Molded plastic couplings used in an industrial application exhibited abnormally brittle properties, as compared to previously produced components. The couplings were specified to be molded from a custom-compounded glass-filled nylon 6/12 resin. An inspection of the molding resin used to produce the discrepant parts revealed that the pellets were of two general types, neither of which matched the pellets from a retained resin lot. Investigation included visual inspection, micro-FTIR in the ATR mode, and analysis using DSC. The thermograms supported the conclusion that the brittle couplings contained a significant level of contamination, polypropylene and nylon 6/6. The source of the polypropylene was likely the purging compound used to clean the compounding extruder. The origin of the nylon 6/6 resin was unknown but may represent a previously compounded resin.

Failures of various types of hydraulic couplings used to connect pipes in a naval vessel are described and used to illustrate some of the general procedures for failure analysis. Cracking of couplings, which were manufactured from nickel-aluminum- bronze extruded bar, occurred in both seawater and air environments. Cracks initiated at an unusually wide variety of sites and propagated in either longitudinal or circumferential directions with respect to the axis of the couplings. Fracture surfaces were intergranular and exhibited little or no sign of corrosion (for couplings cracked in air), and there was very limited plasticity. Macroscopic progression markings were observed on fracture surfaces of several couplings but were not generally evident. At very high magnifications, numerous slip lines, progression markings, and striations were observed. In a few cases, where complete separation had occurred in service, small areas of dimpled overload fracture were observed. It was concluded from these observations, and from comparisons of cracks produced in service with cracks produced by laboratory testing under various conditions, that cracking had occurred by fatigue. The primary cause of failure was probably the unanticipated presence of high-frequency stress cycles with very low amplitudes, possibly due to vibration, resonance, or acoustic waves transmitted through the hydraulic fluid. Secondary causes of failure included the presence of high tensile residual stresses in one type of coupling, undue stress concentrations at some of the crack-initiation sites, and overtorquing of some couplings during installation. Recommendations on ways to prevent further failures based on these causes are discussed.

High-horsepower electric motors were utilized to drive large compressors (made of 4340 steel shafts and gear-type couplings) required in a manufacturing process. The load was transmitted by two keys 180 deg apart. Six of the eight compressor shafts were found cracked in a keyway and one of them fractured after a few months of operation. Visual examination of fractured shaft revealed that the cracks originated from one of the keyways and propagated circumferentially around the shaft. The shaft and coupling slippage was indicated by the upset keys and this type of fracture. The shaft surface both near and in the keyways indicated fretting which greatly reduced the fatigue limit of the shaft metal and initiated fatigue cracks. Fatigue marks were observed on the fractured key. Repetitive impact loading was responsible for propagation of the cracks. The high cyclic bending stresses were caused by misalignment between the electric motor and compressor and were transmitted to the shaft through the geared coupling. Flexible-disk couplings capable of transmitting the required horsepower were installed on the shafts as a corrective measure.

Several tin plated, low-alloy steel couplings designed to connect sections of 180 mm (7 in.) diam casing for application in a gas well fractured under normal operating conditions. The couplings were purchased to American Petroleum Institute (API) specifications for P-110 material. Chemical analysis and mechanical testing of the failed couplings showed that they had been manufactured to the API specification for Q-125, more stringent specification than P-110, and met all requirements of the application. Fractographic examination showed that the point of initiation was an embrittled region approximately 25 mm (1 in.) from the end of the coupling. The source of the embrittlement was determined to be hydrogen charging during tin plating. Changes in the plating process were recommended.

Brass pipe couplings submitted for examination were deep-drawn from disks then annealed and subsequently cold threaded. Chemical analysis confirmed that the specified alloy Ms 63 was used for fabrication. Some of the pipe already showed fine cracks prior to their installation. In most cases however the cracks were detected after a certain period of operation. The intercrystalline course of the cracks indicated stress-cracking as it often appears in brass after heavier cold deformation. The splitting of the couplings could have been avoided by a tempering heat treatment at temperatures between 230 and 300 deg C after rolling the threads. This procedure would have reduced the internal stresses while maintaining strengthening gained by the cold deformation.

Leakage was identified around a coupling welded into a stainless steel holding tank that stored condensate water with low impurity content. The tank and fitting were manufactured from type 304 stainless steel. The coupling joint consisted of an internal groove weld and an external fillet weld. Cracking was found to be apparent on the tank surface, adjacent to the coupling weld. Chlorine, carbon, and oxygen in addition to the base metal elements were revealed by energy-dispersive x-ray spectrometric analysis. A great number of secondary, branching cracks were evident in the weld, heat-affected zone, and base metal. The branching and transgranular cracking was found to emanate primarily from the exterior of the tank. It was concluded that the tank failed as a result of stress-corrosion cracking that initiated at the exterior surface as aqueous chlorides, especially within an acidic environment, have been shown to cause SCC in austenitic stainless steels under tensile stress.

The damage to a screw on the head of a 1.8 liter personal car engine was nucleated as the result of common disadvantageous environmental influences and reversed loads leading to corrosion fatigue.

A 25 mm (1 in.) copper coupling had been uniformly degraded around most of the circumference of the bell and partially on the spigot end. One penetration finally occurred through the thinned area on the spigot end of the pipe. Investigation supported the conclusion that although the pipe was buried in noncorrosive sandy soil, it was found to incur stray currents at 2 Vdc in relation to a Cu/CuSO4 half cell. Recommendations included eliminating, moving, or shielding the source of stray current.

An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.

During a routine start-up exercise of a standby service water pump, a threaded coupling that joined sections of a 41.5 ft (12.7 m) long pump shaft experienced fracture. The pump was taken out of service and examined to determine the cause of fracture. It was apparent early in the examination that the fracture involved hydrogen stress cracking. However, the nature of the corrosive attack suggested an interaction between the threaded coupling and biological organisms living in the freshwater environment of the pump shaft. The organisms had colonized on the coupling, changing the local environment and creating conditions favorable to hydrogen stress cracking. This paper describes the analysis of the fracture of the coupling and provides an example of how biologically induced corrosion can result in unexpected fracture of a relatively basic machine part.

A coupling in a line-shaft vertical turbine pump installed in a dam foundation fractured after a very short time. The coupling material was ASTM A582 416 martensitic stainless steel. Visual, macrofractographic, and scanning electron microscopic examination of the coupling showed that the fracture was brittle and was initiated by an intergranular cracking mechanism. The mode of fracture outside the crack initiation zone was transgranular cleavage. No indication of fatigue was found. The failure was attributed to improper heat treatment during manufacture, which resulted in a brittle microstructure susceptible to corrosion. The crack initiated either by stress-corrosion or hydrogen cracking. It was recommended that the couplings in the system be examined for surface cracking and, if present, corrective measures be taken.

A trunnion bolt that was part of a coupling in a metropolitan railway system failed in service, causing cars to separate. The bolt had been in service for more than ten years prior to failure. Visual examination showed that the failure resulted from complete fracture at the grease port and surface groove located at midspan. Drillings machined from the bolt underwent chemical analysis, which confirmed that the material was AISI 1045 carbon steel, in accordance with specifications. Two sections cut from the bolt were subjected to metallographic examination and hardness testing. The fracture origin was typical of fatigue. The ultimate tensile strength of the bolt was in excess of requirements. Wear patterns indicated that the bolt had been frozen in position for a protracted period and subjected to repeated bending stresses, which resulted in fatigue cracking and final complete fracture. It was recommended that proper lubrication procedures be maintained to allow free rotation of the bolts while in service.

Six ASTM A-574 steel cap screws from a hydraulic coupling failed after 3 months in service. The screws were replacements for smaller-diameter cap screws that had been installed during an outage. Six new cap screws were examined along with the failed screws. Eight fracture locations were identified—three at the head-to-shank fillet, four at the eighth thread root from the cap, and one at the sixth thread root from the cap. Fracture surfaces were examined using a stereomicroscope and SEM, and the fracture mode was shown to be transgranular. EDS on the fracture surfaces showed sulfur and chlorine in the surface deposits. The observations indicated that the screws had failed by fatigue. Insufficient preloading was considered to be the most likely cause of the fatigue cracking. It was recommended that the proper preload on the screws be verified and maintained.