Spalled fragments from the work rolls of a steel bar straightening machine were received for failure analysis. Visual inspection coupled with optical and scanning electron microscopy were used as the principal analytical techniques for the investigation. Fractographic analysis revealed the presence of a characteristic fatigue crack propagation pattern (beach marks) and radial chevron marks indicating the occurrence of final overload through a brittle intergranular fracture. The collected evidence suggests that surface-initiated cracks propagated by fatigue led to spalling, resulting in severe work roll damage as well as machine downtime and increased maintenance costs.

A helicopter was hovering approximately 10 ft above a ship when one spar section failed explosively. Visual inspection revealed a crack had progressed through one member of a dual spar plate assembly at a fold pin lug hole. The remaining spar plate carried the blade load until the aircraft was landed. The helicopter main rotor blade spar fracture was analyzed by conventional and advanced computerized fractographic techniques. Digital fractographic Imaging Analysis of theoretical and actual fracture surfaces was applied for automatic detection of fatigue striation spacing. The approach offered a means of quantification of fracture features, providing for objective fractography.

A fractograph of the failed spring was found to indicate light streaks are parallel to the wire axis. A darker depressed area was visible between the streaks and below the center of the fractograph in which distinct outlines that represent sharp corners in the depressions were revealed by careful examination. A hard material (mill scale) was assumed to have been impressed during drawing of the wire and was broken out during peening, leaving the depressions with sharp-bottomed corners. Spring was concluded to have failed due to a surface defect.

A type 431 stainless steel mushroom-head closure fractured in service at a hydrogen pressure of 3000 atm. Fracture occurred at room temperature after miscellaneous chemical service that included exposures to hydrogen at temperatures from ambient to 350 deg C (662 deg F). Investigation (visual inspection and 2400x/6600x TEM analysis) supported the conclusion that failure was caused by hydrogen embrittlement, not SCC as might have been suspected. No recommendations were made.

The quantitative characterization of fracture surface geometry, that is, quantitative fractography, can provide useful information regarding the microstructural features and failure mechanisms that govern material fracture. This article is devoted to the fractographic techniques that are based on fracture profilometry. This is followed by a section describing the methods based on scanning electron microscope fractography. The article also addresses procedures for three-dimensional fracture surface reconstruction. In each case, sufficient methodological details, governing equations, and practical examples are provided.

The bone cement failed at the distal end of the prosthesis stem of femoral head prosthesis six months after implantation. A small indentation on the lateral contour of the stem was visible where the stem had broken. The degree of loosening (gap between the lateral stem contour and the bone or cement) and implant loading was revealed by the dislocation of fragments of the prosthesis. Secondary cracks that had originated at the lateral aspect of the stem were revealed by metallographic examination of a section parallel to the stem surface and perpendicular to the fracture surface of the distal fragment. Gas pores are apparent in the grain and at the grain boundaries were revealed by a transverse section. Fine parallel line structures that run diagonally through the fractograph may be slip traces were revealed by scanning electron microscopy. One of the cracks was revealed to have propagated through a larger gas pore by a ruptured gas pore. The stresses created through the fatigue process activated glide systems which served the formation of secondary cracks along glide planes.

Recurring, premature failures occurred in TiN-coated M2 gear hobs used to produce carbon steel ring gears. Fractographic and metallographic examination, microhardness testing, and chemical analysis by means of EDS revealed that the primary cause of failure was a coarse cellular carbide network, which created a brittle path for fracture to occur longitudinally. As the cellular carbide network must be dispersed and refined during hot working of the original bar of material, the hobs were not salvageable. Minor factors contributing to the hob failures were premature wear resulting from lower matrix hardness and high sulfur content of the material, which contributed to lower ductility through increased nucleation sites. It was recommended that the hob manufacturer specify a minimum amount of required reduction for the original bar of tool steel material, to provide for sufficient homogenization of the carbides in the resultant hob, and lower sulfur content.

The 8620 steel latch tip, carburized and then induction hardened to a minimum surface hardness of 62 HRC, on the main-clutch stop arm on a business machine fractured during normal operation when the latch tip was subjected to intermittent impact loading. Fractographic examination 9x showed a brittle appearance at the fractures. Micrograph examination of an etched section disclosed several small cracks. Fracture of the parts may have occurred through similar cracks. Also observed was a burned layer approximately 0.075 mm (0.003 in.) deep on the latch surface, and hardness at a depth of 0.025 mm (0.001 in.) in this layer was 52 HRC (a minimum of 55 HRC was specified). Thus, the failure was caused by brittle fracture in the hardness-transition zone as the result of excessive impact loading. The burned layer indicated that the cracks had been caused by improper grinding after hardening. Redesign was recommended to include reinforcing the backing web of the tip, increasing the radius at the relief step to 1.5 x 0.5 mm (0.06 x 0.02 in.), the use of proper grinding techniques, and a requirement that the hardened zone extend a minimum of 1.5 mm (0.06 in.) beyond the step.

A drawbar connecting two tank-type trailers of a highway gasoline rig broke while the rig was on an exit ramp of an interstate highway. The drawbar was a weldment of steel plates, tubes, and castings. Light fractography showed no discernable causes for the failure, but a TEM fractograph at 20,000x revealed fatigue striations and corrosion products on the fracture surface, indicating that this area was probably the site of fracture origin and that it had cracked before the accident happened. The casting on the right side of the drawbar contained large voids and a significant amount of porosity. Electron fractography established that the cast connection on the left side failed by brittle fracture. Metallographic examination showed poor weld quality in the casting-to-tube joint. Evidence found supports the conclusions that the drawbar fractured in fatigue, which originated in the weld joining the cast connector to the right side of the drawbar assembly. The crack initiated in a region of poor weld quality. A contributing factor to fracture of both connectors was the presence of voids and porosity in the castings. Recommendations included revising the welding procedures and instituting receiving inspection of the connection castings.

This paper describes the metallurgical investigation of a broken spindle used to attach an antenna to the mast of a naval vessel. Visual inspections of both failed and intact fastener assemblies were carried out both on-board ship and in the laboratory followed by metallographic and fractographic examinations. Simulations were also performed on stressed material in a suitable environment to assess the relative importance of postulated failure mechanisms. Factors contributing to this failure including assembly procedures and applied preloads, service loading and environment, and material selection and specification. The discussion considers whether this failure was an isolated incident or is likely to be a fleet-wide problem, and suggests ways to prevent reoccurrence.

The circumstances surrounding the in-service failure of a cast Ni-base superalloy (Alloy 713LC) second stage turbine blade and a cast and coated Co-base superalloy (MAR-M302) first stage air-cooled vane in two turbine engines used for marine application are described. An overview of a systematic approach, analyzing the nature of degeneration and failure of the failed components, utilizing conventional metallurgical techniques, is presented. The topographical features of the turbine blade fracture surface revealed a fatigue-induced crack growth pattern, where crack initiation had taken place in the blade trailing edge. An estimate of the crack-growth rate for the stage II fatigue fracture region coupled with the metallographic results helped to identify the final mode of the turbine blade failure. A detailed metallographic and fractographic examination of the air-cooled vane revealed that coating erosion in conjunction with severe hot-corrosion was responsible for crack initiation in the leading edge area.

One 49-in. impeller of a two-stage centrifugal air compressor disrupted without warning, causing extensive damage to the casings, the second impeller, and the driving gear box. Prior to the mishap, the machine had run normally, with no indications of abnormal vibration, temperature, or pressure. Initial failure had taken place in the floating dished inlet plate (eye plate) of the first-stage impeller. Failure occurred predominantly by tearing along the lines of rivet holes for the longer blades, these extended for practically the full radial width of the dished plate. Examination of the fractured surfaces showed that failure had been preceded by fatigue cracking. The material from which the dish plate was forged was a Ni-Cr-Mo steel in the oil hardened and tempered condition. Fractographic examination of the surface of the cracks showed striation markings indicative of the progress of fatigue cracks. Failure of the one impeller and the cracking of the others were attributed to “low-cycle high-strain fatigue” due to fluctuating circumferential (hoop) stresses.

A root cause failure analysis was performed on a vaporizer coil removed from a horizontal forced circulation vaporizer. The carbon steel coil was wound in a right-hand helix with a coil centerline diameter of about 2 m. The vaporizer was gas fired and used Dowtherm A as the heat transfer fluid. Design conditions are based on annular fluid flow to cool the coil wall. NDE, metallographic and fractographic examinations were performed. Numerous, circumferentially oriented, OD initiating cracks were found near the crown for two coils near the non-fired end of the vaporizer. The cracking was confined to the inner diameter of the vaporizer coil at positions from 4:00 to 7:00. The cracking was characterized as transgranular and the fracture surface had beach marks. The failure mechanism was thermal fatigue. The heat transfer calculation predicted that dryout of the coil would occur for coils at the non-fired end of the vaporizer during low flow transients. Dryout results in rapid increase in the tube wall temperature. Thermal cycling of the coil is completed by liquid quenching resulting from resumption of normal flow rates and the return to annular flow. The probable root cause of failure was low flow transient operation.

Important clues about the probable cause of a gun tube explosion were obtained from a fractographic and metallographic examination of the fragments. The size, distribution, and surface markings of fragments may be used to localize the explosion and deduce its intensity. Microstructural features such as voids, adiabatic shear, and structural surface alterations also indicate the explosion intensity and further allow a comparison of the tube structure near and away from the explosion zone. These, and other metallurgical characteristics, are illustrated and discussed for cases of accidental and deliberately caused explosions of large caliber gun tubes.

Several deburring drums that fractured were filled with abrasive, water, and small parts, such as roller bearing rollers, and rotated on their axis at 36 rpm. Cracks were discovered very early in the service lives of these high-chromium white iron cast structures. All of the fractures were through bolt holes in the mounting flange. The holes had a sharp edge and exhibited uneven wear on the inside diameter. In operation, the mounting bolts were frequently found to be loose and in at least one case broken off. A 25x scanning electron microscopy (SEM) fractograph from near this fracture-initiation area showed fatigue striations. No casting or metallurgical structural defects were found that could explain the failures. This evidence supports the conclusion that cracking was a result of the stress-concentration site at the bolt holes where a fatigue-initiated fracture occurred. Recommendations included that the radii be increased at the sharp corners and that lock-wiring be used to secure against bolt loosening.

Stainless steel liners (AISI type 321) used in bellows-type expansion joints in a duct assembly installed in a low-pressure nitrogen gas system failed in service. The duct assembly consisted of two expansion joints connected by a 32 cm (12 in.) OD pipe of ASTM A106 grade B steel. Elbows made of ASTM A234 grade B steel were attached to each end of the assembly, 180 deg apart. A 1.3 mm (0.050 in.) thick liner with an OD of 29 cm (11 in.) was welded inside each joint. The upstream ends were stable, but the downstream ends of the liners remained free, allowing the components to move with the expansion and contraction of the bellows. Investigation (visual inspection, hardness testing, and 30x fractographs) supported the conclusion that the liners failed in fatigue initiated at the intersection of the longitudinal weld forming the liner and the circumferential weld by which it attached to the bellows assembly. Recommendations included increasing the thickness of the liners from 1.3 to 1.9 mm (0.050 to 0.075 in.) in order to damp some of the stress-producing vibrations.

This article describes the visual, fractographic, and metallographic evidence typically encountered when analyzing stress rupture of turbine airfoils. Stress-rupture fractures are generally heavily oxidized, tend to be rough in texture, and are primarily intergranular and/or interdendritic in appearance compared to smoother, transgranular fatigue type fractures. Often, gross plastic yielding is visible on a macroscopic scale. Commonly observed microstructural characteristics include creep voiding along grain boundaries and/or interdendritic regions. Internal voids can also nucleate at carbides and other microconstituents, especially in single crystal castings that do not possess grain boundaries.

An investigation of a damaged crankshaft from a horizontal, six-cylinder, in-line diesel engine of a public bus was conducted after several failure cases were reported by the bus company. All crankshafts were made from forged and nitrided steel. Each crankshaft was sent for grinding, after a life of approximately 300,000 km of service, as requested by the engine manufacturer. After grinding and assembling in the engine, some crankshafts lasted barely 15,000 km before serious fractures took place. Few other crankshafts demonstrated higher lives. Several vital components were damaged as a result of crankshaft failures. It was then decided to send the crankshafts for laboratory investigation to determine the cause of failure. The depth of the nitrided layer near fracture locations in the crankshaft, particularly at the fillet region where cracks were initiated, was determined by scanning electron microscope (SEM) equipped with electron-dispersive X-ray analysis (EDAX). Microhardness gradient through the nitrided layer close to fracture, surface hardness, and macrohardness at the journals were all measured. Fractographic analysis indicated that fatigue was the dominant mechanism of failure of the crankshaft. The partial absence of the nitrided layer in the fillet region, due to over-grinding, caused a decrease in the fatigue strength which, in turn, led to crack initiation and propagation, and eventually premature fracture. Signs of crankshaft misalignment during installation were also suspected as a possible cause of failure. In order to prevent fillet fatigue failure, final grinding should be done carefully and the grinding amount must be controlled to avoid substantial removal of the nitrided layer. Crankshaft alignment during assembly and proper bearing selection should be done carefully.

The drive shaft in a marine propulsion system broke, stranding a large vessel along the Canadian seacoast. The shaft was made from quenched and tempered low-alloy steel. Fractographic investigation revealed that the shaft failed under low rotating-bending variable stress. Fatigue propagation occurred on about 95% of the total cross section of the shaft, under both low-cycle and high-cycle fatigue mechanisms. It was found that the fillet radius at the fracture’s origin was smaller than the one provisioned by design. As a result, the stresses at this location exceeded the values used in the design calculations, thus causing the initiation of the cracking. Moreover, although the shaft had been quenched and tempered, its actual hardness did not have the optimal value for long-term fatigue strength.

Wind turbine blades are secured by a number of high-strength bolts. The failure of one such bolt, which caused a turbine blade to detach, was investigated to determine why it fractured. Based on the results of a detailed analysis, consisting of stress calculations, chemical composition testing, metallurgical examination, mechanical property testing, and fractographic analysis, it was determined that the bolt failed by fatigue accelerated by stress concentration at low temperatures. The investigation also provided suggestions for avoiding similar failures.