Two tubular AISI 1025 steel posts (improved design) in a carrier vehicle failed by cracking at the radius of the flange after five weeks of service. The posts were two of four that supported the chassis of the vehicle high above the wheels. The original design involved a flat flange of low-carbon low-alloy steel that was welded to an AISI 1025 steel tube, and the improved design included placing the welded joint of the flange farther away from the flange fillet. Investigation (visual inspection and chemical analysis) supported the conclusion that the failures in the flanges of improved design were attributed to fatigue cracks initiating at the aluminum oxide inclusions in the flange fillet. Recommendations included retaining the improved design of the flange with the weld approximately 50 mm (2 in.) from the fillet, but changing the metal to a forging of AISI 4140 steel, oil quenched and tempered to a hardness of 241 to 285 HRB. Preheating to 370 deg C (700 deg F) before and during welding with AISI 4130 steel wire was specified. It was also recommended that the weld be subjected to magnetic-particle inspection and then stress relieved at 595 deg C (1100 deg F), followed by final machining.

A carbon-molybdenum (ASTM A209 Grade T1) steel superheater tube section in an 8.6 MPa (1250 psig) boiler cracked because of long-term overheating damage that resulted from prolonged exposure to metal temperatures between 482 deg C (900 deg F) and 551 deg C (1025 deg F). The outer diameter of the tube exhibited a crack (fissure) oriented approximately 45 deg to the longitudinal axis and 3.8 cm (1.5 in.) long. The inner diameter surface showed a fissure in the same location and orientation. Microstructure at the failure near the outer diameter surface exhibited evidence of creep cracking and creep void formation at the fissure. A nearly continuous band of graphite nodules was observed on the surface of the fissure. In addition to the graphite band formation, the microstructure near the failure exhibited carbide spheroidization from long-term overheating in all the tube regions examined. It was concluded that preferential nucleations of graphite nodules in a series of bands weakened the steel locally, producing preferred fracture paths. Formation of these graphite bands probably expedited the creep failure of the tube. Future failures may be avoided by using low-alloy steels with chromium additions such as ASTM A213 Grade T11 or T22, which are resistant to graphitization damage.

A valve stem made of 17-4 PH (AISI type 630) stainless steel, which was used for operating a gate valve in a steam power plant, failed after approximately four months of service, during which it had been exposed to high-purity water at approximately 175 deg C (350 deg F) and 11 MPa (1600 psi). The valve stem was reported to have been solution heat treated at 1040 +/-14 deg C (1900 +/-25 deg F) for 30 min and either air quenched or oil quenched to room temperature. The stem was then reportedly aged at 550 to 595 deg C (1025 to 1100 deg F) for four hours. Investigation (visual inspection, 0.7x/50x images, hardness testing, reheat treatment, and metallographic examination) supported the conclusion that failure was by progressive SCC that originated at a stress concentration. Also, the solution heat treatment had been either omitted or performed at too high of a temperature, and the aging treatment had been at too low of a temperature. Recommendations included the following heat treatments: after forging, solution heat treat at 1040 deg C (1900 deg F) for one hour, then oil quench; to avoid susceptibility to SCC, age at 595 deg C (1100 deg F) for four hours, then air cool.

Tube 3 from a utility boiler in service for 13 years under operating conditions of 540 deg C (1005 deg F), 13.7 MPa (1990 psi) and 1,189,320 kg/h (2,662,000 lb/h) incurred a longitudinal rupture near its 90 deg bend while Tube 4 from the same boiler exhibited deformation near its bend. Metallographic examination revealed creep voids near the rupture in addition to graphite nodules. Exposure of the SA209 Grade T1A steel tubing to a calculated mean operating temperature of 530 deg C (983 deg F) for the 13 years resulted in graphitization and subsequent creep failure in Tube 3. The deformation in Tube 4 was likely the result of steam washing from the Tube 3 failure. Graphitization observed remote from the rupture in Tube 3 and in Tube 4 indicated that adjacent tubing also was susceptible to creep failure. In-situ metallography identified other graphitized tubes to be replaced during a scheduled outage.

A rocket-motor case made of consumable-electrode vacuum arc remelted D-6ac alloy steel failed during hydrostatic proof-pressure testing. Close visual examination, magnetic-particle inspection, and hardness tests showed cracks that appeared to have occurred after austenitizing but before tempering. Microscopic examinations of ethereal picral etched sections indicated that the cracks appeared before or during the final tempering phase of the heat treatment and that cracking had occurred while the steel was in the as-quenched condition, before its 315 deg C (600 deg F) snap temper. Chemical analysis of the cracked metal showed a slightly higher level of carbon than in the component that did not crack. X-ray diffraction studies of material from the fractured dome showed a very low level of retained austenite, and chemical analysis showed a slightly higher content of carbon in the metal of the three cracked components. Bend tests verified the conclusion that the most likely mechanism of delayed quench cracking was isothermal transformation of retained austenite to martensite under the influence of residual quenching stresses. Recommendations included modifying the quenching portion of the heat-treating cycle and tempering in the salt pot used for quenching, immediately after quenching.

Pendant-style reheater, constructed of ASME SA-213, grade T-11, steel ruptured. A set of four tubes, specified to be 64 mm OD x 3.4 mm minimum wall thickness was examined. A small quantity of loose debris was removed from the inside of one of the tubes. The major constituent was revealed by EDS analysis of the debris to be iron with traces of phosphorus, manganese, sodium, calcium, copper, zinc, potassium, silicon, chromium, and molybdenum. Thus the debris was interpreted to be the scale from ID of the tube with boiler feedwater chemicals from the attemperation spray. The likely cause of failure was concluded to be exfoliation of the scale from the ID surface of the tube. Creep failures were interpreted to be caused by localized temperatures higher than the maximum service temperature. Replacement of the affected tubes was recommended. Inspection of the tubes by radiography to find the circuits with the greatest accumulation of debris and replacing them as necessary was recommended on an annual basis.

High-chromium steel pipes 42.25 x 3.25 mm from a blast furnace gas fired recuperator for the preheating of air were heavily oxidized and perforated in places. It was found that the blast furnace gas had a high sulfur content. Both the carburization and the formation of sulfide proved that in addition, from time to time at least, combustion was incomplete and the operation was carried out in a reducing atmosphere, with the result that oxygen deficiency prevented the formation or maintenance of a protective surface layer on the external surface of the pipes. The sulfur would probably not have damaged the nickel-free steel used here at the given temperatures if it had been present as sulfur dioxide in an oxidizing atmosphere. The damage was therefore caused primarily by an incorrectly conducted combustion process.

The accident at Three Mile Island Unit No. 2 on 28 March 1979 was the worst nuclear accident in US history. By Jan 1990, it was possible to electrochemically machine coupons from the lower head using a specially designed tool. The specimens contained the ER308L stainless steel cladding and the A533 Grade B plate material to a depth of about mid-wall. The microstructures of these specimens were compared to that of specimens cut from the Midland, Michigan reactor vessel, made from the same grade and thickness but never placed in service. These specimens were subjected to known thermal treatments between 800 and 1100 deg C for periods of 1 to 100 min. Microstructural parameters in the control specimens and in those from TMI-2 were quantified. Selective etchants were used to better discriminate desired microstructural features, particularly in the cladding. This report is a progress report on the quantification of changes in both the degree of carbide precipitation and delta ferrite content and shape in the cladding as a function of temperature and time to refine the estimates of the maximum temperatures experienced.

Six galvanized high-tensile steel bolts were used to hold the wheels of a four-wheel drive vehicle. The right hand rear wheel of this vehicle detached causing the vehicle to roll and resulting in considerable damage to the body. The wheel was detached by shearing of four of the bolts and stripping the nuts from the other two bolts, which remained unbroken. SEM fractography of the fracture surfaces of the four broken bolts indicated that the failure was due to reversed bending fatigue. Optical microscopy indicated that the bolts were heat treated to a tempered martensite structure and that the nuts were manufactured from low carbon steel. The paper discusses the influence of the microstructure on the failure process the events surrounding the nature of incident and the analysis of in-service failure of the failed components utilizing conventional metallurgical techniques.

When bulging occurred in mortar tubes made of British I steel during elevated-temperature test firing, a test program was formulated to evaluate the high-temperature properties (at 540 to 650 deg C, or 1000 to 1200 deg F) of the British I steel and of several alternative alloys including a maraging steel (18% Ni, grade 250), a vanadium-modified 4337 gun steel (4337V), H19 tool steel, and high-temperature alloys Rene 41, Inconel 718, and Udimet 630. All the alloys evaluated had been used in mortar tubes previously or were known to meet the estimated minimum yield strength. The alloys fall in this order of decreasing strengths: Udimet 630, Inconel 718, Rene 41, H19 tool steel, British I steel, 4337V gun steel, and maraging steel. When cycled between room temperature and 540 to 650 deg C (1000 to 1200 deg F), only Udimet 630, Inconel 718, and Rene 41 retained yield strengths higher than the minimum. Also, these three alloys maintained high strengths over the tested range, whereas the others decreased in yield strength as cycling progressed. Analysis showed Inconel 718 was considered best suited for 81-mm mortar tubes, and widespread industrial use ensured its availability.

The failures of two aircraft components, one from a landing gear and the other from an ejector rack mechanism, were investigated. Both were made from PH 13-8 Mo (UNS S13800) precipitation-hardening stainless steel which had been heat treated to the H1000 and H950 tempers respectively and then chromium plated. The parts were characterized metallographically and mechanically and were found to be compliant. Detailed fractographic examination revealed that the first stage of both failures was similar: subsurface initiation of numerous cracks with a wide range of orientations and cleavage like features. The cracking was followed by fatigue in one case and catastrophic failure in the other. Hydrogen embrittlement was identified as the most likely mechanism of failure.

This article commences with a discussion on the characteristics of stress-corrosion cracking (SCC) and describes crack initiation and propagation during SCC. It reviews the various mechanisms of SCC and addresses electrochemical and stress-sorption theories. The article explains the SCC, which occurs due to welding, metalworking process, and stress concentration, including options for investigation and corrective measures. It describes the sources of stresses in service and the effect of composition and metal structure on the susceptibility of SCC. The article provides information on specific ions and substances, service environments, and preservice environments responsible for SCC. It details the analysis of SCC failures, which include on-site examination, sampling, observation of fracture surface characteristics, macroscopic examination, microscopic examination, chemical analysis, metallographic analysis, and simulated-service tests. It provides case studies for the analysis of SCC service failures and their occurrence in steels, stainless steels, and commercial alloys of aluminum, copper, magnesium, and titanium.

This article explains the main types and characteristic causes of failures in boilers and other equipment in stationary and marine power plants that use steam as the working fluid with examples. It focuses on the distinctive features of each type that enable the failure analyst to determine the cause and suggest corrective action. The causes of failures include tube rupture, corrosion or scaling, fatigue, erosion, and stress-corrosion cracking. The article also describes the procedures for conducting a failure analysis.

This article focuses on the mechanisms and common causes of failure of metal components in lifting equipment in the following three categories: cranes and bridges, particularly those for outdoor and other low-temperature service; attachments used for direct lifting, such as hooks, chains, wire rope, slings, beams, bales, and trunnions; and built-in members such as shafts, gears, and drums.

Overload failures refer to the ductile or brittle fracture of a material when stresses exceed the load-bearing capacity of a material. This article reviews some mechanistic aspects of ductile and brittle crack propagation, including a discussion on mixed-mode cracking, which may also occur when an overload failure is caused by a combination of ductile and brittle cracking mechanisms. It describes the general aspects of fracture modes and mechanisms. The article discusses some of the material, mechanical, and environmental factors that may be involved in determining the root cause of an overload failure. It also presents examples of thermally and environmentally induced embrittlement effects that can alter the overload fracture behavior of metals.