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Hydro-extractors
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001401
EISBN: 978-1-62708-220-4
Abstract
Following disruption of the austenitic stainless steel basket of a hydro-extractor used for the separation of crystals of salt (sodium chloride) from glycerin, samples of the broken parts were analyzed. Examination revealed that the fish-plates joining the reinforcing hoops had broken, the shell had split from top to bottom adjacent to the weld, the top and bottom cover plates had become loose, all the rivets having pulled out, and the shaft was also found to be bent. Fracture took place in an irregular manner and was of the shear type towards both ends; it occurred immediately adjacent to the weld or a short distance from it and on alternate sides. Microscopical examination did not reveal any intergranular carbide precipitation, such as is well known to result in the weld-decay mode of failure. It was concluded that the primary cause of failure was stress-corrosion cracking arising from the combined effect of residual stresses and the corrosive effect of the material being centrifuged. If the shell had been stress-relieved after fabrication, the failure likely would not have occurred.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001420
EISBN: 978-1-62708-220-4
Abstract
A hydroextractor installed new for the drying of sugar massecuite consisted of a metal basket fixed to a vertical spindle. Disruption occurred just after the machine had been run up to speed and was not preceded by any abnormal behavior. The basket assembly consisted of a Ni-Cr-Mo steel shell and two end plates. It was designed to spin at 2200 rpm, using centrifugal force to expel liquids through nearly 3000 drilled holes in the shell wall. Investigators found that the shell separated completely from the bottom plate. The top plate, though it cracked radially, remained attached over most of its circumference. The basket also contained a 22-gauge Monel metal liner that had been perforated by stabbing, raising pronounced burrs that faced each hole. Apart from the local spots of corrosion due to the lining, the inner surface of the basket showed little evidence of general corrosion. What caused the basket to fail was the presence of corrosion-fatigue cracks or fissures radiating from the holes. A secondary cause was that the scantlings of the basket were too light.