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Image
Microstructure of damaged sleeve plate showing precipitation of metal carbi...
Available to Purchase
in Failure Analysis of Fire Tube Sleeve of Heater Treater
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 8 Microstructure of damaged sleeve plate showing precipitation of metal carbides at grain boundaries, 400×
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Microstructure of damaged sleeve showing severe oxidation of metal plate at...
Available to Purchase
in Failure Analysis of Fire Tube Sleeve of Heater Treater
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 9 Microstructure of damaged sleeve showing severe oxidation of metal plate at the edge, 100×
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EDS spectra of the base metal of the screw (a) and the plating on the outsi...
Available to Purchase
in Hydrogen Embrittlement Failure of Socket Head Cap Screws
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 5 EDS spectra of the base metal of the screw (a) and the plating on the outside surface (b).
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Liquid metal embrittlement in two aluminum alloy 2024-T4 plates that were w...
Available to PurchasePublished: 15 January 2021
Fig. 57 Liquid metal embrittlement in two aluminum alloy 2024-T4 plates that were wetted with liquid mercury and then loaded to fracture in tension. Fracture occurred rapidly at a stress well below the nominal yield strength of the plates. Visible on each fracture surface is a flat, mercury
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Published: 15 May 2022
Book Chapter
Brittle Fracture of a Soybean-Oil Storage Tank Caused by High Service Stresses
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c0047508
EISBN: 978-1-62708-221-1
... and drilled for bolting on a heavy steel plate. The tank was filled to a record height. In mid-Jan the temperature dropped to -31 deg C (-23 deg F), with high winds. The tank split open and collapsed. The welding used the shielded metal arc process with E6010 electrodes, which could lead to weld porosity...
Abstract
A riveted 0.25% carbon steel oil-storage tank in Oklahoma was dismantled and reassembled in Minnesota by welding to form a storage tank for soybean oil. An opening was cut in the side of the tank to admit a front-end loader. A frame of heavy angle iron was welded to the tank and drilled for bolting on a heavy steel plate. The tank was filled to a record height. In mid-Jan the temperature dropped to -31 deg C (-23 deg F), with high winds. The tank split open and collapsed. The welding used the shielded metal arc process with E6010 electrodes, which could lead to weld porosity, hydrogen embrittlement, or both. At subzero temperatures, the steel was below its ductile-to-brittle transition temperature. These circumstances suggest a brittle condition. Steps to avoid this type of failure: For cold conditions, the steel plate should have a low carbon content and a high manganese-to-sulfur ratio and be in a normalized condition, low-hydrogen electrodes and welding practices should be used, all corners should be generously radiused, the welds should be inspected and ground or dressed to minimize stress concentrations, postweld heating is advisable, and radiographic and penetrant inspection tests should be performed.
Book Chapter
Brittle Failure of Locking Collar Produced From Rolled 4140 Grade Steel Plate
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0047105
EISBN: 978-1-62708-225-9
... were made. Anisotropy Locking collars Plate metal 4140 UNS G41400 Brittle fracture The locking collar on a machine failed suddenly when the shaft it restrained was inadvertently subjected to an axial load slightly higher than the allowable working load ( Fig. 1a ). The locking collar...
Abstract
The locking collar on a machine failed suddenly when the shaft it restrained was inadvertently subjected to an axial load slightly higher than the allowable working load. The locking collar fractured abruptly, producing four large fragments. This allowed the shaft to be propelled forcefully in the direction of the load, causing substantial damage to other machinery components in the vicinity. The failed component, which was 43 cm (17 in.) in diameter, was machined from 4140 plate and heat treated to 34 to 36 HRC. Analysis (visual inspection, composite micrographs, scanning electron microscopy, and mechanical-property analysis) supported the conclusions that the alloy steel plate used in this application contained significant brittle microstructural fibering or banding. This condition produced considerable anisotropy in ductility and toughness as revealed by mechanical testing. Unfortunately, the potential effects of anisotropy were apparently neglected when this component was designed and manufactured from the plate stock, because the loading was applied in a direction that stressed the weakest planes in the material, that is, a direction normal to the fibering. No recommendations were made.
Book Chapter
Brittle Fracture of an Excavator Boom Suspension Rope Anchorage Plate
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c9001449
EISBN: 978-1-62708-221-1
...-ductility of the material from which the plates were made. Ductiity Fillet welds Plate metal Fe-0.65C-0.22Mn Brittle fracture The anchorage plate which fractured was one of a pair used as intermediate members through which the boom suspension ropes were attached to the jury-mast...
Abstract
An anchorage plate which fractured was one of a pair used as intermediate members through which the boom suspension ropes were attached to the jury-mast of an excavator. Failure of the plate released the ropes on one side of the boom, resulting in extensive damage to the latter and also bending of the other anchorage plate. The anchorage plates were 23 x 9 in. and had been flame-cut from mild steel plate. Collars were fillet-welded on each side at both ends to provide extra bearing area for the pins. Holes had then been flame-cut slightly under size and bored to final dimensions. The plates were given a slight set after flame-cutting to provide a more direct line of pull for the ropes. The fracture surface was bounded by narrow lips, indicative of shear failure. Failure of the anchorage plate was attributed to cracks present at the junctions of the fillet welds, and deficient notch-ductility of the material from which the plates were made.
Book Chapter
Brittleness in Copper and Copper Alloys With Particular Reference to Hydrogen Embrittlement
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001447
EISBN: 978-1-62708-235-8
... of low melting point eutectics or corrosion; show a similar appearance when investigated on a macroscopic scale. Conductors (devices) Plate metal Turbogenerators Copper Hydrogen damage and embrittlement This article originally appeared in the issue of “Der Maschinenschaden” for December...
Abstract
Hydrogen embrittlement is the brittleness affecting copper and copper alloys containing oxygen which develops during heat treatment at temperatures of about 400 deg C (752 deg F) and above in an atmosphere containing hydrogen. The phenomenon of hydrogen embrittlement of copper and its alloys is illustrated by examples from practice and reference is made to data from recent publications on the subject. Embrittlement due to this cause can only be identified by microscopic examination because other modes of failure in copper; e.g., from heat cracking, mechanical overload, the formation of low melting point eutectics or corrosion; show a similar appearance when investigated on a macroscopic scale.
Book Chapter
Fatigue Fracture of a Music-Wire Spring Caused by Poor Electroplating Practice
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048143
EISBN: 978-1-62708-235-8
... contact was broken was revealed to have resulted in an arc that caused local melting of the metal being plated. The molten metal was interpreted to have been quenched instantly by the plating solution and by the mass of the cold metal of the spring. The hard spot caused by arcing during plating...
Abstract
A cadmium-plated music-wire return spring that operated in a pneumatic cylinder designed for infinite life at a maximum stress level of 620 MPa failed after 240,000 cycles. An extremely hard and small kernel, which looked like a weld deposit, was observed at the center of the fractured surface. The kernel was assumed to have resulted from extreme localized overheating. These springs were reported to have been barrel electroplated after fabrication. The intermittent contact with the dangler (suspended cathode contact) as the barrel rotated allowed high local currents when the last contact was broken was revealed to have resulted in an arc that caused local melting of the metal being plated. The molten metal was interpreted to have been quenched instantly by the plating solution and by the mass of the cold metal of the spring. The hard spot caused by arcing during plating was concluded to be the reason of the fatigue failure. Rack plating or barrels with fixed button contacts at many points instead of dangler-type contacts were recommended to avoid hard spots.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047566
EISBN: 978-1-62708-235-8
... of using too large a welding rod and too much heat input, melting of the low-carbon steel handle, which diluted the austenitic stainless steel filler metal and formed martensitic steel in the weld zone. Because it was impractical to preheat and postheat the type 502 stainless steel cover plate, the low...
Abstract
Handles welded to the top cover plate of a chemical-plant downcomer broke at the welds when the handles were used to lift the cover. The handles were fabricated of low-carbon steel rod; the cover was of type 502 stainless steel plate. The attachment welds were made with type 347 stainless steel filler metal to form a fillet between the handle and the cover. The structure was found to contain a zone of brittle martensite in the portion of the weld adjacent to the low-carbon steel handle; fracture had occurred in this zone. The brittle martensite layer in the weld was the result of using too large a welding rod and too much heat input, melting of the low-carbon steel handle, which diluted the austenitic stainless steel filler metal and formed martensitic steel in the weld zone. Because it was impractical to preheat and postheat the type 502 stainless steel cover plate, the low-carbon steel handle was welded to low-carbon steel plate, using low-carbon steel electrodes. This plate was then welded to the type 502 stainless steel plate with type 310 stainless steel electrodes. This design produced a large weld section over which the load was distributed.
Book Chapter
Cracking of a Pressure Vessel Due to Penetration by Solder
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001440
EISBN: 978-1-62708-235-8
...-on patch plate or to employ one of the high-strength, non-metallic adhesives. Explosions Gas cylinders Soldered joints Tensile stress 50Pb-50Sn Plate steel Intergranular fracture Liquid metal induced embrittlement Reference is made in other cases in this series of Reports to failures...
Abstract
A portable propane container with a name-plate soldered onto it exploded in service. When the vessel was inspected afterwards, it was found to have developed a crack in the top end plate. A portion of the end plate cut out to include the midlength and one termination of the crack was examined microscopically. This revealed that the crack was associated with intergranular penetration by molten metal. The microstructure in general was indicative of a good-quality mild steel. It was evident from that solder that was responsible for the penetration and that fused brass from the hand wheel had not played any part. Tensile stress was present at the time of the failure sufficiently high to enable solder penetration to take place. The use of soft solder as a medium for attaching name-plates directly on to stressed steel parts is not recommended. It would be preferable to use a welded-on patch plate or to employ one of the high-strength, non-metallic adhesives.
Book Chapter
Brittle Fracture of a Clapper Weldment for a Disk Valve Due to Improper Filler Metal
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048767
EISBN: 978-1-62708-235-8
... were revealed at the edges of the weld metal. It was revealed by chemical analysis of this band that a stainless steel filler metal had been used which produced mixed composition at the weld boundaries. The plating material was revealed to be nickel by chemical analysis. It was concluded that clapper...
Abstract
The clapper in a 250 mm diam disk valve (made from ASTM A36 steel, stress relieved and cadmium plated) fractured at the welded joint between the clapper and a 20 mm diam support rod (also made of same material). The valve contained a stream of gas consisting of 55% H2S, 39% CO2, 5% H2, and 1% hydrocarbons at 40 deg C and 55 kPa during operation. Voids on the fracture surface and evidence of incomplete weld penetration were revealed by examination. Brittle fracture was indicated by the overall appearance through some fatigue beach marks were observed. Very narrow bands of high hardness were revealed at the edges of the weld metal. It was revealed by chemical analysis of this band that a stainless steel filler metal had been used which produced mixed composition at the weld boundaries. The plating material was revealed to be nickel by chemical analysis. It was concluded that clapper failed by fatigue and brittle fracture because it was welded with an incorrect filler metal. A clapper assembly was welded with a low-carbon steel filler metal, then cadmium plated.
Book Chapter
Use of Electron Fractography to Dianose Stress-Corrosion Cracking of an AISI 4340 Nose Landing Gear Cylinder
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001542
EISBN: 978-1-62708-217-4
..., large non-metallic inclusions near the chromium-plated ID of the cylinder. Also, there were breaks in the chromium plate and pits in the underlying base metal. The cylinder had been in service for 18,017 h, and 5948 h had passed since the first and only overhaul. Substandard plating of the ID...
Abstract
A nose landing gear cylinder made from AISI 4340 Ni-Cr-Mo alloy steel was found cracked and leaking, causing partial depressurization. Investigation revealed the crack to be a stress-corrosion type, judging by the 6500x electron fractograph. It had started in a region of concentrated, large non-metallic inclusions near the chromium-plated ID of the cylinder. Also, there were breaks in the chromium plate and pits in the underlying base metal. The cylinder had been in service for 18,017 h, and 5948 h had passed since the first and only overhaul. Substandard plating of the ID at this time ultimately resulted in pitting of the metal. The combination of surface pitting and stress concentration at the nearby inclusions resulted in stress-corrosion cracking.
Book Chapter
Disruption of a Hydro-Extractor
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001420
EISBN: 978-1-62708-220-4
... steel shell and two end plates. It was designed to spin at 2200 rpm, using centrifugal force to expel liquids through nearly 3000 drilled holes in the shell wall. Investigators found that the shell separated completely from the bottom plate. The top plate, though it cracked radially, remained attached...
Abstract
A hydroextractor installed new for the drying of sugar massecuite consisted of a metal basket fixed to a vertical spindle. Disruption occurred just after the machine had been run up to speed and was not preceded by any abnormal behavior. The basket assembly consisted of a Ni-Cr-Mo steel shell and two end plates. It was designed to spin at 2200 rpm, using centrifugal force to expel liquids through nearly 3000 drilled holes in the shell wall. Investigators found that the shell separated completely from the bottom plate. The top plate, though it cracked radially, remained attached over most of its circumference. The basket also contained a 22-gauge Monel metal liner that had been perforated by stabbing, raising pronounced burrs that faced each hole. Apart from the local spots of corrosion due to the lining, the inner surface of the basket showed little evidence of general corrosion. What caused the basket to fail was the presence of corrosion-fatigue cracks or fissures radiating from the holes. A secondary cause was that the scantlings of the basket were too light.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c9001442
EISBN: 978-1-62708-221-1
... metal adjacent to the fusion face of the fillet to the vane, as is evident from Figure 8 . A short fatigue crack, extending from the root of the fillet weld part way through the back plate, was also present. Further microscopical examination indicated that the striations seen on the fracture were...
Abstract
The impeller of a 4 ft. diam extraction fan driven by a 120 hp motor at 1,480 rpm. disrupted suddenly. The majority of the vanes had become detached where they were welded to the plates. At other locations, separation of the vanes was accompanied by tearing of the adjacent plate, failure being initiated at the weld fillets of the inner end of the vanes. An unusual feature was that the blades disclosed regions having a pronounced striated and stepped appearance. The etched microstructure was typical of a low carbon rolled plate having the usual banded appearance. A cross section through the fillet welds and zone showed lamellar tearing, which confirmed that failure had occurred in weld metal adjacent to the fusion face of the fillet to the vane. Results of the investigation indicated that the primary cause of failure of the impeller was the development of fatigue cracks from the unwelded roots of the fillet welds, by which the vanes were attached to the supporting plates. The impeller would have shown increased resistance to fatigue crack initiation if the T joint between the vanes and plates had been of the full penetration type.
Book Chapter
Failure of a Carbon Steel Galvanizing Vat
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0046911
EISBN: 978-1-62708-227-3
... thick ASTM A285, grade B, steel plate. One joint was welded using the semiautomatic submerged arc process with one pass on each side. A second joint was welded manually by the shielded metal arc process using E6010 welding rod and four passes on each side. The silicon content of the shielded metal arc...
Abstract
A steel galvanizing vat measuring 3 x 1.2 x 1.2 m (10 x 4 x 4 ft) and made of 19 mm thick carbon steel plate (ASTM A285, grade B)) at a shipbuilding and ship-repair facility failed after only three months of service. To verify suspected failure cause, two T joints were made in 12.5 mm thick ASTM A285, grade B, steel plate. One joint was welded using the semiautomatic submerged arc process with one pass on each side. A second joint was welded manually by the shielded metal arc process using E6010 welding rod and four passes on each side. The silicon content of the shielded metal arc weld was 0.54%, whereas that of the submerged arc weld was 0.86%. After being weighed, the specimens were submerged in molten zinc for 850 h. Analysis (visual inspection, chemical analysis, 100x 2% nital-etched micrographs) supported the conclusions that the vat failed due to molten-zinc corrosion along elongated ferrite bands, possibly because silicon was dissolved in the ferrite and thus made it more susceptible to attack by the molten zinc. Recommendations included rewelding the vat using the manual shielded metal arc process with at least four passes on each side.
Book Chapter
Brittle Fracture of a Clamp Because of Burning During Forging
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047176
EISBN: 978-1-62708-235-8
.... Evidence that burning was confined to the hinge end of the clamp indicated that the metal was overheated before or during the upset forging operation. Recommendations included notifying the supplier of the burned condition on the end of the clamp. The clamps should be macroetched before cadmium plating...
Abstract
A ring clamp (8740 (AMS 6322), steel forged and cadmium plated) used for attaching ducts to an aircraft engine became loose after three hours of service. When the clamp was removed from the engine, the hinge tabs on one clamp half were found to be broken. Analysis (visual inspection and microscopic and metallographic examination) supported the conclusion that both hinge tabs on the clamp half fractured in a brittle manner as the result of gross overheating, or burning, during forging. The mechanical properties of the metal, especially toughness and ductility, were greatly reduced by burning. Evidence that burning was confined to the hinge end of the clamp indicated that the metal was overheated before or during the upset forging operation. Recommendations included notifying the supplier of the burned condition on the end of the clamp. The clamps should be macroetched before cadmium plating to detect overheating. The clamps in stock should be inspected to ensure that the metal had not been weakened by overheating during the upset forging operation.
Book Chapter
Stress-Corrosion Cracking of Stainless Steel Falling Film Black Liquor Evaporator
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.pulp.c9001567
EISBN: 978-1-62708-230-3
... of the plates indicates significant residual stresses. Fig. 3 Cracking initiated at the spot welds and progressed into the base metal. Magnification 2× Fig. 4 Transgranular, branching type SCC in the 316L heat exchangers. Magnification 100× Fig. 5 SCC fracture surface with cleavage...
Abstract
A falling film black liquor evaporator consisted of flat twin plate heat exchangers and was used to increase black liquor solids content prior to its burning in the recovery boiler. Several plate heat exchangers were fabricated of AISI type 316L stainless steel by electric resistance welding. Cracks initiated at the inside surface of the welded areas and penetrated through the wall thickness. In several locations, the weld fractured and the plates separated with significant spring back, indicative of high residual stresses attributed to fabrication and weld procedures. The cracks had extended radially from the electric resistant weld into the base metal. Metallographic examination revealed the cracks were transgranular and branching, characteristic of SCC in austenitic stainless steels. The fracture surfaces had a brittle cleavage-like appearance, typical of SCC in austenitic stainless steels. Chlorides in the service environment were a contributory factor. The primary factor causing SCC localized at the electric resistant welds was substantial residual stresses as a result of fabrication procedures. It was recommended that the heat exchanger plates be subjected to stress-relief heat treatment following fabrication and welding.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001843
EISBN: 978-1-62708-241-9
... Abstract The operator of an electric transit system purchased a large number of tin-plated copper connectors, putting some in service and others in reserve. Later, when some of the reserve connectors were inspected, the metal surfaces were covered with spots consisting of an ash-like powder...
Abstract
The operator of an electric transit system purchased a large number of tin-plated copper connectors, putting some in service and others in reserve. Later, when some of the reserve connectors were inspected, the metal surfaces were covered with spots consisting of an ash-like powder and the plating material had separated from the substrate in many areas. Several connectors, including some that had been in service, were examined to determine what caused the change. The order stated that the connectors were to be coated with a layer of tin-bismuth (2% Bi) to guard against tin pest, a type of degradation that occurs at low temperatures. Based on the results of the investigation, which included SEM/EDS analysis, inductively coupled plasma spectroscopy, and x-ray diffraction, the metal surfaces contained less than 0.1% Bi and thus were not adequately protected against tin pest, which was confirmed as the failure mechanism in the investigation.
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