shaped cracks. At the origins of these cracks on the concave inner surface of the springs, crater-like depressions and beads of melted and resolidified material were found. Fracture of the springs was caused by stress cracks as a consequence of local hardening. The hardening caused by melting and resolidification, and therefore the cracks in the springs, was the result of a faulty procedure during cadmium electroplating.
Book Chapter
Bulging of a Shotgun Barrel Caused by a Change from Lead Shot to Iron Shot
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c0092135
EISBN: 978-1-62708-222-8
.... For example, at a distance of 5 mm (0.2 in.) from the muzzle, the wall thickness varied from 1.3 to 2 mm (0.051 to 0.080 in.). The microstructure of the barrel material was a mixture of ferrite and coarse pearlite. The alloy had a hardness of 163 to 198 HB (converted from Vickers hardness measurements...
Abstract
A shotgun barrel fabricated from 1138 steel deformed when test firing alternative nontoxic ammunition. The test shells contained soft iron shot, which at 72 HB, is much harder than traditional lead shot (typically 30 to 40 HB). An investigation based on ID and OD profiling supported the conclusion that the iron shot increased stresses in the choke zone of the barrel, causing it to deform. Variations in the amount of bulging were attributed to a lack of uniformity in wall thickness. Recommendations included making the barrel from steel with a higher yield strength, making the barrel walls thicker and more uniform, and/or developing an alternative nontoxic metal shot with a hardness in the range of 30 to 40 HB.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0089696
EISBN: 978-1-62708-220-4
..., 0.93% Mn, 0.023% P, 0.023% S, 0.53% Si, 0.044% Cu, 0.003% Sn, 0.50% Ni, 0.52% Cr, 0.20% Mo, 0.068% Al, and 0.003% V. Mechanical Properties Hardness Vickers hardness testing (500 g load) found the as-cast base metal to have readings of 215, 229, and 229 HV, for an average hardness of 224 HV...
Abstract
A failed crosshead of an industrial compressor was examined using optical and SEM. The crosshead was an ASTM A148 grade 105-85 steel casting. On the basis of the observations reported and available background information, it was concluded that the failure began with the initiation of cracks at slag inclusions and sharp fillets in weld-repair areas in the casting. The weld-repair procedures were unsatisfactory. The cracks propagated in a fatigue mode. he casting quality was judged unacceptable because of the presence of excessive shrinkage porosity. It was recommended that crosshead castings be properly inspected before machining. Revision of foundry practice to reduce or eliminate porosity was also recommended.
Book Chapter
Investigation on Bulging of Blow Pipe in a Blast Furnace
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001850
EISBN: 978-1-62708-241-9
... Point 1 35.80 0.79 0.89 62.52 Point 2 36.62 0.86 0.86 61.66 Point 3 34.50 0.86 0.93 63.70 Point 4 46.47 0.73 1.19 51.60 Point 5 0.42 1.27 98.30 Measurement of Mechanical Properties Hardness Hardness values were measured using a Vickers hardness testing...
Abstract
After about a year of uninterrupted service, one of the blow pipes on a blast furnace developed a bulge measuring 300 x 150 x 12 mm. The conical shaped section was removed from the furnace and examined to determine why it failed. The investigation consisted of visual inspection, chemical analysis, microstructural characterization, and mechanical property testing. The pipe was made from nonresulfurized carbon steel as specified and was lined with an alumina refractory. Visual inspection revealed cracks in the refractory lining, which corresponded with the location of the bulge. Microstructural and EDS analysis yielded evidence of overheating, revealing voids, scale, grain boundary oxidation, decarburization, and grain coarsening on the inner surface of the pipe, which also suggest the initiation of creep. Based on the information gathered during the investigation, the blow pipe was exposed to high temperatures when the liner cracked and subsequently bulged out due to creep.
Book
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.9781627082952
EISBN: 978-1-62708-295-2
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