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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001671
EISBN: 978-1-62708-234-1
... Abstract Important clues about the probable cause of a gun tube explosion were obtained from a fractographic and metallographic examination of the fragments. The size, distribution, and surface markings of fragments may be used to localize the explosion and deduce its intensity. Microstructural...
Abstract
Important clues about the probable cause of a gun tube explosion were obtained from a fractographic and metallographic examination of the fragments. The size, distribution, and surface markings of fragments may be used to localize the explosion and deduce its intensity. Microstructural features such as voids, adiabatic shear, and structural surface alterations also indicate the explosion intensity and further allow a comparison of the tube structure near and away from the explosion zone. These, and other metallurgical characteristics, are illustrated and discussed for cases of accidental and deliberately caused explosions of large caliber gun tubes.
Image
in The Role of Metallography and Fractography in the Analysis of Gun Tube Failures
> ASM Failure Analysis Case Histories: Failure Modes and Mechanisms
Published: 01 June 2019
Fig. 1 Overall view of gun tube in which the failure was caused by deliberately detonating a high explosive projectile inside the tube. The failure is characterized by an intact muzzle section (forefront), large fragments to the rear of this area, fragments from the area of detonation
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Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c0089657
EISBN: 978-1-62708-233-4
... Abstract The gun mount used in two types of self-propelled artillery consists of an oil-filled recoil cylinder and a sand-cast (MIL-I-11466, grade D7003) ductile-iron piston that connects to the gun tube through a threaded rod. The piston contains several orifices through which oil is forced...
Abstract
The gun mount used in two types of self-propelled artillery consists of an oil-filled recoil cylinder and a sand-cast (MIL-I-11466, grade D7003) ductile-iron piston that connects to the gun tube through a threaded rod. The piston contains several orifices through which oil is forced as a means of absorbing recoil energy. During operation, the piston is stressed in tension, pulled by oil pressure on one end and the opposing force of the gun tube on the other. The casting specification stipulated that the graphite be substantially nodular and that metallographic test results be provided for each lot. Investigation (visual inspection, fatigue testing, 0.25x/0.35x/50x magnifications, 2% nital etched 60x/65x magnifications, and SEM views) showed that most of the service fractures occurred in pistons containing vermicular graphite. Recommendations included ultrasonic testing of pistons already in the field to identify and reject those containing vermicular graphite. In addition, metallographic control standards were suggested for future production lots.
Image
in The Role of Metallography and Fractography in the Analysis of Gun Tube Failures
> ASM Failure Analysis Case Histories: Failure Modes and Mechanisms
Published: 01 June 2019
Fig. 2 Sketch of assembled fragments on which the crack surface directions on individual fragments are shown pointing to the origin of failure (upper right) at the muzzle end of the gun tube.
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Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0047010
EISBN: 978-1-62708-234-1
... including a maraging steel (18% Ni, grade 250), a vanadium-modified 4337 gun steel (4337V), H19 tool steel, and high-temperature alloys Rene 41, Inconel 718, and Udimet 630. All the alloys evaluated had been used in mortar tubes previously or were known to meet the estimated minimum yield strength...
Abstract
When bulging occurred in mortar tubes made of British I steel during elevated-temperature test firing, a test program was formulated to evaluate the high-temperature properties (at 540 to 650 deg C, or 1000 to 1200 deg F) of the British I steel and of several alternative alloys including a maraging steel (18% Ni, grade 250), a vanadium-modified 4337 gun steel (4337V), H19 tool steel, and high-temperature alloys Rene 41, Inconel 718, and Udimet 630. All the alloys evaluated had been used in mortar tubes previously or were known to meet the estimated minimum yield strength. The alloys fall in this order of decreasing strengths: Udimet 630, Inconel 718, Rene 41, H19 tool steel, British I steel, 4337V gun steel, and maraging steel. When cycled between room temperature and 540 to 650 deg C (1000 to 1200 deg F), only Udimet 630, Inconel 718, and Rene 41 retained yield strengths higher than the minimum. Also, these three alloys maintained high strengths over the tested range, whereas the others decreased in yield strength as cycling progressed. Analysis showed Inconel 718 was considered best suited for 81-mm mortar tubes, and widespread industrial use ensured its availability.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
... electrons from a tungsten filament are termed cold-field-emission SEMs, or high-resolution SEMs, and have the highest resolution capabilities of all SEMs. A compromise is reached in the thermal-field-emission (or Schottky gun) SEM when a combination of heat and electric field are used to produce an electron...
Abstract
The scanning electron microscope (SEM) is one of the most versatile instruments for investigating the microscopic features of most solid materials. The SEM provides the user with an unparalleled ability to observe and quantify the surface of a sample. This article discusses the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described, and the application of SEM in fractography is discussed. The article covers the failure mechanisms of ductile failure, brittle failure, mixed-mode failure, and fatigue failure. Lastly, image dependence on microscope type and operating parameters is also discussed.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003533
EISBN: 978-1-62708-180-1
.... A compromise is reached in the thermal-field-emission (or Schottky gun) SEM, where a combination of heat and electric field are used to produce electrons. These machines have better resolution than conventional SEMs, while being easier to use than the high-resolution machines. A conventional SEM also...
Abstract
The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical column, signal detection and display equipment, and vacuum system. It discusses the preparation of samples for observation using an SEM and describes the application of SEM in fractography. If the surface remains unaffected and undamaged by events subsequent to the actual failure, it is often a simple matter to determine the failure mode by the use of an SEM. In cases where the surface is altered after the initial failure, the case may not be so straightforward. The article presents typical examples that illustrate these points. Image dependence on the microscope type and operating parameters is also discussed.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006943
EISBN: 978-1-62708-395-9
.... The fundamental construction of the electron column is basically the same in various SEM instruments. The electron column consists of an electron gun, electron lenses, condenser lenses, and objective lenses, which are necessary to collimate and focus the electron beam for optimum operation of the instrument...
Abstract
This article discusses the operating principles, advantages, and limitations of scanning electron microscopy, atomic force microscopy, x-ray photoelectron spectroscopy, and secondary ion mass spectroscopy that are used to analyze the surface chemistry of plastics.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
..., the secondary ions can be detected using a mass spectrometer. A quadrupole mass spectrometer can be installed on an existing Auger system fitted with an ion etching gun, and simultaneous AES and SIMS analyses can be made. Stand-alone SIMS systems can provide improved performance as a result of a smaller ion...
Abstract
This article focuses on the visual or macroscopic examination of damaged materials and interpretation of damage and fracture features. Analytical tools available for evaluations of corrosion and wear damage features include energy dispersive spectroscopy, electron probe microanalysis, Auger electron spectroscopy, secondary ion mass spectroscopy, and X-ray powder diffraction. The article discusses the analysis and interpretation of base material composition and microstructures. Preparation and examination of metallographic specimens in failure analysis are also discussed. The article concludes with a review of the evaluation of polymers and ceramic materials in failure analysis.
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006757
EISBN: 978-1-62708-295-2
... of an ion beam with a material. Thus, when an ion beam, as used in AES analysis for depth profiling, impinges on a surface, the secondary ions can be detected using a mass spectrometer. A quadrupole mass spectrometer can be installed on an existing Auger system fitted with an ion etching gun...
Abstract
Examination of a damaged component involves a chain of activities that, first and foremost, requires good observation and documentation. Following receipt and documentation, the features of damage can be recorded and their cause(s) investigated, as this article briefly describes, for typical types of damage experienced for metallic components. This article discusses the processes involved in visual or macroscopic examination of damaged material; the interpretation of fracture features, corrosion, and wear damage features; and the analysis of base material composition. It covers the processes involved in the selection of metallurgical samples, the preparation and examination of metallographic specimens in failure analysis, and the analysis and interpretation of microstructures. Examination and evaluation of polymers and ceramic materials in failure analysis are also briefly discussed.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006771
EISBN: 978-1-62708-295-2
... Depth Profiles Compositional depth profiling is possible with the use of auxiliary sputter ion guns. Several different options for ion sources are available and depend on the material to be depth profiled. All ion guns are used to slowly remove material, thus exposing a new surface to be analyzed...
Abstract
This article covers the three most popular techniques used to characterize the very outermost layers of solid surfaces: Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (XPS), and time-of-flight secondary ion mass spectrometry (TOF-SIMS). Some of the more important attributes are listed for preliminary insight into the strengths and limitations of these techniques for chemical characterization of surfaces. The article describes the basic theory behind each of the different techniques, the types of data produced from each, and some typical applications. Also discussed are the different types of samples that can be analyzed and the special sample-handling procedures that must be implemented when preparing to do failure analysis using these surface-sensitive techniques. Data obtained from different material defects are presented for each of the techniques. The examples presented highlight the typical data sets and strengths of each technique.
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006797
EISBN: 978-1-62708-295-2
... iron shot were fired, the shotgun barrel had a longitudinal profile of inside diameter as shown in the “After test” curve in Fig. 7(a) . Comparison of this curve with the profile before the test shows that the effect of firing soft iron shot was to deform the gun barrel so that the choke taper...
Abstract
Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated with a functional failure. Then, a more general consideration of distortion in failure analysis is introduced. Several common aspects of failure by distortion are discussed and suitable examples of distortion failures are presented for illustration. The article provides information on methods to compute load limits, errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003573
EISBN: 978-1-62708-180-1
... profile of inside diameter as shown in the “After test” curve in Fig. 7(a) . Comparison of this curve with the profile before the test shows that the effect of firing soft iron shot was to deform the gun barrel so that the choke taper was shifted toward the muzzle. After the test, there was a bulge...
Abstract
Distortion failure occurs when a structure or component is deformed so that it can no longer support the load it was intended to carry. Every structure has a load limit beyond which it is considered unsafe or unreliable. Estimation of load limits is an important aspect of design and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action. The article summarizes the general process of distortion failure analysis. It also discusses three types of distortion failures that provide useful insights into the problems of analyzing unusual mechanisms of distortion. These include elastic distortion, ratcheting, and inelastic cyclic buckling.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003569
EISBN: 978-1-62708-180-1
... disks, vibrating devices, or venturi tubes to achieve the required fluid velocities ( Ref 56 ). Another device used to produce cavitation and erosion is the liquid gun, which projects short, discrete slugs of liquid out of a nozzle onto the specimen ( Ref 57 ). Details of other nonstandard test...
Abstract
This article considers two mechanisms of cavitation failure: those for ductile materials and those for brittle materials. It examines the different stages of cavitation erosion. The article explains various cavitation failures including cavitation in bearings, centrifugal pumps, and gearboxes. It provides information on the cavitation resistance of materials and other prevention parameters. The article describes two American Society for Testing and Materials (ASTM) standards for the evaluation of erosion and cavitation, namely, ASTM Standard G 32 and ASTM Standard G 73. It concludes with a discussion on correlations between laboratory results and service.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006831
EISBN: 978-1-62708-329-4
Abstract
The information provided in this article is intended for those individuals who want to determine why a casting component failed to perform its intended purpose. It is also intended to provide insights for potential casting applications so that the likelihood of failure to perform the intended function is decreased. The article addresses factors that may cause failures in castings for each metal type, starting with gray iron and progressing to ductile iron, steel, aluminum, and copper-base alloys. It describes the general root causes of failure attributed to the casting material, production method, and/or design. The article also addresses conditions related to the casting process but not specific to any metal group, including misruns, pour shorts, broken cores, and foundry expertise. The discussion in each casting metal group includes factors concerning defects that can occur specific to the metal group and progress from melting to solidification, casting processing, and finally how the removal of the mold material can affect performance.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003508
EISBN: 978-1-62708-180-1
Abstract
This article focuses on the general root causes of failure attributed to the casting process, casting material, and design with examples. The casting processes discussed include gravity die casting, pressure die casting, semisolid casting, squeeze casting, and centrifugal casting. Cast iron, gray cast iron, malleable irons, ductile iron, low-alloy steel castings, austenitic steels, corrosion-resistant castings, and cast aluminum alloys are the materials discussed. The article describes the general types of discontinuities or imperfections for traditional casting with sand molds. It presents the international classification of common casting defects in a tabular form.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003551
EISBN: 978-1-62708-180-1
... layers or more with thicknesses varying from at least 100 mm (4 in.) up to 500 mm (20 in.) or more. Refractories are either shaped materials (bricks and various other formats, including lances, tubes, nozzles, and so forth) or unshaped or monolithic materials (delivered to the users in bags, sacks...
Abstract
This article provides a discussion on the structural ceramics used in gas turbine components, the automotive and aerospace industries, or as heat exchangers in various segments of the chemical and power generation industries. It covers the fundamental aspects of chemical corrosion and describes the corrosion resistance characteristics of specific classes of refractories and structural ceramics. The article also examines the prevention strategies that minimize corrosion failures of both classes of materials.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003534
EISBN: 978-1-62708-180-1
... with the use of an inert gas sputter ion gun. The ion gun is used to slowly remove material, thus exposing a new surface to be analyzed. By sequentially sputtering and taking XPS data, a compositional depth profile can be generated ( Fig. 6 ). If the chemical matrix of the sample is not severely damaged...
Abstract
This article provides information on the chemical characterization of surfaces by Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (XPS), and time-of-flight secondary ion mass spectrometry (TOF-SIMS). It describes the basic theory behind each of these techniques, the types of data produced from each, and some typical applications. The article explains the strengths of AES, XPS, and TOF-SIMS based on data obtained from the surface of a slightly corroded stainless steel sheet.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.9781627083959
EISBN: 978-1-62708-395-9
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006782
EISBN: 978-1-62708-295-2
Abstract
Corrosion is the deterioration of a material by a reaction of that material with its environment. The realization that corrosion control can be profitable has been acknowledged repeatedly by industry, typically following costly business interruptions. This article describes the electrochemical nature of corrosion and provides the typical analysis of environmental- and corrosion-related failures. It presents common methods of testing of laboratory corrosion and discusses the processes involved in the prevention of environmental- and corrosion-related failures of metals and nonmetals.
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