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Magnetic particle inspection
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Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006758
EISBN: 978-1-62708-295-2
Abstract
The goal of using nondestructive evaluation (NDE) in conjunction with failure analysis is to obtain the most comprehensive set of data in order to characterize the details of the damage and determine the factors that allowed the damage to occur. The NDE results can be used to determine optimal areas upon which to focus for sectioning and metallography in order to further investigate the condition of the component. This article provides information on the inspection method available for failure analysis, including standard methods such as visual testing, penetrant testing, and magnetic particle testing. It covers the effects of various factors on the properties of the part that may impact failure analysis, describes the characterization of damage modes and crack sizes, and finally discusses the processes involved in application of NDE results to failure analysis.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0048102
EISBN: 978-1-62708-224-2
Abstract
A bridge wheel from a 272,160 kg stripper crane fractured in the web near the rim after one year of service. The wheel was forged from 1055 steel, and the tread, hub faces, and hub bore were machined. Beach marks indicative of fatigue at ten locations were revealed by macroscopic examination of the fracture surfaces. The surface of the web was heavily scaled and decarburized. A gross forging defect extending about 1.8 mm along the fracture surface was disclosed by examination of a micrograph of a section through one of the fatigue origins. Shallower forging defects were visible along the web surface. Fatigue cracking of the wheel was initiated at forging defects in the web. Replacement wheels were machined all over and were magnetic particle inspected to detect any cracks that could act as stress raisers.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0047860
EISBN: 978-1-62708-218-1
Abstract
The 1040 steel crankshaft in a reciprocating engine cracked within one year of operation. The journals of the main and crankpin bearings were inspected by the magnetic-particle method. Three to six indications of 1.5 to 9.5 mm long discontinuities were observed in at least four of the main-bearing journals. A crack along the fillet, almost entirely through the web, was observed in one of the main-bearing journals. Numerous coarse segregates, identified as sulfide inclusions, were identified by macroetching the surface during metallographic examination of a section taken through the main-bearing journal at the primary crack. Fatigue cracking with low-stress high-cycle characteristics was disclosed during macroscopic examination of the crack surface. Sulfide inclusions, which acted as stress raisers, were found to be present in the region where cracking originated. As a corrective measure, ultrasonic inspection was used in addition to magnetic-particle inspection to detect discontinuities.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001569
EISBN: 978-1-62708-229-7
Abstract
This paper reviews several fatigue failures from the waterwall, superheater, and economizer portions of the boiler, their causes and how they were mitigated and monitored. Some cases required simple field modifications by cutting or welding, repair of existing controls, and/or changes in maintenance. Nondestructive inspections by visual, magnetic particle, ultrasonic, and radiographic methods for detecting and monitoring damage are discussed. These failures are presented to provide hindsight that will help others in increasing the success rate for anticipating and analyzing the remaining life of other units.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001421
EISBN: 978-1-62708-235-8
Abstract
The bottom flange of a vertical pipe coupled to an isolating valve in a steam supply line to a turbine failed. Steam pressure was 1,500 psi and the temperature 416 deg C (780 deg F). Multiple cracking occurred in the bore of the flange. A quarter-segment was cut out and examined. The cracks were located in the part of the flange that formed a continuation of the pipe bore. The majority of them originated at the end of the flange bore and extended axially along the pipe and radially across the flange face. Magnetic crack detection revealed a further number of cracks in the weld deposit. While the fracture in the weld metal was of the ductile type exhibiting a fine fibrous appearance, that in the flange material was of the cleavage type. Microscopic examination revealed that the cracks were blunt-ended fissures of the type characteristic of corrosion-fatigue. It was concluded that cracking was due to corrosion-fatigue, which arose from the combined effect of a fluctuating tensile stress in the presence of a mildly corrosive environment.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c0046242
EISBN: 978-1-62708-236-5
Abstract
An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0059924
EISBN: 978-1-62708-235-8
Abstract
The large steel ring produced for a nuclear application from a billet of 8822 steel was inspected. The large billet was first forged into a doughnut preform in a large press, and then formed into the ring by ring rolling. A straight-beam ultrasonic inspection was instituted and calibrated using the back-surface-reflection method to determine whether adequate ultrasonic penetration was available. Areas of indications were noted at approximately midheight and adjacent to the bore area. An axial angle-beam inspection from the outside was performed, mainly in the area of indications to reveal detectable indications. The indications were not considered serious enough to reject the forgings. A few small indications in the areas tested were revealed by magnetic particle inspection. The area was conditioned by grinding and polishing to obtain an additional inspection at a greater depth from the inside surface. A much more severe condition was revealed after the test. The indications were classified as areas of chemical segregation and nonmetallic inclusions. The ring was considered unsatisfactory for the application and replacement of the defective ring from an acceptable billet was the most economical solution.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047148
EISBN: 978-1-62708-235-8
Abstract
A connecting rod (forged from 15B41 steel and heat treated to a hardness of 29 to 35 HRC) from a truck engine failed after 73,000 Km (45,300 mi) of service. A piece of the I-beam sidewall of the rod, about 6.4 cm (2 in.) long, was missing when the connecting rod arrived at a laboratory for testing. Analysis (visual inspection, 100x nital-etched micrograph, fluorescent magnetic-particle testing, and metallographic examination) supported the conclusion that the rod failed in fatigue with the origin along the lap and located approximately 4.7 mm below the forged surface. The presence of oxides may have been a partial cause for the defect. Recommendations included better inspection of the forgings by fluorescent magnetic-particle testing before machining.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047161
EISBN: 978-1-62708-235-8
Abstract
Routine magnetic-particle inspection revealed crack indications in a number of shafts produced from hot-rolled 4130 steel bar. A pronounced indication of this size is cause for rejection if the defect is not eliminated during subsequent machining. A microstructural analysis of the shaft cross section revealed that the crack was approximately 0.5 mm (0.020 in.) deep and oriented in a radial direction. Furthermore, no stringer-type nonmetallic inclusions were observed in the vicinity of the flaw, which did not display the intergranular characteristics of a quench crack. The defect did, however, contain substantial amounts of oxide, which evidently resulted from the hot-working operation. This evidence supports the conclusion that the appearance of this discontinuity, with the long axis parallel to the working direction and radial orientation with regard to depth, strongly suggests a seam produced during rolling. Use of components with surface-defect indications as small as 0.5 mm (0.02 in.) can be risky in certain circumstances. Depending on the orientation of the flaw with respect to applied loads, the nature of the applied forces (for example, cyclic), and the operating environment, such a surface flaw can become the initiating site for a fatigue crack or a corrosion-related failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0046044
EISBN: 978-1-62708-235-8
Abstract
A rocket-motor case made of consumable-electrode vacuum arc remelted D-6ac alloy steel failed during hydrostatic proof-pressure testing. Close visual examination, magnetic-particle inspection, and hardness tests showed cracks that appeared to have occurred after austenitizing but before tempering. Microscopic examinations of ethereal picral etched sections indicated that the cracks appeared before or during the final tempering phase of the heat treatment and that cracking had occurred while the steel was in the as-quenched condition, before its 315 deg C (600 deg F) snap temper. Chemical analysis of the cracked metal showed a slightly higher level of carbon than in the component that did not crack. X-ray diffraction studies of material from the fractured dome showed a very low level of retained austenite, and chemical analysis showed a slightly higher content of carbon in the metal of the three cracked components. Bend tests verified the conclusion that the most likely mechanism of delayed quench cracking was isothermal transformation of retained austenite to martensite under the influence of residual quenching stresses. Recommendations included modifying the quenching portion of the heat-treating cycle and tempering in the salt pot used for quenching, immediately after quenching.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048099
EISBN: 978-1-62708-235-8
Abstract
A bridge wheel on a crane, forged from 1055 steel, fractured after one year of service. The wheel fractured in the web between the hub and the rim. A small area containing beach marks that originated in a heavily burned area on the web surface was revealed by visual examination of the fracture surface. Surface burning to a depth of approximately 0.8 mm was disclosed by metallographic examination of a section taken through the region that contained the beach marks. A forging defect was indicated by the degree of decarburization and oxide dispersion that were visible. The failure was concluded to have been caused by surface burning during the forging operation. As a preventive measure more closely controlled heating practice during forging to eliminate surface burning was recommended. The burnt region was suggested to be removed in case burning occurs.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0089734
EISBN: 978-1-62708-235-8
Abstract
A system of carbon steel headers, handling superheated water of 188 deg C (370 deg F) at 2 MPa (300 psi) for automobile-tire curing presses, developed a number of leaks within about four months after two to three years of leak-free service. All the leaks were in shielded metal arc butt welds joining 200 mm (8 in.) diam 90 deg elbows and pipe to 200 mm (8 in.) diam welding-neck flanges. A flange-elbow-flange assembly and a flange-pipe assembly that had leaked were removed for examination. Investigation (visual inspection, hardness testing, chemical analysis, magnetic-particle testing, radiographic inspection, and 2% nital etched 1.7x views) showed varying IDs on the assemblies and supported the conclusions that the failures of the butt welds were the result of fatigue cracks caused by cyclic thermal stresses that initiated at stress-concentrating notches at the toes of the interior fillet welds on the surfaces of the flanges. Recommendations included using ultrasonic testing to identify the appropriate joints and then replacing them. Special attention to accuracy of fit-up in the replacement joints was also recommended to achieve smooth, notch-free contours on the interior surfaces.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047118
EISBN: 978-1-62708-235-8
Abstract
An automobile manufacturer rejected several 1035 steel stub axles because of what appeared to be short longitudinal cracks in the surfaces of the pins. The cracks were found when six axles were examined for defects by magnetic-particle inspection. However, metallographic examination showed that these lines were not cracks but slag inclusions at and immediately below the surface. Analysis (visual inspection, metallographic examination, and 100x/500x magnetic-particle inspection) supported the conclusions that the inclusions consisted of pieces of fireclay from channel brick that were flushed into the ingot mold. Although no true cracks were present, rejection of the stub axles was nevertheless justified. Slag streaks could reduce the strength of the stub axles and lead to the formation of fatigue fractures during operation. No recommendations were made.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0047151
EISBN: 978-1-62708-227-3
Abstract
A motorboat engine connecting rod forged from carbon steel fractured in two places and cracked at the small end during service. The analysis (visual inspection, 50x micrographs of sections etched with 2% nital, magnetic-particle inspection, and metallographic examination) supported the conclusion that the connecting rods were rendered susceptible to fatigue-crack initiation and propagation by the notch effect of coarse folds formed during the forging operation. One fracture was caused by fatigue resulting from operating stresses, and the other was a secondary tensile fracture. No recommendations were made.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0047964
EISBN: 978-1-62708-223-5
Abstract
Drastic reduction in the service life of a production gearbox was observed. Within the gearbox, the axial load on a bevel gear (8620 steel, OD 9.2 cm) was taken by a thrust-type roller bearing (3.8 cm ID, 5.6 cm OD) in which a ground surface on the back of the bevel gear served as a raceway. Spalling damage on the ground bearing raceway at five equally spaced zones was disclosed by inspection of the bevel gear. The bearing raceway was checked for runout by mounting the gear on an arbor. It was found that the raceway undulated to the extent of 0.008 mm total indicator reading and a spalled area was observed at each high point. The presence of numerous cracks that resembled grinding cracks was revealed both by magnetic-particle inspection and microscopic examination. Spalling was produced by nonuniform loading in conjunction with grinding cracks. As corrective measures, the spindle of the grinding machine was reconditioned to eliminate the undulations and retained austenite was minimized by careful heat treatment.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0089563
EISBN: 978-1-62708-217-4
Abstract
A lever (machined from a casting made of AISI type 410 stainless steel, then surface hardened by nitriding) that was a component of the main fuel-control linkage of an aircraft engine fractured in flight after a service life of less than 50 h. Investigation (radiographic inspection) supported the conclusions that the lever broke at a cold shut extending through approximately 95% of the cross section. The normally applied load constituted an overload of the remainder of the lever. Recommendations included adding magnetic-particle inspection to the inspection procedures for this cast lever.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0047856
EISBN: 978-1-62708-217-4
Abstract
The master connecting rod of a reciprocating aircraft engine revealed cracks during routine inspection. The rods were forged from 4337 (AMS 6412) steel and heat treated to a specified hardness of 36 to 40 HRC. H-shaped cracks in the wall between the knuckle-pin flanges were revealed by visual examination. The cracks were originated as circumferential cracks and then propagated transversely into the bearing-bore wall. No inclusions in the master rod were detected by magnetic-particle and x-ray inspection. Three large inclusions lying approximately parallel to the grain direction and fatigue beach marks around two of the inclusions were revealed by macroscopic examination of the fracture surface. Large nonmetallic inclusions that consisted of heavy concentrations of aluminum oxide (Al2O3) were revealed by microscopic examination of a section through the fracture origin. The forging vendors were notified about the excess size of the nonmetallic inclusions in the master connecting rods and a nondestructive-testing procedure for detection of large nonmetallic inclusions was established.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001552
EISBN: 978-1-62708-217-4
Abstract
This report covers case histories of failures in fixed-wing light aeroplane and helicopter components. A crankshaft of AISI 4340 Ni-Cr-Mo alloy steel, heat treated and nitrided all over, failed in bending fatigue. The nitrided layer was ground too rapidly causing excessive heat generation which induced grinding cracks and grinding burn. Tensional stresses resulting from grinding developed in a thin surface layer. On another crankshaft, chromium plating introduced undesirable residual tensile stresses. Such plating is an unsatisfactory finish for crankshafts of aircraft engines. Aircraft engine manufacturers and aeronautical standards require magnetic particle inspection to detect grinding cracks after reconditioning. Renitriding after any grinding is needed also, regardless of the amount of undersize as it introduces beneficial residual compressive stresses.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001902
EISBN: 978-1-62708-217-4
Abstract
In a spring leg of a main landing gear, large brittle fracture zones indicated a predominately cleavage pattern with some ductile dimples, and a tiny fatigue segment disclosed fine striations. Factors influencing failure were surface decarburization, notch sensitivity of the modified SAE 6150 spring steel, Canada's cold weather which may have had an embrittling effect on the steel, and cumulative fatigue damage from severe landing loads during service life. Replacement with heavier-duty spring legs will probably not eliminate this type of failure, but their use has reduced the number of failures substantially. Precautionary measures recommended to preclude accidents include removal of decarburization, proper operation of main landing gears, and adequate magnetic particle inspection of the legs at the beginning and end of the ski season to detect any fatigue cracks that might develop in attachment holes.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001904
EISBN: 978-1-62708-217-4
Abstract
A steel eyebolt which attached a rear lift strut to the right wing of a helicopter failed by fatigue. As a contributing factor, thread cutting produced sharp notches at thread roots, reducing fatigue life. Also, design fatigue life may have been exceeded as the part was in use about 10,000 h. Cumulative damage resulting from a previous accident could have occurred too. Because of this accident, inspectors were instructed to examine threaded zones of eyebolts by magnetic particle inspection after every 100 h in service. A maraging steel drive shaft of a helicopter also failed because of corrosion (pits), and continuous abnormal misalignment as well. Corrosion probably developed from moisture and water droplets on shaft diaphragm profiles. Improved diaphragm pack seals and coatings made by an electron-coat process (such as a Sermetal finish) are now used in new shafts.
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