Six ASTM A-574 steel cap screws from a hydraulic coupling failed after 3 months in service. The screws were replacements for smaller-diameter cap screws that had been installed during an outage. Six new cap screws were examined along with the failed screws. Eight fracture locations were identified—three at the head-to-shank fillet, four at the eighth thread root from the cap, and one at the sixth thread root from the cap. Fracture surfaces were examined using a stereomicroscope and SEM, and the fracture mode was shown to be transgranular. EDS on the fracture surfaces showed sulfur and chlorine in the surface deposits. The observations indicated that the screws had failed by fatigue. Insufficient preloading was considered to be the most likely cause of the fatigue cracking. It was recommended that the proper preload on the screws be verified and maintained.

Uncoated high-strength alloy steel cap screws retaining a cast aluminum (356.0) diffuser assembly in a centrifugal refrigerant compressor failed in a brittle manner a short time after the system was placed in operation. Evidence obtained during the failure analysis indicated that the failures were the result of hydrogen embrittlement produced by galvanic corrosion and attendant evolution of hydrogen at the dissimilar junction, which was also the site of the highest tensile stress. Suggested measures for minimizing recurrences included use of lower-strength, galvanically-compatible fasteners and appropriately-applied and treated compatible coatings.

Several cadmium-plated carbon steel socket head cap screws that were part of a slide valve assembly on a regenerator line in a petrochemical plant failed during initial loading. Metallographic and XDS chemical analysis in conjunction with SEM examination of one failed and one unfailed cap screw indicated that the screws had failed by hydrogen embrittlement. The plating process was the likely source of the hydrogen. It was recommended that the remainder of the cap screws from the same lot as the failed screws be baked at approximately 190 deg C (375 deg F) for 24 h.

A drive-line assembly failed during vehicle testing. The vehicle had traveled 9022 km (5606 mi) before the failure occurred. Both the intact and fractured parts of the assembly were analyzed to determine the cause and sequence of failure. Visual examination of the assembly showed three of four bearing caps, two cap screws, and one universal-joint spider had fractured. Examination of the three fractured bearing caps and the spider showed no evidence of fatigue but showed that fracture occurred in a brittle manner. The bearing cap that was not destroyed still contained portions of the two fractured cap screws. It was found that the two cap screws failed in fatigue under service stresses. The three bearing caps and the universal-joint spider broke in a brittle manner. The properties of the material in the cap screws did not fulfill the specifications. The modified 1035 steel was of insufficient alloy content. Also, the tensile strength and endurance limit were lower than specified and were inadequate for the application. The material for the cap screw was changed from modified 1035 steel to 5140 steel.

Socket head cap screws used in a naval application were failing in service due to delayed fracture. The standard ASTM A 574 screws were zinc plated and dichromate coated. Investigation (visual inspection, 1187 SEM images, chemical analysis, and tension testing) of both the failed screws and two unused, exemplar fasteners from the same lot supported the conclusion that the cap screws appear to have failed due to hydrogen embrittlement, as revealed by delayed cracking and intergranular fracture morphology. Static brittle overload fracture occurred due to the tension preload, and prior hydrogen charging that occurred during manufacturing. The probable source of charging was the electroplating, although postplating baking was reportedly performed as well. Recommendations included examining the manufacturing process in detail.

A 20 ton polar crane motor fell during a 3400 kg (7500 lb) lift, narrowly missing personnel working beneath the crane. Witnesses reported that the motor fall was preceded by a falling oil mass, and it was believed that the motor was intact prior to impact. The maintenance history of the crane showed that the motor had been removed, repaired, and reinstalled 2 years prior to the failure. Observations of oil leakage were noted yearly up to the failure. The motor casing was held onto the adapter plate by eight 14-20 UNC x 25 mm (1 in.) long hex socket cap screws. Examination of the motor adapter plate, motor casing shards (aluminum), the gear side of the motor housing, and seven fractured cap screws (ASTM A574) showed that the motor casing was intact at the time of “uncontrolled descent” and that the screws had failed by high nominal stress reverse bending load fatigue, which was probably the result of insufficient torque on the bolts.

A failed tapered-ring sprocket locking device consisted of an assembly of four tapered rings that are retained by a series of cap screws. The middle wedge-shaped rings were pulled closer as the screws were tightened forcing the split inner ring to clamp tightly onto the shaft. One of the wedge-shaped middle rings fractured prior to having been fully torqued, preventing the sprocket from being locked to the shaft. “Woody” fracture features, as a result of decohesion between a high volume fractions of manganese sulfide stringers and the matrix, was revealed during examination. The material was revealed by chemical analysis to be resulfurized grade of carbon steel (SAE type 1144, UNS G11440) which has enhanced longitudinal tensile properties but low transverse properties. It was observed that when the fastening screws were torqued, a significant hoop stress was placed on the middle rings and it caused the failure at the large inclusion present at the minimum section thickness zone of the middle ring. It was concluded that since the material contained a high volume fraction of these inclusions, the material choice was not appropriate for this application. A nonresulfurized grade of low-alloy steel was suggested as recommendation.