An evaluation of indications in the main turbine building column horizontal plate welds was conducted by the joint efforts of field metallography and nondestructive examinations. The turbine building main column horizontal plate welds were selected at random and were inspected to find discontinuities, metallurgical evaluation of the discontinuities, analysis of any failure modes, and determination of the best repair techniques. The welds were made with prequalified joints in accordance with AWS D1.1-77 and required only visual inspection. More sensitive inspection methods were applied to the welds in order to better define the indications found with the visual inspections. Cracks were found in 17 field welds and in two test plate welds. The causes of the cracking are related to the weld design and installation procedure. Three field welds were rejected because of the depth of the cracks. The NDT inspections, evaluations, method of field metallography, analysis and conclusions are discussed with recommendations for corrective actions in the following report.

Stress-corrosion cracking of low-alloy steel turbine discs has emerged as a generic concern in nuclear generating stations. An investigation that made extensive use of field metallographic techniques to examine suspected cracking in such a component is described. The crack position, and its relationship to surface topographic features, were examined and recorded by magnetic rubber and high-resolution dental rubber replicating materials. Corrosion deposits on keyway surfaces and within the crack were collected with acetate foil replicas applied and then stripped from the keyway surfaces. Microstructural details were revealed by the use of field metallographic preparation techniques and replicated by acetate foil for examination with optical and scanning electron microscopes. It was possible by these techniques to establish the cracking mechanism as stress corrosion possibly related to chloride or sulphate ion steam contaminants. Subsequent sectioning and conventional metallography confirmed both the validity of the conclusions and the replication techniques.

Field metallography and replication were performed on a type 316 stainless steel column in diglycol amine vacuum service to determine the cause of visible OD pitting on the column in several areas above the insulation support rings. The examination revealed transgranular stress-corrosion cracking beneath the pitted areas on the OD. The likely cause of the cracking was chloride stress corrosion, with chlorides deriving from the marine atmosphere and concentrating under the insulation around the support rings. A complete insulation evaluation, including repair or replacement, was recommended to prevent chloride buildup. Painting of the steel surface with an epoxy-phenolic or epoxy-coal tar was also suggested.

The 4140 steel steering spindle on a tricycle agricultural field chemical applicator failed, causing the loss of the front wheel and overturn of the vehicle. The spindle was a solid 120 mm (4.75 in.) diam forging. It had been machined to 115 mm (4.5 in.) in diameter to fit tightly inside a collar at one point and to 90 mm (3.5 in.) for attachment to the steering mechanism at another. Visual examination showed that the spindle fractured at the fillet welds that attached it to the collar. Macrofractography and metallography revealed that the failure initiated at the root of a weld that bridged a wide gap. The most probable cause of failure was improper preheat during welding.

The goal of using nondestructive evaluation (NDE) in conjunction with failure analysis is to obtain the most comprehensive set of data in order to characterize the details of the damage and determine the factors that allowed the damage to occur. The NDE results can be used to determine optimal areas upon which to focus for sectioning and metallography in order to further investigate the condition of the component. This article provides information on the inspection method available for failure analysis, including standard methods such as visual testing, penetrant testing, and magnetic particle testing. It covers the effects of various factors on the properties of the part that may impact failure analysis, describes the characterization of damage modes and crack sizes, and finally discusses the processes involved in application of NDE results to failure analysis.

Four truck cross members intended for use in heavy-duty transport trucks were investigated. Two of the members had cracked on a prototype vehicle and two had been fatigue tested in the laboratory. The cross members were fabricated from SAE 950X plate and consisted of a formed channel section and an internal fillet-welded diaphragm. Sections from each of the cross members were subjected to a complete analysis, including chemical analysis, magnetic particle testing, mechanical testing, scanning electron microscope/fractography, and metallography. The primary mode of failure was found to be fatigue cracking that initiated at the toes of the fillet welds. Secondary fatigue cracking occurred at the torque rod mounting holes. Failure was attributed to cyclic stresses at the weld toes that exceeded the lowered fatigue strength at this location. A design change that eliminated the fillet welds alleviated the problem.

Failure analysis is an investigative process that uses visual observations of features present on a failed component fracture surface combined with component and environmental conditions to determine the root cause of a failure. The primary means of recording the conditions and features observed during a failure analysis investigation is photography. Failure analysis photographic imaging is a combination of both science and art; experience and proper imaging techniques are required to produce an accurate and meaningful fracture surface photograph. This article reviews photographic principles and techniques as applied to failure analysis, both in the field and in the laboratory. The discussion covers the processes involved in field and laboratory photographic documentations, provides a description of professional digital cameras, and gives information on photographic lighting and microscopic photography. Special techniques can be employed to deal with highly reflective conditions and are also described in this article.

Cracks on the outer surface near a hanger lug were revealed by visual inspection of a type 316 stainless steel main steam line of a major utility boiler system. Cracking was found to have initiated at the outside of the pipe wall or immediately beneath the surface. The microstructure of the failed pipe was found to consist of a matrix precipitate array (M23C6) and large s-phase particles in the grain boundaries. A portable grinding tool was used to prepare the surface and followed by swab etching. All material upstream of the boiler stop valve was revealed to have oriented the cracking normally or nearly so to the main hoop stress direction. Residual-stress measurements were made using a hole-drilling technique and strain gage rosettes. Large tensile axial residual stresses were measured at nearly every location investigated with a large residual hoop stress was found for locations before the stop valve. It was concluded using thermal stress analysis done using numerical methods and software identified as CREPLACYL that one or more severe thermal downshocks might cause the damage pattern that was found. The root cause of the failure was identified to be thermal fatigue, with associated creep relaxation.

The principal task of a failure analyst during a physical-cause investigation is to identify the sequence of events involved in the failure. Technical skills and tools are required for such identification, but the analyst also needs a mental organizational framework that helps evaluate the significance of observations. This article discusses the processes involved in the characterization and identification of damage and damage mechanisms. It describes the relationships between damage causes, mechanisms, and modes with examples. In addition, some of the more prevalent and encompassing characterization approaches and categorization methods of damage mechanism are also covered.

Argonne National Laboratory has conducted analyses of failed components from nuclear power-generating stations since 1974. The considerations involved in working with and analyzing radioactive components are reviewed here, and the decontamination of these components is discussed. Analyses of four failed components from nuclear plants are then described to illustrate the kinds of failures seen in service. The failures discussed are (1) intergranular stress-corrosion cracking of core spray injection piping in a boiling water reactor, (2) failure of canopy seal welds in adapter tube assemblies in the control rod drive head of a pressurized water reactor, (3) thermal fatigue of a recirculation pump shaft in a boiling water reactor, and (4) failure of pump seal wear rings by nickel leaching in a boiling water reactor.

Two failures of AP15A grade J-55 electric resistance welded (ERW) tubing in as our gas environment were investigated. The first failure occurred after 112 days of service. Replacement pipe failed 2 days later. Surface examination of the failed tubing indicated that fracture initiated at the outside surface. Metallographic analysis showed that the fracture originated in the upturned fibers adjacent to the ERW bond line. Cross sections of the weld were removed from three random locations in the test sample. At each location, the up turned fibers of the weld zone contained bands of hard-appearing microstructure. Hardness measurements confirmed these observations. The cracks followed these bands. It was concluded that the tubing failed from sulfide stress cracking, which resulted from bands of susceptible microstructure in the ERW zone. The banded microstructure in the pipe suggested that chemical segregation contributed to the hard areas. Postweld normalized heat treatment apparently did not sufficiently reduce the hardness of these areas.

An intergranular stress-corrosion cracking failure of 304 stainless steel pipe in 2000 ppm B as H3BO3 + H2O at 100 deg C was investigated. Constant extension rate testing produced an intergranular type failure in material in air. Chemical analysis was performed on both the base metal and weld material, in addition to fractography, EPR testing and optical microscopy in discerning the mode of failure. Various effects of Cl-, O2 and MnS are discussed. Results indicated that the cause of failure was the severe sensitization coupled with probable contamination by S and possibly by Cl ions.

Failure analysis is a process that is performed in order to determine the causes or factors that have led to an undesired loss of functionality. This article is intended to demonstrate proper approaches to failure analysis work. The goal of the proper approach is to allow the most useful and relevant information to be obtained. The discussion covers the principles and approaches in failure analysis work, objectives and scopes of failure analysis, the planning stages for failure analysis, the preparation of a protocol for a failure analysis, practices used by failure analysts, and procedures of failure analysis.

Large quantities of aluminum-clad spent nuclear materials have been in interim storage in the fuel storage basins at The Savannah River Site while awaiting processing since 1989. This extended storage as a result of a moratorium on processing resulted in corrosion of the aluminum clad. Examinations of this fuel and other data from a corrosion surveillance program in the water basins have provided basic insight into the corrosion process and have resulted in improvements in the storage facilities and basin operations. Since these improvements were implemented, there has been no new initiation of pitting observed since 1993. This paper describes the corrosion of spent fuel and the metallographic examination of Mark 31A target slugs removed from the K-basin storage pool after 5 years of storage. It discusses the SRS Corrosion Surveillance Program and the improvements made to the storage facilities which have mitigated new corrosion in the basins.

Failure analysis was performed on a fractured impeller from a boiler feed pump of a fossil fuel power plant. The impeller was a 12% Cr martensitic stainless steel casting. The failure occurred near the outside diameter of the shroud in the vicinity of a section change at the shroud/vane junction. Sections cut from the impeller were examined visually and by SEM fractography. Microstructural, chemical, and surface analyses and surface hardness tests were conducted on the impeller segments. The results indicated that the impeller failed in fatigue with casting defects increasing stress and initiating fracture. In addition, the composition and hardness of the impeller did not meet specifications. Revision of the casting process and institution of quality assurance methods were recommended.

Cracks were discovered between interference-fit fasteners (MoS2-coated Ti-6Al-4V) that had been incorporated into a fighter aircraft primary structural frame (D6ac steel) to enhance structural fatigue life. Examination of sections cut from the cracked frame established that the cracks propagated by stress-corrosion cracking. The cause of cracking was twofold: use of interference-fit fasteners exposed to moisture intrusion from a marine environment and poor hole quality. Failure was intensified by dissimilar-metal contact in the presence of weak acidic electrolyte (dissociated MoS2). Control of machining parameters to prevent formation of brittle martensite, use of galvanically compatible fasteners, and use of an alternate lubricant were recommended.

As a failure investigation progresses, the time arrives when the data and results of the various testing and analyses are compiled, compared, and interpreted. Data interpretation should be relatively straightforward for results that align well. However, interpretation can be challenging when results from various tests seem contradictory or inconclusive. Regardless, conclusions must eventually be drawn from the data. This article discusses the processes involved in reviewing data, formulating conclusions, failure analysis report preparation and writing, and providing recommendations and follow-up with appropriate personnel to prevent future failures.

Alloy 430 stainless steel tube-to-header welds failed in a heat recovery steam generator (HRSG) within one year of commissioning. The HRSG was in a combined cycle, gas-fired, combustion turbine electric power plant. Alloy 430, a 17% Cr ferritic stainless steel, was selected because of its resistance to chloride and sulfuric acid dewpoint corrosion under conditions potentially present in the HRSG low-pressure feedwater economizer. Intergranular corrosion and cracking were found in the weld metal and heat-affected zones. The hardness in these regions was up to 35 HRC, and the weld had received a postweld heat treatment (PWHT). Metallographic examination revealed that the corroded areas contained undertempered martensite. Fully tempered weld areas with a hardness of 93 HRB were not attacked. No evidence of corrosion fatigue was found. Uneven temperature control during PWHT was the most likely cause of failure.

Metallographic examination is one of the most important procedures used by metallurgists in failure analysis. Typically, the light microscope (LM) is used to assess the nature of the material microstructure and its influence on the failure mechanism. Microstructural examination can be performed with the scanning electron microscope (SEM) over the same magnification range as the LM, but examination with the latter is more efficient. This article describes the major operations in the preparation of metallographic specimens, namely sectioning, mounting, grinding, polishing, and etching. The influence of microstructures on the failure of a material is discussed and examples of such work are given to illustrate the value of light microscopy. In addition, information on heat-treatment-related failures, fabrication-/machining-related failures, and service failures is provided, with examples created using light microscopy.

Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.