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K.V. Kasiviswanathan, N.G. Muralidharan, Baldev Raj
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Daryl C. Collins
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Friedrich Karl Naumann, Ferdinand Spies
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W.J.D. Shaw
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S.S. Akhtar, A.F.M. Ari
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Friedrich Karl Naumann, Ferdinand Spies
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Friedrich Karl Naumann, Ferdinand Spies
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(a) AISI 420 stainless steel mold containing a defect (arrow) observed afte...
Available to PurchasePublished: 01 January 2002
Fig. 28 (a) AISI 420 stainless steel mold containing a defect (arrow) observed after polishing the inside diameter surface. (b) Microscopic examination revealed a large silicate inclusion (unetched).
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Image
(a) AISI 420 stainless steel mold containing a discontinuity (arrow) observ...
Available to PurchasePublished: 15 January 2021
Fig. 22 (a) AISI 420 stainless steel mold containing a discontinuity (arrow) observed after polishing the inside-diameter surface. (b) Microscopic examination revealed a large silicate inclusion (unetched).
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Book Chapter
Failure of a Yoke Body of Master Slave Manipulator Due to Casting Defect
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001074
EISBN: 978-1-62708-214-3
... Abstract A cast housing, part of a multi-shaft yoking mechanism, failed during assembly and installation of the equipment in which it was to be used. The housing, or yoke body, was cast from AISI 420 grade ferritic stainless steel. Analysis revealed that the failure was caused by the presence...
Abstract
A cast housing, part of a multi-shaft yoking mechanism, failed during assembly and installation of the equipment in which it was to be used. The housing, or yoke body, was cast from AISI 420 grade ferritic stainless steel. Analysis revealed that the failure was caused by the presence of shrinkage cavities, which lowered the load-bearing capability. The failure occurred at the location where there was an abrupt change in the section thickness. A redesign to provide a smooth contour at the section junction was recommended along with optimization of casting parameters to avoid shrinkage cavities.
Book Chapter
Corrosion Fatigue Failure of Stainless Steel Load Cells in a Milk Storage Tank
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001386
EISBN: 978-1-62708-215-0
... Abstract Two type 420 martensitic stainless steel load cell bodies, which had been installed under two of the four legs of a milk storage tank failed in service. The failure occurred near a change in section and involved fracture of the entire cross section. Examination showed a brittle...
Abstract
Two type 420 martensitic stainless steel load cell bodies, which had been installed under two of the four legs of a milk storage tank failed in service. The failure occurred near a change in section and involved fracture of the entire cross section. Examination showed a brittle fracture that was preceded by a small fatigue region. Pitting corrosion was evident at the fracture origin. The areas around the load cells had been subjected to regular washdowns using high-pressure hot water, and the pitting was attributed to crevice corrosion between the load cell and the holddown bolts. Prevention of such corrosion by the use of a flexible sealant to eliminate the crevice was recommended.
Book Chapter
Broken Rim of a Rolling Mill Transmission
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001231
EISBN: 978-1-62708-232-7
... Abstract The rim of a gear wheel of 420 mm width and 3100 mm in diam broke after four years of operation time in a sheet bar three-high rolling mill. The rim was forged from steel with about 0.4C, 0.8Si and 1.1Mn. The rim started to break in the tooth bottom from a fatigue fracture which...
Abstract
The rim of a gear wheel of 420 mm width and 3100 mm in diam broke after four years of operation time in a sheet bar three-high rolling mill. The rim was forged from steel with about 0.4C, 0.8Si and 1.1Mn. The rim started to break in the tooth bottom from a fatigue fracture which extended from the gear side to more than half the rim width. A second incipient failure commenced from the opposite tooth bottom. Both fractures joined below the tooth of the rim. Both incipient cracks were fatigue fractures with several starting points, all located in the transition between tooth flank and tooth bottom. The remaining failure was a fine-grained ductile fracture. It was found that the teeth were not supported uniformly over the entire width and were thus overloaded on one side. The transition from the tooth flanks to the tooth bottom was sharp-edged, causing a tension peak there. The tooth bottom was machined only roughly. Also, the yield point was a little bit too low.
Book Chapter
Combined EDX/AES Analysis of Failed Inconel 600 Steam Line Bellows
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.pulp.c0045911
EISBN: 978-1-62708-230-3
... Abstract Within the first few months of operation of an 8 km (5 mile) long 455 mm (18 in.) diam high-pressure steam line between a coal-fired electricity-generating plant and a paper mill, several of the Inconel 600 bellows failed. The steam line operated at 6030 kPa (875 psi) and 420 deg C...
Abstract
Within the first few months of operation of an 8 km (5 mile) long 455 mm (18 in.) diam high-pressure steam line between a coal-fired electricity-generating plant and a paper mill, several of the Inconel 600 bellows failed. The steam line operated at 6030 kPa (875 psi) and 420 deg C (790 deg F). Metallographic sections, energy-dispersive x-ray spectra, chemical analyses, tensile tests, and Auger microscope analyses showed the failed bellows met the specifications for the material. However, investigation also showed entire oxide thickness was contaminated with relatively large amounts of sodium, calcium, potassium, aluminum, and sulfur, alkali, alkali earth, and other contaminants that completely permeated even the thin oxides on the fracture surfaces. Additional investigation of the purity of the steam itself as reported by the power plant showed that corrosion and cracks were ultimately caused by the steam. While under normal operation, the steam's purity posed no problem to the material, during boiler cleaning operations, the generating plant had allowed contamination to get into the steam line.
Book Chapter
Failure Analysis of a Spoon Broken by a Parapsychic Person
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c9001677
EISBN: 978-1-62708-222-8
... that should be applied when analyzing failures of unknown origin. Fractography Spoons Tableware 420 UNS S42000 Fatigue fracture A good deal of speculation and controversy surrounds the area of paranormal effects on metals. This area caught the public's attention with the emergence of Uri...
Abstract
A spoon that was twisted and broken by a person claiming to possess parapsychic powers was submitted for failure analysis. Exemplar tests were conducted on material taken from the bowl region of the same spoon. In addition, tests on other unbroken samples of spoons were evaluated in order to establish both macroscopic and microscopic comparative behavior. These controlled tests produced known failure mechanisms and their respective fracture morphology in this material. A direct comparison could then be made with the unknown failure. The paper identifies a method of analysis that should be applied when analyzing failures of unknown origin.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001805
EISBN: 978-1-62708-241-9
... delamination brittle cleavage SEM/EDS analysis tensile yield strength 420 (martensitic stainless steel) UNS S42000 AMS 2404E (electroless nickel plating) Background Surgical tools are defined as any device or instrument used during a surgical procedure. These tools range from simple knives...
Abstract
Several surgical tool failures were analyzed to understand why they occur and how to prevent them. The study included drills, catheters, and needles subjected to the rigors of biomedical applications such as corrosive environments, high stresses, sterilization, and improper cleaning procedures. Given the extreme conditions to which surgical tools can be exposed, and the potential for misuse, failures are inevitable and systematic methods for analyzing them are necessary to keep them in check.
Image
Precipitates on lattice planes and twin planes of former austenite. Etch: P...
Available to Purchase
in Steel Casting with Insufficient Strength Properties
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Fig. 6 Precipitates on lattice planes and twin planes of former austenite. Etch: Picral. approx. 420 ×
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Image
Metallographic image of a typical cable stop. This martensitic microstructu...
Available to PurchasePublished: 01 December 2019
Fig. 18 Metallographic image of a typical cable stop. This martensitic microstructure is consistent with type 420 stainless steel (approximately ×1000)
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Image
Corrosion pitting and cracking appeared under the green (G) epoxy primer an...
Available to Purchase
in Hydrogen Embrittlement of Aircraft Components
> ASM Failure Analysis Case Histories: Air and Spacecraft
Published: 01 June 2019
Fig. 3 Corrosion pitting and cracking appeared under the green (G) epoxy primer and gray paint (P) near the start of fracture of Fig. 2 . Magnification 420 times.
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Image
Variation of maximum von Mises stress ( a ) and maximum principal strain ( ...
Available to Purchase
in Fatigue Failure of Extrusion Dies: Effect of Process Parameters and Design Features on Die Life
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 6 Variation of maximum von Mises stress ( a ) and maximum principal strain ( b ) until steady state is reached. The corresponding maximum value distributions at critical die location are also shown. The simulation conditions and die configuration are temperature = 420 °C, strain rate = 1
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Image
Microstructure and fracture appearance of type 316L stainless steel tested ...
Available to PurchasePublished: 15 January 2021
. The scanning electron fractograph (b) shows the fracture appearance characterized by poorly-formed shear dimples and particle dragging. (a) Electrolytically etched with oxalic acid. Original magnification: 84×. (b) Original magnification: 420×. Courtesy of W.E. White, Petro-Canada Ltd.
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Image
Plastic mold die made from AISI S7 tool steel that was found to be cracked ...
Available to PurchasePublished: 01 January 2002
). Etched with 3% nital. 420×
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Image
Plastic-mold die made from AISI S7 tool steel that was found to be cracked ...
Available to PurchasePublished: 30 August 2021
retained austenite and coarse plate martensite). Etched with 3% nital. Original magnification: 420×
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Book Chapter
Fatigue Failure of Extrusion Dies: Effect of Process Parameters and Design Features on Die Life
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001788
EISBN: 978-1-62708-241-9
... cases for each parameter are considered. The details are shown in Table 1 . For the effect of temperature, flow curves of billet material at three temperatures, 300, 420, and 540 °C, are used as simulation inputs. These flow curves are considered at average strain rate of 1 s –1 . Bearing land of 8 mm...
Abstract
Several failed dies were analyzed and the results were used to evaluate fatigue damage models that have been developed to predict die life and aid in design and process optimization. The dies used in the investigation were made of H13 steels and fractured during the hot extrusion of Al-6063 billet material. They were examined to identify critical fatigue failure locations, determine corresponding stresses and strains, and uncover correlations with process parameters, design features, and life cycle data. The fatigue damage models are based on Morrow’s stress and strain-life models for flat extrusion die and account for bearing length, fillet radius, temperature, and strain rate. They were shown to provide useful information for the analysis and prevention of die failures.
Book Chapter
Failure of Polyethylene Terephthalate Assemblies
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0090451
EISBN: 978-1-62708-218-1
.... This transition, at 215 °C (420 °F), suggested the melting of annealed crystals, indicating that the part had been exposed to a temperature approaching 215 °C (420 °F). The thermal shock testing appeared to be the only possible source of this thermal exposure. Analysis of the molding resin also produced...
Abstract
Cracking occurred within the plastic jacket (injection molded from an impact-modified, 15% glass-fiber-reinforced PET resin.) of several assemblies used in a transportation application during an engineering testing regimen which involved cyclic thermal shock (exposing the parts to alternating temperatures of -40 and 180 deg C (-40 and 360 deg F)). Prior to molding, the resin had reportedly been dried at 135 deg C (275 deg F). The drying process usually lasted 6 h, but occasionally, the material was dried overnight. Comparison investigation (visual inspection, 20x SEM views, micro-FTIR, and analysis using DSC and TGA) with non-failed parts supported the conclusion that that the failure was via brittle fracture associated with the exertion of stresses that exceeded the strength of the resin as-molded caused by the disparity in the CTEs of the PET jacket and the mating steel sleeve. The drying process had exposed the resin to relatively high temperatures, which caused substantial molecular degradation, thus limiting the part's ability to withstand the stresses. The drying temperature was found to be significantly higher than the recommendation for the PET resin, and the testing itself exposed the parts to temperatures above the recognized limits for PET.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001746
EISBN: 978-1-62708-217-4
... out radiating river markings. Magnification 6.3 times. Fig. 3 Corrosion pitting and cracking appeared under the green (G) epoxy primer and gray paint (P) near the start of fracture of Fig. 2 . Magnification 420 times. Fig. 4 illustrates eyebolts which broke when used to lift...
Abstract
Brittle intergranular fracture, typical of a hydrogen-induced delayed failure, caused the failure of an AISI 4340 Cr-Mo-Ni landing gear beam. Corrosion resulting from protective coating damage released nascent hydrogen, which diffused into the steel under the influence of sustained tensile stresses. A second factor was a cluster of non-metallic inclusions which had ‘tributary’ cracks starting from them. Also, eyebolts broke when used to lift a light aircraft (about 7000 lb.). The bolt failure was a brittle intergranular fracture, very likely due to a hydrogen-induced delayed failure mechanism. As for the factors involved, cadmium plating, acid pickling, and steelmaking processes introduce hydrogen on part surfaces. As a second contributing factor, both bolts were 10 Rc points higher in hardness than specified (25 Rc), lessening ductility and notch toughness. A third factor was inadequate procedure, which resulted in bending moments being applied to the bolt threads.
Book Chapter
Oxidized Recuperator Pipes
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001233
EISBN: 978-1-62708-232-7
... channel on entering Group 1 of the recuperator was 1150 to 1200°C, falling in Group 1 to 1125°C, in Group 2 to 1050 to 1000°C and in Group 3 to 860 to 840°C. The air was heated to 420 to 450°C in Group 3, to 580 to 640°C in Group 1 and to 750 to 820°C in Group 2. Theoretically the maximum wall temperature...
Abstract
High-chromium steel pipes 42.25 x 3.25 mm from a blast furnace gas fired recuperator for the preheating of air were heavily oxidized and perforated in places. It was found that the blast furnace gas had a high sulfur content. Both the carburization and the formation of sulfide proved that in addition, from time to time at least, combustion was incomplete and the operation was carried out in a reducing atmosphere, with the result that oxygen deficiency prevented the formation or maintenance of a protective surface layer on the external surface of the pipes. The sulfur would probably not have damaged the nickel-free steel used here at the given temperatures if it had been present as sulfur dioxide in an oxidizing atmosphere. The damage was therefore caused primarily by an incorrectly conducted combustion process.
Book Chapter
Steel Casting with Insufficient Strength Properties
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001251
EISBN: 978-1-62708-235-8
.... Etch: Picral. approx. 420 × Fig. 7 Precipitates in grain boundaries and planes, unetched section of outer zone of flange disk. 1500 × Fig. 8 Precipitates in grain boundaries and planes, unetched section of outer zone of flange disk. 1500 × The optical examination...
Abstract
In a steel foundry, tensile and bend specimens of castings made in a 2-ton basic arc furnace showed, at irregular intervals, regions with coarse-grained fractures where the specimens broke prematurely, so that the specified strength and toughness values could not be reached. Several cast tensile specimens and some forcibly-broken pieces of the flanges of armature yokes made of cast steel GS C 25 according to DIN 17 245 were investigated. Microscopic examination showed that the cause of damage was the superabundant use of aluminum as deoxidizer. According to recommendations, the aluminum addition was reduced by one-half. Since then, there have been no additional rejects due to insufficient tensile and bend values.
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