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Flanges, corrosion
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Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001336
EISBN: 978-1-62708-215-0
... Abstract Catastrophic pitting corrosion occurred in type 304L stainless steel pipe flange assemblies in an industrial food processor. During regular service the pumped medium was pureed vegetables. In situ maintenance procedures included cleaning of the assemblies with a sodium hypochlorite...
Abstract
Catastrophic pitting corrosion occurred in type 304L stainless steel pipe flange assemblies in an industrial food processor. During regular service the pumped medium was pureed vegetables. In situ maintenance procedures included cleaning of the assemblies with a sodium hypochlorite solution. It was determined that the assemblies failed due to an austenite-martensite galvanic couple activated by a chlorine bearing electrolyte. The martensitic areas resulted from a transformation during cold-forming operations. Solution annealing after forming, revision of the design of the pipe flange assemblies to eliminate the forming operation, and removal of the source of chlorine were recommended.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001060
EISBN: 978-1-62708-214-3
... was caused by intergranular corrosion/stress-corrosion cracks that initiated from the external surface of the pipe reducer section. Contributory factors were the sensitized condition of the flange and the concentration of corrosive elements from the bleach stock plant environment on the external surface...
Abstract
A type 316 stainless steel pipe reducer section failed in service of bleached pulp stock transfer within 2 years in a pulp and paper mill. The reducer section fractured in the heat-affected zone of the flange-to-pipe weld on the flange side. The pipe reducer section consisted of 250 and 200 mm (10 and 8 in.) diam flanges welded to a tapered pipe section. The tapered pipe section was 3.3 mm (0.13 in.) thick type 316 stainless steel sheet, and the flanges were 5 mm (0.2 in.) thick CF8M (type 316) stainless steel castings. Visual and metallographic analysis indicated that the fracture was caused by intergranular corrosion/stress-corrosion cracks that initiated from the external surface of the pipe reducer section. Contributory factors were the sensitized condition of the flange and the concentration of corrosive elements from the bleach stock plant environment on the external surface. In the absence of the sensitized condition of the flange, the service of the pipe reducer section was acceptable. A type 316L stainless steel reducer section was recommended to replace the 316 component because of its superior resistance to sensitization.
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in Corrosion of Steel Pipe in a Heating and Cooling System
> ASM Failure Analysis Case Histories: Failure Modes and Mechanisms
Published: 01 June 2019
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in Intergranular Corrosion/Cracking of a Stainless Steel Pipe Reducer Section in Bleached Pulp Stock Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 2 Internal surface of the flange was free of corrosion. Several secondary stress-corrosion cracks penetrated the flange thickness. 1.5×.
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in Intergranular Corrosion/Cracking of a Stainless Steel Pipe Reducer Section in Bleached Pulp Stock Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 6 Intergranular corrosion on the external surface of the flange and IGSCC in the weld HAZ. Note that the type 316 weld and the wrought stainless steel pipe section were unaffected by corrosion. 5×.
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in Intergranular Corrosion/Cracking of a Stainless Steel Pipe Reducer Section in Bleached Pulp Stock Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 7 Intergranular corrosion at the external surface of the flange and IGSCC next to the flange fillet. 5×.
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in Intergranular Corrosion/Cracking of a Stainless Steel Pipe Reducer Section in Bleached Pulp Stock Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 8 Intergranular corrosion at the external surface of the flange. The voids are the locations of the spalled grains. 50×.
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Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001421
EISBN: 978-1-62708-235-8
... deposit. While the fracture in the weld metal was of the ductile type exhibiting a fine fibrous appearance, that in the flange material was of the cleavage type. Microscopic examination revealed that the cracks were blunt-ended fissures of the type characteristic of corrosion-fatigue. It was concluded...
Abstract
The bottom flange of a vertical pipe coupled to an isolating valve in a steam supply line to a turbine failed. Steam pressure was 1,500 psi and the temperature 416 deg C (780 deg F). Multiple cracking occurred in the bore of the flange. A quarter-segment was cut out and examined. The cracks were located in the part of the flange that formed a continuation of the pipe bore. The majority of them originated at the end of the flange bore and extended axially along the pipe and radially across the flange face. Magnetic crack detection revealed a further number of cracks in the weld deposit. While the fracture in the weld metal was of the ductile type exhibiting a fine fibrous appearance, that in the flange material was of the cleavage type. Microscopic examination revealed that the cracks were blunt-ended fissures of the type characteristic of corrosion-fatigue. It was concluded that cracking was due to corrosion-fatigue, which arose from the combined effect of a fluctuating tensile stress in the presence of a mildly corrosive environment.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0006428
EISBN: 978-1-62708-217-4
..., 217, and 250. Scanning electron microscopy (SEM) examination of the fractures showed that failure initiated by SCC or a corrosion pit on all failures examined. The failures then progressed by fatigue. Dye penetrant testing revealed no additional flaws on the wheels that had failed in the flange area...
Abstract
Four nose wheels fabricated from 2014-T6 aluminum alloy and cold worked at the flange were examined. Visual examination showed that the failure started in the tube well area on the wheel with serial number 31. The failure initiated in the flange fillet on wheels with serial numbers 67, 217, and 250. Scanning electron microscopy (SEM) examination of the fractures showed that failure initiated by SCC or a corrosion pit on all failures examined. The failures then progressed by fatigue. Dye penetrant testing revealed no additional flaws on the wheels that had failed in the flange area. There was, however, one flaw area in the flange of the wheel that failed in the tube well. This flaw resembled a corrosion pit. It was concluded that failure of nose wheels 67, 217, and 250 was caused by cracking due to SCC or pitting. The failures progressed by fatigue. Because failure occurred in the same general area on all three wheels, these locations are suspect as being underdesigned. It was recommended that the nose wheel be redesigned and additional service data be accumulated to understand the contributing factors that resulted in wheel failure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001774
EISBN: 978-1-62708-241-9
... steel; the flange from type 321, and the ring gasket from 347. Examination revealed that the failure occurred by transgranular stress-corrosion cracking, initiated by the presence of polythionic acid. Detailed metallurgical investigation was subsequently conducted to identify what may have caused...
Abstract
A ring-type joint in a reactor pipeline for a hydrocracker unit had failed. Cracks were observed on the flange and the associated ring gasket during an inspection following a periodic shutdown of the unit. The components were manufactured from stabilized grades of austenitic stainless steel; the flange from type 321, and the ring gasket from 347. Examination revealed that the failure occurred by transgranular stress-corrosion cracking, initiated by the presence of polythionic acid. Detailed metallurgical investigation was subsequently conducted to identify what may have caused the formation of polythionic acid in the process gas.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0006406
EISBN: 978-1-62708-217-4
... Abstract A crack was found in an aircraft main wing spar flange fabricated from 7079-T6 aluminum alloy during a routine nondestructive x-ray inspection after the craft had logged 300 h. Scanning electron microscopy (SEM) revealed an intergranular fracture pattern indicative of stress-corrosion...
Abstract
A crack was found in an aircraft main wing spar flange fabricated from 7079-T6 aluminum alloy during a routine nondestructive x-ray inspection after the craft had logged 300 h. Scanning electron microscopy (SEM) revealed an intergranular fracture pattern indicative of stress-corrosion cracking (SCC) and fatigue striations near the crack origin. Visual examination of the crack edge revealed that the installation of the fasteners produced a fit up stress. Further inspection of the opened fracture showed that the crack had been present for some time because a heavy buildup of corrosion products was seen on the fractured surface. Metallographic examination of the flange in the area of fracture initiation showed the presence of end grain exposure, which would promote SCC. Electron optical examination of the fracture clearly showed the flange was cracking by a mixed mode of stress corrosion and fatigue. The cracking was accelerated because of an inadvertent fit up stress during installation. The age of the crack could not be established. However, a reevaluation of prior x-ray inspections in this area would result in some close estimate of the age of the crack. End grain exposure further promoted SCC.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c9001249
EISBN: 978-1-62708-236-5
... Abstract The flanged bearing bush carrying the drive shaft of a feed pump suddenly fractured after about two years of service. The chemical composition was normal for high chromium ledeburitic cast steel, which was corrosion and wear resistant as well as refractory. For unknown reasons...
Abstract
The flanged bearing bush carrying the drive shaft of a feed pump suddenly fractured after about two years of service. The chemical composition was normal for high chromium ledeburitic cast steel, which was corrosion and wear resistant as well as refractory. For unknown reasons the rotating shaft came into direct contact with the flange. Mechanical friction caused a rise in temperature on both contact surfaces. This mutual contact lasted long enough for the temperature in the contact zone to exceed 1200 deg C, at which the flange material became softened or molten. As a result, considerable structural changes took place on the inner wall of the flange. Thermal stresses and excessive mechanical loads due to smearing of the flange material then led to fracture of the flange.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001071
EISBN: 978-1-62708-214-3
... kPa (150 psi) and 120 deg C (250 deg F) maximum in 93 to 99% sulfuric acid. The fracture originated at stress-corrosion cracks that occurred in a high-stress transition region at the valve body-to-flange juncture. The mechanical properties of the failed valve were below those of the manufacturer's...
Abstract
A gray cast iron (ASTM 247 type A) gate valve in an oleum and sulfuric acid piping loop at a chemical process plant fractured catastrophically after approximately 10 years of service. The valve was a 150 mm (6 in.) bolted flange type rated to conform to ANSI B16.1 for service at 1034 kPa (150 psi) and 120 deg C (250 deg F) maximum in 93 to 99% sulfuric acid. The fracture originated at stress-corrosion cracks that occurred in a high-stress transition region at the valve body-to-flange juncture. The mechanical properties of the failed valve were below those of the manufacturer's cited specification, and the wall thickness through which the fracture occurred exceeded the minimum 9.5 mm (38 in.) thickness cited by the manufacturer The valve flange had been unbolted and rebolted to a maintenanced piping coil immediately prior to failure. It was recommended that the flange-to-valve body juncture be redesigned to reduce stress levels. A method of maintenance and inspection in concert with a criterion for life prediction for this and other valves and components in the system was also recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001679
EISBN: 978-1-62708-229-7
... Outside Diffuser Shot Peen 1988 EB 1 yes—erosion yes—corrosion and crack propagation no 1988 MP =12 yes—cavitation yes—corrosion and crack propagation no 1989 EB (cracked) =6 no corrosion product/no cracking yes—EB weld out on flange 1989 EB no no corrosion product...
Abstract
Several mercury diffusion pump stages in the Tritium Purification process at the Savannah River Site (SRS) have been removed from service for scheduled preventive maintenance. These stages have been examined to determine if failure has occurred. Evidence of fatigue around the flange portion of the pump has been seen. In addition, erosion and cavitation inside the throat of the venturi tube and corrosion on the other surface of the venturi tube has been observed. Several measures are being examined in an attempt to improve the performance of these pumps. These measures, as well as the noted observations, are described. Six stages [two machined (MP) and four electron beam (EB) welded] from the mercury diffusion pumps operating in the Tritium Purification process at SRS have been analyzed to determine their condition after nine months of usage. Several cracks were found around the necked region of the two MP stages. The EB welded stages, however, seemed to perform better in service; only two of four stages showed cracking. The cracking is caused by fatigue that has been enhanced by high stresses and tritium in the flange area. The EB welded stage appears to be a step in the right direction. Since the EB weld is a shrink fit, the surface is in compression, thereby eliminating crack propagation. In addition, shot peening has been employed to produce a compressive material surface since fatigue usually originates at the surface. Pitting was observed down the throat of the venturi. This pitting was caused by cavitation and erosion along the length of the venturi tube. Corrosion and pitting was seen on the exterior walls of the diffuser tubes. Stress-corrosion cracks were observed emanating from these corrosion pits. The corrosion likely occurred from the chloride ions present in the process cooling water. Shot peening is now being used in an attempt to place the outside of the diffuser tube in compression to eliminate the stress-corrosion cracking.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0047076
EISBN: 978-1-62708-217-4
... electron microscope fractographs, hardness testing, and electrical conductivity testing) supported the conclusions that the failure was caused by fatigue cracks originating on the inside curved surface of the flanges. The cracks had initiated in surface defects caused by either corrosion pitting or forming...
Abstract
Two cracks were discovered in a deck plate of an aircraft during overhaul and repair after 659 h of service. The cracks were on opposite sides of the deck plate in the flange joggles. The plate had been formed from 7178-T6 aluminum alloy sheet. Analysis (visual inspection, 0.2x/2x/2.3x electron microscope fractographs, hardness testing, and electrical conductivity testing) supported the conclusions that the failure was caused by fatigue cracks originating on the inside curved surface of the flanges. The cracks had initiated in surface defects caused by either corrosion pitting or forming notches, acting in combination with lateral forces evidenced by the moderate distortion of the fastener holes. Recommendations included eliminating the surface defects by revised cleaning and/or forming procedures. Revised design and installation should also alleviate the lateral forces.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001308
EISBN: 978-1-62708-215-0
... flange such that the crack plane was perpendicular to the tangential direction of the turntable rail. There was no visible evidence of plastic deformation associated with the crack. The contact surfaces of the rail appeared worn and contained many shallow wear craters. Slight corrosion of the contact...
Abstract
Persistent cracking in a forged 1080 steel turntable rail in a wind tunnel test section was investigated. All cracks were oriented transverse to the axis of the rail, and some had propagated through the flange into the web. Through-flange cracks had been repair welded. A section of the flange containing one through-flange crack was examined using various methods. Results indicated that the cracks had initiated from intergranular quench cracks caused by the use of water as the quenching medium. Brittle propagation of the cracks was promoted by high residual stresses acting in conjunction with applied loads. Repair welding was discontinued to prevent the introduction of additional residual stress., Finite-element analysis was used to show that the rail could tolerate existing cracks. Periodic inspection to monitor the degree of cracking was recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0091617
EISBN: 978-1-62708-220-4
... cracks in the flange-to-cone weld and in the base metal of the cone were characteristic of chloride stress-corrosion cracks in type 316 stainless steel. There were two possible sources of chlorides: boiler feedwater and insulation. The boiler feedwater was an unlikely source because it was monitored...
Abstract
A 680,000 kg (750 ton) per day ammonia unit was shut down following a fire near the outlet of the waste heat exchanger. The fire had resulted from leakage of ammonia from the type 316 stainless steel outlet piping. The outlet piping immediately downstream from the waste heat exchanger consisted of a flange made from a casting, and a reducing cone, a short length of pipe, and a 90 deg elbow, all made of 13 mm thick plate. A liner wrapped with insulation was welded to the smaller end of the reducing cone. All of the piping up to the flange was wrapped with insulation. Investigation (visual inspection, 10x unetched images, liquid-penetrant inspection, and chemical analysis of the insulation) supported the conclusion that the failure occurred in the area of the flange-to-cone weld by SCC as the result of aqueous chlorides leached from the insulation around the liner by condensate. Recommendations included eliminating the chlorides from the system, maintaining the temperature of the outlet stream above the dewpoint at all times, or that replacing the type 316 stainless steel with an alloy such as Incoloy 800 that is more resistant to chloride attack.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001537
EISBN: 978-1-62708-234-1
... corrosion mechanism. It probably started at the root of the straightening crack and then extended into the flange. Though a fatigue mechanism was operative in Region 3, it was not the cause of the large crack. Rather, it merely assisted crack growth by the stress corrosion mechanism. Region 4, which...
Abstract
After completing a fatigue test of an aluminum alloy component machined from a 7079-T6 forging, technicians noted a 5 in. crack which ran longitudinally above and through the flange. When the fracture face was examined by light microscopy, observers could not ascertain the exact mode of fracture. Electron fractography revealed that five different modes of crack growth were operative as the part failed. Region 1 was a shallow zone (about 0.002 in. at its deepest) of dimpled structure typical of an overload failure. Region 2 was a zone that grew by a stress corrosion mechanism. Through a fatigue mechanism was operative in Region 3, it was not the cause of the large crack. Region 4, which covered 50% of the fracture area, developed mainly by stress corrosion. This zone gradually changed into the combination of intergranular and transgranular overload in Region 5, which covered approximately the remaining 50% of the fracture. Apparently, after stress corrosion moved halfway through, the part failed by overload. This failure analysis proved that a crack, originally thought to be a fatigue failure, was actually a stress corrosion crack.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0091394
EISBN: 978-1-62708-227-3
... of austenitic stainless steel: the bottom surface, weld or HAZ pits, and crevices. Recommendations included proper material selection for piping, flanges, and weld rods with greater corrosion resistance. Proper filtering to prevent entrained abrasives and timely breakdown inspections were also advised...
Abstract
An austenitic stainless steel (type 316/316L stainless steel, schedule 40, 64 mm (2.5 in.) diam and larger) piping network used in the fire-sprinkler system in a large saltwater passenger and car ferry failed by rapid leaking. Operating conditions involved stagnant seawater at ambient temperatures. The pipe was in service for four weeks when three leaks appeared. Investigation (visual inspection and photographic images) supported the conclusion that the failure was caused by attack and corrosion damage of Cl ions in conditions that were ideal for three modes of highly accelerated pitting of austenitic stainless steel: the bottom surface, weld or HAZ pits, and crevices. Recommendations included proper material selection for piping, flanges, and weld rods with greater corrosion resistance. Proper filtering to prevent entrained abrasives and timely breakdown inspections were also advised.
Image
in Corrosion Fatigue of Aircraft Nose Wheels
> ASM Failure Analysis Case Histories: Air and Spacecraft
Published: 01 June 2019
Fig. 1 Aluminum alloy 2014-T6 aircraft nose wheel (a) that failed at the flange. (b) Close-up of tube well on wheel 31. (c) Appearance of flange failure on wheel 67. The topography is typical of other flange failures. (d) Close-up of wheel 31; note indentation (arrow). (e) Close-up of wheel
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