During construction of a revolving sky-tower observatory, a 2.4 m (8 ft) diam cylindrical column developed serious circumferential cracks overnight at the 14 m (46 ft) level where two 12 m (40 ft) sections were joined by a girth weld. The temperatures ranged from 12 deg C (53 deg F) to 7 deg C (45 deg F) that night. The column was shop fabricated in 12 m (40 ft) long sections of 19 mm (3/4 in.) thick steel plate of ASTM A36 steel. Crack initiation was caused by high residual stress during girth welding, and the presence of notches formed by the termination of the incomplete welds. Continuation of the cracks was attributed to the brittle condition of the steel when cooled by the night air. A steel with a much lower ductile-to-brittle transition temperature is essential for this type of structure. Other necessary steps include better control of the girth-welding, choice of a more favorable electrode to avoid porosity, careful termination of all welds to avoid formation of notches, and completion of all welds before other sections of the column are erected.

A portion of the roof of a single story building collapsed during a thunder storm. A failure analysis was conducted to determine whether this structural failure was due to improper design, substandard construction materials, faulty erection, or extreme weather conditions. The failure analysis consisted of an onsite inspection, macrofractographic examination of the fractures where the girders were welded to the columns, macrofractographic examination of the fractured trusses, metallographic examination of the girder and truss materials, chemical analysis of the low-carbon steel girder and truss materials, and mechanical testing of the truss material. It was concluded that substandard structural components in combination with faulty construction was responsible for this service failure.

A portion of a 19 mm (0.75 in.) diam structural steel bolt was found on the floor of a manufacturing shop. This shop contained an overhead crane system that ran on rails supported by girders and columns. Inspection of the crane system revealed that the bolt had come from a joint in the supporting girders and could be considered one of the principal fasteners in the track system. Analysis (visual inspection, metallographic exam, and hardness testing) supported the conclusions that fatigue induced by the overhead movement of the crane produced failure of the bolt. The bolt was deficient in strength for the cyclic applied loads in this case and probably was not tightened sufficiently. Recommendations included removing the remaining bolts in the crane support assembly and replacing them with a higher-strength, more fatigue-resistant bolt, for example, SAE grade F, 104 to 108 HRB. The bolts should be tightened according to the specifications of the manufacturer, and the system should be periodically inspected for correct tightness.

Crane collapse due to bolt fatigue and fatigue failure of a crane support column, crane tower, overhead yard crane, hoist rope, and overhead crane drive shaft are described. The first four examples relate to the structural integrity of cranes. However, equipment such as drive and hoist-train components are often subject to severe fatigue loading and are perhaps even more prone to fatigue failure. In all instances, the presence of fatigue cracks at least contributed to the failure. In most instances, fatigue was the sole cause. Further, in each case, with regular inspection, fatigue cracks probably would have been detected well before final failure.

Field metallography and replication were performed on a type 316 stainless steel column in diglycol amine vacuum service to determine the cause of visible OD pitting on the column in several areas above the insulation support rings. The examination revealed transgranular stress-corrosion cracking beneath the pitted areas on the OD. The likely cause of the cracking was chloride stress corrosion, with chlorides deriving from the marine atmosphere and concentrating under the insulation around the support rings. A complete insulation evaluation, including repair or replacement, was recommended to prevent chloride buildup. Painting of the steel surface with an epoxy-phenolic or epoxy-coal tar was also suggested.

An evaluation of indications in the main turbine building column horizontal plate welds was conducted by the joint efforts of field metallography and nondestructive examinations. The turbine building main column horizontal plate welds were selected at random and were inspected to find discontinuities, metallurgical evaluation of the discontinuities, analysis of any failure modes, and determination of the best repair techniques. The welds were made with prequalified joints in accordance with AWS D1.1-77 and required only visual inspection. More sensitive inspection methods were applied to the welds in order to better define the indications found with the visual inspections. Cracks were found in 17 field welds and in two test plate welds. The causes of the cracking are related to the weld design and installation procedure. Three field welds were rejected because of the depth of the cracks. The NDT inspections, evaluations, method of field metallography, analysis and conclusions are discussed with recommendations for corrective actions in the following report.

One of the coils in the radiant section of a primary reformer furnace used in an ammonia plant was found leaking. The bottom of one of seven outlet headers (made of ASME SA-452, grade TP316H, stainless steel) was revealed during examination to be ruptured. It was revealed by metallurgical examination that it had failed as a result of intergranular fissuring and oxidation (creep rupture). The ruptured area revealed that the header had failed by conventional long-time creep rupture as a result of exposure to operating temperatures probably between 900 and 955 deg C. Three samples from different sections (ruptured area, slightly bulged but nonruptured area and visually sound metal) were inspected. The presence of pinhead-size intergranular fissures throughout the cross sections of the latter two samples was observed. An ultrasonic attenuation method was employed to investigate the remaining headers. All headers were revealed by ultrasonic readings to be in an advanced stage of creep rupture and no areas were found to be fissured to a degree that they needed immediate replacement. As a conclusion, the furnace was deemed serviceable and it was established that in the absence of local hot spots, the headers would survive for a reasonable period of time.

The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical column, signal detection and display equipment, and vacuum system. It discusses the preparation of samples for observation using an SEM and describes the application of SEM in fractography. If the surface remains unaffected and undamaged by events subsequent to the actual failure, it is often a simple matter to determine the failure mode by the use of an SEM. In cases where the surface is altered after the initial failure, the case may not be so straightforward. The article presents typical examples that illustrate these points. Image dependence on the microscope type and operating parameters is also discussed.

Following the discovery numerous cracks at many of the welded seams of a mild steel CO2 absorber vessel, a sample for examination was removed from the worst affected area where repairs had been effected. A 12 in. long circumferential crack was visible. Specimens were taken to cover the several locations of cracking which, in all cases, were found to be similar and of the intergranular type filled with oxide or corrosion product. The association of the cracks with the weld seams indicated that contraction stresses from welding were primarily responsible. Failure of the absorber vessel was found to be due to stress corrosion. Although the active agent present was not positively identified, the aqueous solution of monoethanolamine was thought to be the most probable. The origin of the stresses was not elucidated but the association of the cracks with the welded seams indicated inherent residual stresses as being primarily responsible. Tests carried out tend to suggest that stress relief was not carried out. For the replacement plant, consideration of stress relieving or the use of an alternative material was advised.

The scanning electron microscope (SEM) is one of the most versatile instruments for investigating the microscopic features of most solid materials. The SEM provides the user with an unparalleled ability to observe and quantify the surface of a sample. This article discusses the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described, and the application of SEM in fractography is discussed. The article covers the failure mechanisms of ductile failure, brittle failure, mixed-mode failure, and fatigue failure. Lastly, image dependence on microscope type and operating parameters is also discussed.

The Rocky Point Viaduct, located near Port Orford, OR, was replaced after only 40 years of service. A beam from the original viaduct was studied in detail to determine the mechanisms contributing to severe corrosion damage to the structure. Results are presented from the delamination survey, potential and corrosion mapping, concrete chemistry, and concrete physical properties. The major cause of corrosion damage appears to have been the presence of both pre-existing and environmentally-delivered chlorides in the concrete.

This article addresses some established protocols for characterizing thermoplastics and whether they are homogeneous resins, alloyed, or blended compositions or highly modified thermoplastic composites. It begins with a discussion on characterizing mechanical, rheological, and thermal properties of polymer. This is followed by a section describing molecular weight determination using viscosity measurements. Next, the article discusses the use of cone and plate and parallel plate geometries in melt rheology. It then reviews the processes involved in the analysis of thermoplastic resins by chromatography. Finally, the article covers three operations of thermoanalysis, namely differential scanning calorimetry, thermogravimetric analysis, and thermomechanical testing.

Distortion failure occurs when a structure or component is deformed so that it can no longer support the load it was intended to carry. Every structure has a load limit beyond which it is considered unsafe or unreliable. Estimation of load limits is an important aspect of design and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action. The article summarizes the general process of distortion failure analysis. It also discusses three types of distortion failures that provide useful insights into the problems of analyzing unusual mechanisms of distortion. These include elastic distortion, ratcheting, and inelastic cyclic buckling.

Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated with a functional failure. Then, a more general consideration of distortion in failure analysis is introduced. Several common aspects of failure by distortion are discussed and suitable examples of distortion failures are presented for illustration. The article provides information on methods to compute load limits, errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure.

Optimized modeling of fracture-critical structural components and connections requires the application of elastic-plastic fracture mechanics. Such applications, however, can require sophisticated analytical techniques such as crack tip opening displacement (CTOD), failure assessment diagram (FAD), and deformation plasticity failure assessment diagram (DPFAD). This article presents the origin and description of FAD and addresses R6 FAD using J-integral. It details the fracture criteria of BS 7910. The factors to be considered during the use of FAD and the applications of FAD are also reviewed.

This article presents tools, techniques, and procedures that engineers and material scientists can use to investigate plastic part failures. It also provides a brief survey of polymer systems and the key properties that need to be measured during failure analysis. It describes the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy, differential scanning calorimetry, differential thermal analysis, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses the use of X-ray diffraction for analyzing crystal phases and structures in solid materials.

This article illustrates the defects, which result because of poor-quality welds in the bridge components. The cracks resulting from the use of low fatigue strength details are also discussed. The article describes the effect of out-of-plane distortion in floor-beam-girder connection plates, multiple-girder diaphragm connection plate, and tied-arch floor beams.

This article addresses the effects of damage to equipment and structures due to explosions (blast), fire, and heat as well as the methodologies that are used by investigating teams to assess the damage and remaining life of the equipment. It discusses the steps involved in preliminary data collection and preparation. Before discussing the identification, evaluation, and use of explosion damage indicators, the article describes some of the more common events that are considered in incident investigations. The range of scenarios that can occur during explosions and the characteristics of each are also covered. In addition, the article primarily discusses level 1 and level 2 of fire and heat damage assessment and provides information on level 3 assessment.

This article discusses the operating principles, advantages, and limitations of scanning electron microscopy, atomic force microscopy, x-ray photoelectron spectroscopy, and secondary ion mass spectroscopy that are used to analyze the surface chemistry of plastics.

This article provides an overview of the structural design process and discusses the life-limiting factors, including material defects, fabrication practices, and stress. It details the role of a failure investigator in performing nondestructive inspection. The article provides information on fatigue life assessment, elevated-temperature life assessment, and fitness-for-service life assessment.