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in Creep, Stress Relaxation, and Yielding Mechanisms
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
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Comparison of creep curves for base material and longitudinal seam-weld met...
Available to Purchase
in Failure Investigation of Longitudinal Seam Welded Elevated Temperature Header
> ASM Failure Analysis Case Histories: Power Generating Equipment
Published: 01 June 2019
Fig. 7 Comparison of creep curves for base material and longitudinal seam-weld metal at 665 C and 41.4 MPa.
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Book Chapter
Fracture of Steam Pipes Removed From Service
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001128
EISBN: 978-1-62708-214-3
... Abstract Creep crack growth and fracture toughness tests were performed using test material machined from a seam welded ASTM A-155-66 class 1 (2.25Cr-1Mo) steel steam pipe that had been in service for 15 years. The fracture morphology was examined using SEM fractography. Dimpled fracture...
Abstract
Creep crack growth and fracture toughness tests were performed using test material machined from a seam welded ASTM A-155-66 class 1 (2.25Cr-1Mo) steel steam pipe that had been in service for 15 years. The fracture morphology was examined using SEM fractography. Dimpled fracture was found to be characteristic of fracture toughness specimens. Creep crack growth generally followed the fusion line region and was characterized as dimpled fracture mixed with cavities. These fracture morphologies were similar to those of an actual steam pipe. It was concluded that creep crack growth behavior was the prime failure mechanism of seam-welded steam pipes.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001132
EISBN: 978-1-62708-214-3
... environment. On this basis, it was concluded that creep of the solder alloy was the most probable cause of failure. Creep (materials) Fire protection Soldered joints Solders Solder alloy Creep fracture/stress rupture Background A sprinkler head unit that was installed in a smoking lounge...
Abstract
A sprinkler head unit that was installed in a smoking lounge of a multi story office building in 1975 failed, causing substantial water damage. There was no fire in the building. A set of four sprinkler heads -- three that had been installed in 1975 (the failed unit, an unfailed unit from the same room, and an unfailed unit from another room) and an unused 1991 unit -- were examined. casting revealed no material defects or mechanical damage. Because of several environmental factors, it was suspected that the failed unit was exposed to temperatures much above the normal office environment. On this basis, it was concluded that creep of the solder alloy was the most probable cause of failure.
Book Chapter
Metallographic Studies of a Reformer Tube Failure Due to Thermal Fatigue
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001675
EISBN: 978-1-62708-220-4
... high local stress. The study indicates that standard metallographic procedures can be used to identify failure modes in high temperature petrochemical plants. Creep (materials) Petrochemical plants Reformer tubes Incoloy 800H UNS N08810 Thermal fatigue fracture Tubing operating at high...
Abstract
The failure of a reformer tube furnace manifold has been examined using metallography. It has been shown that the cause of failure was thermal fatigue; the damage was characterized by the presence of voids produced by creep mechanisms operating during the high temperature cycle under high local stress. The study indicates that standard metallographic procedures can be used to identify failure modes in high temperature petrochemical plants.
Book Chapter
High-Temperature Failure by Perforation of Incoloy 800H Pigtails in Reformer Furnaces
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001108
EISBN: 978-1-62708-214-3
... be used for fabrication of the curved parts. A change of alloy to a low-alloy chromium-molybdenum allay to protect against heat was also suggested. Chemical processing equipment Chemical reactors Creep (materials) Pipe bends Tubing Incoloy 800H UNS N08810 Intergranular fracture Creep...
Abstract
The curved parts of exit pigtails made of wrought Incoloy 800H tubing used in steam reforming furnaces failed by performance after a period of service shorter than that predicted by the designers. Examination of a set of tubes consisting of both curved (perforated) and straight parts revealed that the cracks initiated at the outer surface by a combined mechanism of creep and intergranular embrittlement. A smaller grain size resulting from cold bending fabrication procedures for the curved parts was responsible for accelerating the embrittlement. It was recommended that hot bending be used for fabrication of the curved parts. A change of alloy to a low-alloy chromium-molybdenum allay to protect against heat was also suggested.
Book Chapter
Graphitization-Related Failure of a Low-Alloy Steel Superheater Tube
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001337
EISBN: 978-1-62708-215-0
... with chromium additions such as ASTM A213 Grade T11 or T22, which are resistant to graphitization damage. Boiler tubes Creep (materials) Graphitization, Heating effects Mechanical properties Microstructural effects Overheating ASTM A209 grade T1 UNS K11522 High-temperature corrosion and oxidation...
Abstract
A carbon-molybdenum (ASTM A209 Grade T1) steel superheater tube section in an 8.6 MPa (1250 psig) boiler cracked because of long-term overheating damage that resulted from prolonged exposure to metal temperatures between 482 deg C (900 deg F) and 551 deg C (1025 deg F). The outer diameter of the tube exhibited a crack (fissure) oriented approximately 45 deg to the longitudinal axis and 3.8 cm (1.5 in.) long. The inner diameter surface showed a fissure in the same location and orientation. Microstructure at the failure near the outer diameter surface exhibited evidence of creep cracking and creep void formation at the fissure. A nearly continuous band of graphite nodules was observed on the surface of the fissure. In addition to the graphite band formation, the microstructure near the failure exhibited carbide spheroidization from long-term overheating in all the tube regions examined. It was concluded that preferential nucleations of graphite nodules in a series of bands weakened the steel locally, producing preferred fracture paths. Formation of these graphite bands probably expedited the creep failure of the tube. Future failures may be avoided by using low-alloy steels with chromium additions such as ASTM A213 Grade T11 or T22, which are resistant to graphitization damage.
Book Chapter
Elevated-Temperature Life Assessment
Available to PurchaseSeries: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006807
EISBN: 978-1-62708-329-4
... it necessary to incorporate a service life when designing components for elevated-temperature service. Creep is one of the most common damage mechanisms of concern at elevated temperatures. Creep, in a general sense, refers to the progressive reduction in the ability of a material to resist stress...
Abstract
This article provides some new developments in elevated-temperature and life assessments. It is aimed at providing an overview of the damage mechanisms of concern, with a focus on creep, and the methodologies for design and in-service assessment of components operating at elevated temperatures. The article describes the stages of the creep curve, discusses processes involved in the extrapolation of creep data, and summarizes notable creep constitutive models and continuum damage mechanics models. It demonstrates the effects of stress relaxation and redistribution on the remaining life and discusses the Monkman-Grant relationship and multiaxiality. The article further provides information on high-temperature metallurgical changes and high-temperature hydrogen attack and the steps involved in the remaining-life prediction of high-temperature components. It presents case studies on heater tube creep testing and remaining-life assessment, and pressure vessel time-dependent stress analysis showing the effect of stress relaxation at hot spots.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006780
EISBN: 978-1-62708-295-2
... of creep-related failures, where the mechanical strength of a material becomes limited by creep rather than by its elastic limit. The majority of information provided is applicable to metallic materials, and only general information regarding creep-related failures of polymeric materials is given...
Abstract
The principal types of elevated-temperature mechanical failure are creep and stress rupture, stress relaxation, low- and high-cycle fatigue, thermal fatigue, tension overload, and combinations of these, as modified by environment. This article briefly reviews the applied aspects of creep-related failures, where the mechanical strength of a material becomes limited by creep rather than by its elastic limit. The majority of information provided is applicable to metallic materials, and only general information regarding creep-related failures of polymeric materials is given. The article also reviews various factors related to creep behavior and associated failures of materials used in high-temperature applications. The complex effects of creep-fatigue interaction, microstructural changes during classical creep, and nondestructive creep damage assessment of metallic materials are also discussed. The article describes the fracture characteristics of stress rupture. Information on various metallurgical instabilities is also provided. The article presents a description of thermal-fatigue cracks, as distinguished from creep-rupture cracks.
Book Chapter
Oxidation Cracking and Residual Creep Life of an Incoloy 800H Bottom Manifold in a Steam Reformer at 800 °C
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001738
EISBN: 978-1-62708-220-4
... showed that the cracking could not be caused by creep. It was found that the cracking was confined to a 4-mm deep coarse-grained zone (ASTM 0-1) at the outer diameter. The cracking appeared to be caused by strain-induced intergranular oxidation. When the cracks reached the fine-grained material...
Abstract
During a planned shut-down in 1990 it appeared that the bottom manifold parts made of wrought Incoloy 800H had undergone diametrical expansion of up to 2% due to creep. Further, cracking at the outer diam was found. It was decided to replace these parts. Microscopical investigations showed that the cracking could not be caused by creep. It was found that the cracking was confined to a 4-mm deep coarse-grained zone (ASTM 0-1) at the outer diameter. The cracking appeared to be caused by strain-induced intergranular oxidation. When the cracks reached the fine-grained material, the oxidation-cracks stopped. To determine the residual creep life of the sound (non-cracked) bottom manifold material, iso-stress creep tests were performed. It was found that tertiary creep started at 7% strain. The time-to-rupture was greater than 100,000 h. It was concluded that the bottom manifold (and thus the furnace) could be used safely during the foreseen production period.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001341
EISBN: 978-1-62708-215-0
... temperature, replacing the Schedule 40 100 deg bends with Schedule 80 pipe, and solution annealing the pipe after bending. Boiler tubes Brittle fracture Contaminants Creep (materials) Ductility Intergranular fracture Lead (metal), Impurities Mechanical properties SB407 Incoloy 800H UNS N08810...
Abstract
An SB407 alloy 800H tube failed at a 100 deg bend shortly after startup of a new steam superheater. Three bends failed and one bend remote from the failure area was examined. Visual examination showed that the fracture started on the outside surface along the inside radius of the bend and propagated in a brittle, intergranular fashion. Chemical analysis revealed that lead contamination was a significant factor in the failure and phosphorus may have contributed. The localized nature of the cracks and minimum secondary cracking suggested a distinct, synergistic effect of applied tensile stress with the contamination. Stress analysis found that stress alone was not enough to cause failure; however the operating stresses in the 100 deg bends were higher than at most other locations in the superheater Reduced creep ductility may be another possible cause of failure. Remedial actions included reducing the tube temperature, replacing the Schedule 40 100 deg bends with Schedule 80 pipe, and solution annealing the pipe after bending.
Book Chapter
Damage in a Gas Turbine Hot Gas Casing
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001737
EISBN: 978-1-62708-229-7
..., the material being AISI 321 stainless steel. The purpose of the present study was to determine optimum repair welding procedures on the premise that the material was basically sound and undamaged by creep. The cracking was the result of thermal fatigue, and such cracks can propagate at elevated temperature...
Abstract
The hot gas casing of a gas turbine used for peak load power production had developed extensive cracking during operation. The operating time was 18,000 h, and it had been subjected to 1,600 operating cycles. The gas temperature on the hot side was 985 deg C, on the cold side 204 deg C, the material being AISI 321 stainless steel. The purpose of the present study was to determine optimum repair welding procedures on the premise that the material was basically sound and undamaged by creep. The cracking was the result of thermal fatigue, and such cracks can propagate at elevated temperature, with damage ahead of the crack tip occurring by means of very local processes of creep. Metallographic examination disclosed heavy surface layers of carbides, such that the material was extremely brittle when subjected to bending. Accordingly, although it was demonstrated that the casing could be welded successfully, it was suggested that the remaining useful life was effectively exhausted and that it should be replaced. Thermal stresses produced during operation would rapidly result in additional cracks.
Book Chapter
Creep and Stress Rupture Failures
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003545
EISBN: 978-1-62708-180-1
... by the elastic limit for a given alloy. Creep deformation may produce sufficiently large changes in the dimensions of a component to either render it useless for further service or cause fracture. When excessive creep deformation causes the material to reach or exceed some design limit on strain, the term creep...
Abstract
This article reviews the applied aspects of creep and stress-rupture failures. It discusses the microstructural changes and bulk mechanical behavior of classical and nonclassical creep behavior. The article provides a description of microstructural changes and damage from creep deformation, including stress-rupture fractures. It also describes metallurgical instabilities, such as aging and carbide reactions, and evaluates the complex effects of creep-fatigue interaction. The article concludes with a discussion on thermal fatigue and creep fatigue failures.
Book Chapter
Failure Investigation of Longitudinal Seam Welded Elevated Temperature Header
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001669
EISBN: 978-1-62708-229-7
... initiation are: (1) operational transients leading to creep-fatigue interaction; or, (2) the expected redistribution of stress from the I.D. to the O.D. surface was interrupted due to differences in the material properties between subsurface weld beads, which were tempered by subsequent passes, and the final...
Abstract
As the result of a leak detected in a plate-formed header at PENELEC'S Shawville Unit No. 3, an extensive failure investigation was initiated to determine the origin of cracking visible along the longitudinal weld seam. Fabricated from SA387-D material and designed for a superheater outlet temperature of 566 deg C, the 11.4 cm thick header had operated for approximately 187,000 h at the time of the failure. Discussion focuses on the results of a metallographic examination of boat samples removed from the longitudinal seam weldment in the vicinity of the failure and at other areas of the header where peak temperatures were believed to have been reached. The long-term mechanical properties of the service-exposed base metal and creep-damaged weld metal were determined by creep testing. Based on the utility's decision to replace the header within one to three years, an isostress overtemperature lead specimen approach was taken, whereby failure of a test specimen in the laboratory would precede failures in the plant. These tests revealed approximately a 2:1 difference in life for the base metal as compared to weld metal.
Book Chapter
Creep, Stress Relaxation, and Yielding Mechanisms
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006934
EISBN: 978-1-62708-395-9
... Abstract This article describes the general aspects of creep, stress relaxation, and yielding for homogeneous polymers. It then presents creep failure mechanisms in polymers. The article discusses extrapolative methods for the prediction of long-term creep failure in polymer materials...
Abstract
This article describes the general aspects of creep, stress relaxation, and yielding for homogeneous polymers. It then presents creep failure mechanisms in polymers. The article discusses extrapolative methods for the prediction of long-term creep failure in polymer materials. Then, the widely used models to simulate the service life of polymers are highlighted. These include the Burgers power-law model, the Findley power-law model, the time-temperature superposition (or equivalence) principle (TTSP), and the time-stress superposition principle (TSSP). The Larson-Miller parametric method, one of the most common to describe the material deformation and rupture time, is also discussed.
Book Chapter
Structural Instability of Cold Worked Alloy 304 in 650 °C Service
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001581
EISBN: 978-1-62708-235-8
... of this alloy would provide more than a 1000-fold improvement in creep strength. Design and Material Requirements A typical catalyst profile screen wire design is shown in Fig. 1 . The Type 304 cold rolled profile wire had a thickness of 3.2 mm (0.125 in.) tapering to 0.8 mm (0.032 in.) at the trailing...
Abstract
A heavily worked 304 stainless steel wire basket recrystallized and distorted while in service at 650 deg C (1200 deg F). This case study demonstrates that heavily cold worked austenitic stainless steel components can experience large losses in creep strength, and potentially structural collapse, under elevated temperature service, even at temperatures more than 300 deg C (540 deg F) below the normal solution annealing temperature. The creep strength of the recrystallized 304/304L steel was more than 1000 times less than that achievable with solution annealed 304H. These observations are consistent with limitations (2000 Addendum to ASME Boiler and Pressure Vessel Code) on the use of cold worked austenitic stainless steels for elevated temperature service.
Book Chapter
Creep Rupture in a Superheated Steam Transfer Line
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001000
EISBN: 978-1-62708-229-7
.... Fig. 1 Schematic showing where failure occurred in superheated steam transfer line. Metallographic analysis of the material disclosed an advanced stage of creep damage accumulation in the form of local cracks, microcracks and aligned damage centers which show up as voids following upon...
Abstract
Rupture occurred at a bend in a superheated steam transfer line between a header and a desuperheater of a boiler producing 230 t/h of steam at 540 deg C and 118 kPa. The boiler had operated for 77,000 h. Rupture occurred along the outer bend radius of the 168 mm diam tube, this being of 1 Cr, 0.5 Mo steel with a wall thickness of 14 mm. The design temperature of this tube was 490 deg C, but there is evidence that it was operating at a temperature much above 500 deg C. Metallographic analysis disclosed an advanced stage of creep damage accumulation in the form of local cracks, microcracks, and aligned damage centers which showed up as voids upon repeated polish-etch cycles. Because of the local nature of creep damage that can occur, any inspection that involves in situ metallography must be conducted at exactly the right or critical position or the presence of damage may not be detected.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006941
EISBN: 978-1-62708-395-9
..., (σ 0 /η)t, on the nearly purely viscous fluid element, and Fig. 5(d) the resultant strain, D(t)*σ 0 , on the viscoelastic material. This generalized description of constant stress is the basis of typical creep testing, in which the compliance modulus function can be empirically measured by testing...
Abstract
This article describes the viscoelastic behavior of plastics in their solid state only, from the standpoint of the material deforming without fracturing. The consequences of viscoelasticity on the mechanical properties of plastics are described, especially in terms of time-dependencies, as well as the dependence of the viscoelastic character of a plastic on chemical, physical, and compositional variables. By examining the viscoelastic behavior of plastics, the information obtained are then applied in situations in which it may be important to anticipate the long-term properties of a material. This includes assessing the extent of stress decay in materials that are pre-stressed, the noise and vibration transmission characteristics of a material, the amount of heat build-up in a material subjected to cyclic deformation, and the extent a material can recover from any prior deformation. Several qualitative graphs are presented, which highlights the possible differences in the viscoelastic behavior that can exist among plastics.
Book Chapter
Failure Analysis of a Set of 1CrMoV Studs From a Steam Turbine and Techniques for Its Assessment
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001004
EISBN: 978-1-62708-229-7
... bearing thread. Crack extension was the result of marked creep embrittlement and reverse temper embrittlement (RTE). Selected approaches were examined to assess the effects of RTE on the material toughness of selected studs. It was observed that Auger electron microscopy results which indicated the extent...
Abstract
The results of a failure analysis of a series of Cr-Mo-V steel turbine studs which had experienced a service lifetime of some 50,000 h are described. It was observed that certain studs suffered complete fracture while others showed significant defects located at the first stress bearing thread. Crack extension was the result of marked creep embrittlement and reverse temper embrittlement (RTE). Selected approaches were examined to assess the effects of RTE on the material toughness of selected studs. It was observed that Auger electron microscopy results which indicated the extent of grain boundary phosphorus segregation exhibited a good relationship with ambient temperature Charpy data. The electrochemical polarization kinetic reactivation, EPR, approach, however, proved disappointing in that the overlapping scatter in the minimum current density, Ir, for an embrittled and a non-embrittled material was such that no clear decision of the toughness properties was possible by this approach. The initial results obtained from small punch testing showed good agreement with other reported data and could be related to the FATT. Indeed, this small punch test, combined with a miniature sample sampling method, represents an attractive approach to the toughness assessment of critical power plant components.
Book Chapter
Stress-Rupture Characterization in Nickel-Based Superalloy Gas Turbine Engine Components
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001758
EISBN: 978-1-62708-241-9
... to an EQ casting. (Photo courtesy Alcoa Howmet, Whitehall, Michigan.) [ 1 ] Creep Curve and Stress Rupture As mentioned, one of the most important variables for materials operating at high temperatures is their creep behavior. Creep describes the tendency of a material to accumulate plastic...
Abstract
This article describes the visual, fractographic, and metallographic evidence typically encountered when analyzing stress rupture of turbine airfoils. Stress-rupture fractures are generally heavily oxidized, tend to be rough in texture, and are primarily intergranular and/or interdendritic in appearance compared to smoother, transgranular fatigue type fractures. Often, gross plastic yielding is visible on a macroscopic scale. Commonly observed microstructural characteristics include creep voiding along grain boundaries and/or interdendritic regions. Internal voids can also nucleate at carbides and other microconstituents, especially in single crystal castings that do not possess grain boundaries.
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