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Surface treatment related failures
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Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0048128
EISBN: 978-1-62708-225-9
... steel Surface treatment related failures Metalworking-related failures Figure 1 shows light streaks arranged in a diagonal direction on the wire surface. The streaks are parallel to the wire axis. A darker depressed area is visible between the streaks and below the center of the fractograph...
Abstract
A fractograph of the failed spring was found to indicate light streaks are parallel to the wire axis. A darker depressed area was visible between the streaks and below the center of the fractograph in which distinct outlines that represent sharp corners in the depressions were revealed by careful examination. A hard material (mill scale) was assumed to have been impressed during drawing of the wire and was broken out during peening, leaving the depressions with sharp-bottomed corners. Spring was concluded to have failed due to a surface defect.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0091674
EISBN: 978-1-62708-217-4
... that the interference fit of the bushing in the lug hole be discontinued. Aircraft components Hinge brackets Marine environments 2014-T6 UNS A92014 Stress-corrosion cracking Surface treatment related failures Forged aluminum alloy 2014-T6 hinge brackets in naval aircraft rudder and aileron linkages...
Abstract
Forged aluminum alloy 2014-T6 hinge brackets in naval aircraft rudder and aileron linkages were found cracked in service. The cracks were in the hinge lugs, adjacent to a bushing made of cadmium-plated 4130 steel. Investigation (visual inspection and 250X micrographs) supported the conclusion that the failure of the hinge brackets occurred by SCC. The corrosion was caused by exposure to a marine environment in the absence of paint in stressed areas due to chipping. The stress resulted from the interference fit of the bushing in the lug hole. Recommendations included inspecting all hinge brackets in service for cracks and for proper maintenance of paint. Also suggested was replacing the aluminum alloy 2015-T6 with alloy 7075-T6, and surface treatment for the 7075-T6 brackets was recommended using sulfuric acid anodizing and dichromate sealing. Finally, it was also recommended that the interference fit of the bushing in the lug hole be discontinued.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048124
EISBN: 978-1-62708-235-8
... it was reoriented to the plane normal to the major tensile axis by sufficient loading. The shot-peening procedure was altered to create adequate surface compression at all stressed points on the springs. Cracks Galling Orientation Tensile stress Valve spring steel Surface treatment related failures...
Abstract
Presence of transverse marks which were remnant of grinding was indicated in a failed valve spring made from ground rod. The shot-peening pattern was light at this location. A transverse crack was found to grow from one such mark under the influence of local stress fields until it was reoriented to the plane normal to the major tensile axis by sufficient loading. The shot-peening procedure was altered to create adequate surface compression at all stressed points on the springs.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c0048674
EISBN: 978-1-62708-222-8
... structure and the method of plating the fastener with zinc was changed from electroplating to a mechanical deposition process to thus avoid hydrogen embrittlement. Fasteners, corrosion Electroplating Lawn furniture 1060 UNS G10600 Surface treatment related failures Hydrogen damage...
Abstract
Fasteners, made in high-production progressive dies from 0.7 mm thick cold-rolled 1060 steel, were used to secure plastic fabric or webbing to the aluminum framework of outdoor furniture. It was found that approximately 30% of the fasteners cracked and fractured as they were compressed to clamp onto the framework prior to springback. The heat treatment cycle of the fasteners consisted of austenitizing, quenching, tempering to obtain a tempered martensite microstructure, acid cleaning, zinc electroplating, coating with a clear dichromate and thereafter baking to remove the nascent hydrogen. It was revealed that fasteners treated in this manner were brittle due to hydrogen embrittlement as the baking process was found to not be able to remove all the nascent hydrogen which had induced during acid cleaning and electroplating. The heat treatment cycle was modified to produce a bainitic structure and the method of plating the fastener with zinc was changed from electroplating to a mechanical deposition process to thus avoid hydrogen embrittlement.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047428
EISBN: 978-1-62708-235-8
... of the dragline bucket were warned against further hardfacing of these teeth. Hard surfacing Weld deposited coatings Steel casting Brittle fracture Surface treatment related failures A cast dragline bucket tooth failed by fracturing after a short time in service. The tooth was made of medium-carbon...
Abstract
A cast dragline bucket tooth failed by fracturing after a short time in service. The tooth was made of medium-carbon low-alloy steel heat treated to a hardness of 555 HRB. The fracture surface was covered with chevron marks. These converged at several sites on the surface of the tooth. A hardfacing deposit was located at each of these sites. Visual inspection of the hardfacing deposits revealed numerous transverse cracks, characteristic of many types of hardfacing. This failure was caused by cracks present in hardfacing deposits that had been applied to the ultrahigh-strength steel tooth. Given the small critical crack sizes characteristic of ultrahigh-strength materials, it is generally unwise to weld them. It is particularly inadvisable to hardface ultrahigh-strength steel parts with hard, brittle, crack-prone materials when high service stresses will be encountered. The operators of the dragline bucket were warned against further hardfacing of these teeth.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c9001573
EISBN: 978-1-62708-226-6
.... Arcing Pitting (wear) Surgical implants Wire Ti-6Al-4V Titanium nitride coating UNS R56406 Surface treatment related failures (Other, miscellaneous, or unspecified) wear Background The TiN coated back surgery wires were made of Ti6A14V. The reported failure was the presence of pits...
Abstract
TiN coated back surgery wires were made of Ti-6Al-4V. The reported failure was the presence of pits located in the uncoated area of the wires. The uncoated area of the wire is where the wire is fixtured in the coating chamber during coating. Examination and analysis of the pits using SEM/EDX detection unit revealed significant peaks of B, O, Zr and Fe. Moreover, the shape of the pits was similar to an arc crater. The formation of pits in the wire was caused during coating due to microarcing. A contaminated fixture used during the coating most likely caused the microarcing.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001019
EISBN: 978-1-62708-217-4
... fatigue crack. It was concluded that the over-all failure was initiated in the crankshaft, and the failure of the bearing resulted from that failure. Aerospace engines Chromium plating Crankshafts Overheating Roller bearings Chromium-plated steel Fatigue fracture Surface treatment related...
Abstract
A broken aircraft crankshaft and a severely damaged main brass bearing were examined to determine whether engine failure was initiated in the bearing or in the crankshaft. The steel crankshaft failure was a classical fatigue fracture. The bearing had been subjected to extremely high temperatures, as indicated by melting in the brass components and the extreme distortion in the rollers. Microscopic examination on the crankshaft material showed it to be a good quality steel. On the other hand, the chromium plate was thick, porous, and cracked in many places, including the point of the main fatigue crack. It was concluded that the over-all failure was initiated in the crankshaft, and the failure of the bearing resulted from that failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001520
EISBN: 978-1-62708-235-8
... Hydraulic cylinders Surface defects 15-5 PH UNS S15500 Hydrogen damage and embrittlement Surface treatment related failures Problem Over the past few years, two types of chromium-plated hydraulic cylinders have failed by cracking on their outer surfaces. In one case, the parts had a history...
Abstract
Two types of chromium-plated hydraulic cylinders failed by cracking on their outer surfaces. In one case, the parts had a history of cracking in the nominally unstressed, as-fabricated condition. In another, cracks were detected after the cylinders were subjected to a pressure impulse test. Both part types were made of 15-5 PH (UNS S15500) precipitation hardening stainless steel. Hydrogen embrittlement cracking was the likely cause of failure for both part types. Cracking of the as-fabricated parts was ultimately prevented by changing the manufacturing procedure to allow for a reheat treatment. For parts that cracked after pressure testing, excessive dimensional changes precluded the inclusion of a reheat treatment as a manufacturing step, and further failure was averted by carefully employing proper machining practices, avoiding abusive machining.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001556
EISBN: 978-1-62708-218-1
... was attributed to hydrogen embrittlement that occurred during chrome plating. Chromium plating Piston rods Residual stress Fe-0.3C-3.0Cr-0.4Mo Hydrogen damage and embrittlement Surface treatment related failures A few Cr-Mo (C 0.3%, Cr 3.0%, Mo 0.4%) steel piston rods from different production...
Abstract
A few Cr-Mo steel piston rods from different production batches were found identically cracked in the eye end near the radius after chrome plating and baking treatment. Two of them cracked in the plating stage itself instantly broke on slight tapping. Cracking initiated from the outer base surface of the forked eye end. The 40 mm diam forged piston rods were subjected to plating after heavy machining on the part without any stress-relieving treatment. Also, time lapses between plating and baking were varied from 3 to 11 h. The brittle cracking along forked eye-end radius portion was attributed to hydrogen embrittlement that occurred during chrome plating.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0048630
EISBN: 978-1-62708-217-4
... was specified for a sample quantity of bolts from each lot. Electroplating Hydrogen embrittlement Cadmium-plated steel Surface treatment related failures Hydrogen damage and embrittlement Two clevis-head self-retaining bolts used in the throttle-control linkage of a naval aircraft failed...
Abstract
Two clevis-head self-retaining bolts used in the throttle-control linkage of a naval aircraft failed on the aircraft assembly line. Specifications required the bolts to be heat treated to a hardness of 39 to 45 HRC, followed by cleaning, cadmium electroplating, and baking to minimize hydrogen embrittlement. The bolts broke at the junction of the head and shank. The nuts were, theoretically, installed fingertight. The failure was attributed to hydrogen embrittlement that had not been satisfactorily alleviated by subsequent baking. The presence of burrs on the threads prevented assembly to finger-tightness, and the consequent wrench torquing caused the actual fractures. The very small radius of the fillet between the bolt head and the shank undoubtedly accentuated the embrittling effect of the hydrogen. To prevent reoccurrence, the cleaning and cadmium-plating procedures were stipulated to be low-hydrogen in nature, and an adequate post plating baking treatment at 205 deg C (400 deg F), in conformity with ASTM B 242, was specified. A minimum radius for the head-to-shank fillet was specified at 0.25 mm (0.010 in.). All threads were required to be free of burrs. A 10-day sustained-load test was specified for a sample quantity of bolts from each lot.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048143
EISBN: 978-1-62708-235-8
... was concluded to be the reason of the fatigue failure. Rack plating or barrels with fixed button contacts at many points instead of dangler-type contacts were recommended to avoid hard spots. Cadmium plating Cylinders Electric arcs Pneumatic devices Spring steel Surface treatment related failures...
Abstract
A cadmium-plated music-wire return spring that operated in a pneumatic cylinder designed for infinite life at a maximum stress level of 620 MPa failed after 240,000 cycles. An extremely hard and small kernel, which looked like a weld deposit, was observed at the center of the fractured surface. The kernel was assumed to have resulted from extreme localized overheating. These springs were reported to have been barrel electroplated after fabrication. The intermittent contact with the dangler (suspended cathode contact) as the barrel rotated allowed high local currents when the last contact was broken was revealed to have resulted in an arc that caused local melting of the metal being plated. The molten metal was interpreted to have been quenched instantly by the plating solution and by the mass of the cold metal of the spring. The hard spot caused by arcing during plating was concluded to be the reason of the fatigue failure. Rack plating or barrels with fixed button contacts at many points instead of dangler-type contacts were recommended to avoid hard spots.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001552
EISBN: 978-1-62708-217-4
... plating Crankshafts Magnetic particle testing Nitriding Surface grinding 4340 UNS G43400 Fatigue fracture Metalworking-related failures Surface treatment related failures Fig. 1 illustrates a crankshaft of AISI 4340, heat treated and nitrided all over, which failed in bending fatigue...
Abstract
This report covers case histories of failures in fixed-wing light aeroplane and helicopter components. A crankshaft of AISI 4340 Ni-Cr-Mo alloy steel, heat treated and nitrided all over, failed in bending fatigue. The nitrided layer was ground too rapidly causing excessive heat generation which induced grinding cracks and grinding burn. Tensional stresses resulting from grinding developed in a thin surface layer. On another crankshaft, chromium plating introduced undesirable residual tensile stresses. Such plating is an unsatisfactory finish for crankshafts of aircraft engines. Aircraft engine manufacturers and aeronautical standards require magnetic particle inspection to detect grinding cracks after reconditioning. Renitriding after any grinding is needed also, regardless of the amount of undersize as it introduces beneficial residual compressive stresses.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001746
EISBN: 978-1-62708-217-4
... was inadequate procedure, which resulted in bending moments being applied to the bolt threads. Acid pickling Bolts Cadmium plating Landing gear Torque 4340 UNS G43400 Surface treatment related failures Hydrogen damage and embrittlement Fig. 1 shows a failed beam from a landing gear...
Abstract
Brittle intergranular fracture, typical of a hydrogen-induced delayed failure, caused the failure of an AISI 4340 Cr-Mo-Ni landing gear beam. Corrosion resulting from protective coating damage released nascent hydrogen, which diffused into the steel under the influence of sustained tensile stresses. A second factor was a cluster of non-metallic inclusions which had ‘tributary’ cracks starting from them. Also, eyebolts broke when used to lift a light aircraft (about 7000 lb.). The bolt failure was a brittle intergranular fracture, very likely due to a hydrogen-induced delayed failure mechanism. As for the factors involved, cadmium plating, acid pickling, and steelmaking processes introduce hydrogen on part surfaces. As a second contributing factor, both bolts were 10 Rc points higher in hardness than specified (25 Rc), lessening ductility and notch toughness. A third factor was inadequate procedure, which resulted in bending moments being applied to the bolt threads.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047956
EISBN: 978-1-62708-235-8
... the raceways enough to cause fluctuations in machine output. Solvent-vapor cleaning was employed as a corrective technique for removing bearing lubricant. Lubricants Solvents Vapor degreasing Bearing steel Fretting wear Surface treatment related failures During the early stages of production...
Abstract
Randomly selected dictating-machine drive mechanisms, which contained small ball bearings, were found to exhibit unacceptable fluctuations in drive output during the early stages of production. It was indicated that the bearing raceways were being true brinelled before or during installation of the bearings. The preinstallation practices and the procedures for installing the bearings were carefully studied. It was revealed that during one preinstallation step, the lubricant applied by the bearing manufacturer was removed and the bearing was relubricated with another type of lubricant prior to which the bearings were ultrasonically cleaned in trichloroethylene to ensure extreme cleanness. Equally spaced indentations resembling true brinelling were revealed by careful examination of the bearing raceways. It was concluded that the ultrasonic energy transmitted to the balls brinelled the raceways enough to cause fluctuations in machine output. Solvent-vapor cleaning was employed as a corrective technique for removing bearing lubricant.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c9001694
EISBN: 978-1-62708-222-8
.... Austenite Bicycles Chromium plating Grain boundaries Metallography Chromium-plated steel Hydrogen damage and embrittlement Surface treatment related failures A number of vehicle accidents and failures have been evaluated over the years. These range from aircraft accidents, to railroad locomotive...
Abstract
The outer tube, or stem, on a bicycle frame fractured after two years of use. Detailed investigation revealed that the lower stem bearing had been loose for some time and the bottom bearing cup contained many cracks. Metallographic examination of the chromium-plated cup confirmed the brittle nature of the cracks, located along prior austenite boundaries. The failure was attributed to hydrogen embrittlement due to improper manufacturing procedures following chromium plating. The cracking led to looseness in the bearing and consequent scoring, cracking, and overloading of the stem.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0090626
EISBN: 978-1-62708-218-1
... the compressive residual-stress levels in the springs. Recommendation was made to increase the time the spring was shot peened from 12 to 60 min. Automotive components Residual stresses Shot peening Spring steel Surface treatment related failures A steel spring used in an automotive application...
Abstract
A steel spring used in an automotive application suddenly began to fail in the field, although “nothing had changed” in the fabrication process. Fatigue tests using springs fabricated prior to field failures lasted 500,000 cycles to failure, whereas fatigue tests performed on springs fabricated after field failures lasted only 50,000 cycles to failure. It was discovered that the percent coverage of shot peening prior and subsequent to the increase in failure incidence was much less than 100%, with a shot peening time of 12 min. The residual-stress state of “as fabricated” springs in three conditions were evaluated using XRD: springs manufactured prior to failure incidence increase, 12 min peen; springs manufactured following failure incidence increase, 12 min peen; and 60 min peen. The conclusion was that the failure occurred because low peening time significantly decreased the compressive residual-stress levels in the springs. Recommendation was made to increase the time the spring was shot peened from 12 to 60 min.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c9001229
EISBN: 978-1-62708-223-5
... or during operation. Chromium plating Saw blades Chromium-plated steel Surface treatment related failures Fatigue fracture Hydrogen damage and embrittlement Two slitting saw blades were delivered for the purpose of determining the cause of damage. One had cracked while the other one came...
Abstract
Two slitting saw blades were delivered for the purpose of determining the cause of damage. One had cracked while the other one came from a prior sheet delivery, that had less tendency to crack formation according to the manufacturer. The blades were supposed to have been stamped out of a sheet made from a 55 kp/sq mm strength steel. The saw blades were used for separating steel profiles at high rotational speeds. The cracks in question were located at the base of the teeth, i.e. at the point of highest operating stress. Metallographic examination showed that all cracks were non-decarburized and were free of chromium deposits. Therefore they could not have existed before heat treatment and chrome plating. It was concluded that the damage was due neither to poor quality of the sheet nor to defective stamping or heat treatment, but had occurred later either during surface treatment or during operation.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c9001158
EISBN: 978-1-62708-225-9
.... Surface defects Valve springs Spring steel Surface treatment related failures Fatigue fracture Ductile fracture The fractured valve spring shown in Fig. 1 showed a small fatigue fracture and a large ductile fracture emanating from it in the fibrous fracture structure, that also appeared...
Abstract
A steel valve spring meeting Steel-Iron-Test 1570 fractured during the high-stress condition of the operation of its valve. Metallographic examination of a transverse section adjacent to the fracture and a longitudinal section through the crack showed the steel was free of major defects and was of high purity, although a number of minor surface defects such as rolling laps were found. The spring was heat treated and its surface strengthened by shot-peening, but the surface was also decarburized to a depth of approximately 0.03 mm which resulted in a lowering of the surface hardness. The fracture of this valve spring is therefore primarily due to surface defects, and secondly perhaps also to weak surface decarburization. No recommendation resulted from the investigation except to note that comparatively minor effects suffice to cause fractures in highly stressed springs.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0048626
EISBN: 978-1-62708-225-9
... embrittlement 8735 UNS G87350 Surface treatment related failures Hydrogen damage and embrittlement Cadmium-plated high-strength steel bolts were used to facilitate quick disassembly of a vehicle. One bolt was found fractured across the root of a thread after being torqued in place for 1 week. The bolts...
Abstract
Cadmium-plated high-strength steel bolts were used to facilitate quick disassembly of a vehicle. One bolt was found fractured across the root of a thread after being torqued in place for one week. The bolts were made of 8735 steel heat treated to a tensile strength of 1241 to 1379 MPa (180 to 200 ksi) with a hardness of 39 to 43 HRC, followed by cadmium plating. The bolt that failed and several that did not were examined. It was found that failure of the bolts was the result of time-dependent hydrogen embrittlement. Had the remaining bolts been torqued to the normal stress levels, all would have failed within two weeks. The bolts were baked, as specified by ASTM B 242, at 205 deg C (400 deg F) for 30 min. No further failures occurred. Baking for 30 min is the minimum baking time; however, baking times up to 24 h are recommended for greater safety.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001185
EISBN: 978-1-62708-228-0
... treatment related failures U-shaped leaf springs, intended to serve as spacers between oil tank floats and the inner walls of the containers, broke while being fitted, or after a short time in use, in the bend of the U. The springs were made of tempered strip steel of type C 88 with 0.84 % C, bent...
Abstract
U-shaped leaf springs, intended to serve as spacers between oil tank floats and the inner walls of the containers, broke while being fitted, or after a short time in use, in the bend of the U. The springs were made of tempered strip steel of type C 88 with 0.84 % C, bent at room temperature, and electroplated with cadmium for protection against corrosion. Each fracture showed seven or eight kidney-shaped cracks. At the origins of these cracks on the concave inner surface of the springs, crater-like depressions and beads of melted and resolidified material were found. Fracture of the springs was caused by stress cracks as a consequence of local hardening. The hardening caused by melting and resolidification, and therefore the cracks in the springs, was the result of a faulty procedure during cadmium electroplating.
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