This article introduces some of the general sources of heat treating problems with particular emphasis on problems caused by the actual heat treating process and the significant thermal and transformation stresses within a heat treated part. It addresses the design and material factors that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated with nonferrous heat treatments. The processes involved in cold working of certain ferrous and nonferrous alloys are also covered.

This article is dedicated to the fields of mechanical engineering and machine design. It also intends to give a nonexhaustive view of the preventive side of the failure analysis of rolling-element bearings (REBs) and of some of the developments in terms of materials and surface engineering. The article presents the nomenclature, numbering systems, and worldwide market of REBs as well as provides description of REBs as high-tech machine components. It discusses heat treatments, performance, and properties of bearing materials. The processes involved in the examination of failed bearings are also explained. Finally, the article discusses in detail the characteristics and prevention of the various types of failures of REBs: wear, fretting, corrosion, plastic flow, rolling-contact fatigue, and damage. The article includes an Appendix, which lists REB-related abbreviations, association websites, and ISO standards.

Component slippage in the left-side final drive train of a tracked military vehicle was detected after the vehicle had been driven 13,700 km (8500 miles) in combined highway and rough-terrain service. The slipping was traced to the mating surfaces of the final drive gear and the adjacent splined coupling sleeve. Specifications included that the gear and coupling be made from 4140 steel bar oil quenched and tempered to a hardness of 265 to 290 HB (equivalent to 27 to 31 HRC) and that the finish-machined parts be single-stage gas nitrided to produce a total case depth of 0.5 mm (0.020 in.) and a minimum surface hardness equivalent to 58 HRC. Investigation (visual inspection, low-magnification images, 500X images of polished sections etched in 2% nital, spectrographic analysis, and hardness testing) supported the conclusion that the failure occurred by crushing, or cracking, of the case as a result of several factors. Recommendations included reducing the high local stresses at the pitch line to an acceptable level with a design modification. Also suggested was specification of a core hardness of 35 to 40 HRC to provide adequate support for the case and to permit attainment of the specified surface hardness of 58 HRC.

SAE grade 5 U-bolts were used to fasten auxiliary dual wheels to the axles on a farm tractor. Under typical farm usage, the bolts are expected to have infinite life. However, several U-bolts made of 29 mm diam rod broke after less than 100 h of service. The bolt legs in which the failures occurred were all in the same position relative to the direction of wheel rotation. Visual examination showed the break was a fairly flat transverse fracture in the threaded section between the washer and the nut. The appearance of the fracture surfaces was characteristic of failure by low-cycle fatigue, with a smooth matte fatigue failure region showing beach marks and generally extending over about 40 to 60% of the fracture surface, which indicated severe overload. The point of initiation of fatigue was at the root of the last thread at the edge of the nut on the side toward this washer. The U-bolts fractured in fatigue because the bolt material had poor hardenability relative to the diam of the bolts. The bolt material was changed from 1045 steel to 1527 steel, a warm-finished low-alloy steel. The diameter of the bolts was reduced to 27.2 mm and the threads were rolled rather than cut.

An agricultural tine, which is a relatively large double torsion spring with outer legs that are used to sweep through hay or other crops and turn them over, had failed. It was made hard-drawn carbon steel. Bending fatigue was revealed by visual examination to be almost certainly the cause of failure. The fatigue fracture origin was found on the inside surface of the legs at the point where they joined the coiled body of the spring. It was established that the tines after being wound up by loading with hay, sprung back through the neutral unloaded position and into the unwind direction. This movement into the unwind direction was concluded to be happening often enough to initiate fatigue. The stress relieving temperature was recommended to be increased to reduce the residual stresses from coiling and hence improve fatigue performance.

Cast iron bearing caps in tractor engines fractured repeatedly after only short operating periods. The fracture originated in a cast-in groove and ran approximately radially to the shaft axis. The smallest cross section was at the point of fracture. The core structure of the caps consisted of graphite in pearlitic-ferritic matrix. Casting stresses did not play a decisive role because of the simple shape of the pieces that were without substantial cross sectional variations. Two factors exerted an unfavorable effect in addition to comparatively low strength. First, the operating stress was raised locally by the sharp-edged groove, and second, the fracture resistance of the cast iron was lowered at this critical point by the existence of a ferritic bright border. To avoid such damage in the future it was recommended to observe one or more of the following precautions: 1) Eliminate the grooves; 2) Remove the ferritic bright border; 3) Avoid undercooling in the mold and therefore the formation of granular graphite; 4) Inoculate with finely powdered ferrosilicon into the melt for the same purpose; and, 5) Anneal at lower temperature or eliminate subsequent treatment in consideration of the uncomplicated shape of the castings.

A tool used to stretch reinforcement wires in prestressed concrete failed. All eight individual jaws were broken. Visual examination of the fracture surfaces indicated that about half of the broken parts had a partially dendritic appearance. Further, fracture surfaces near the exteriors of the parts were clean and smooth, and there was evidence of a case. Examination of the flat surfaces of the parts revealed surface cracking where actual failure had not occurred. Chemical analysis showed the material to be a low-alloy carburizing steel. The microstructure was compatible with a steel which is cast, carburized, quenched, and tempered. The structure was generally satisfactory, except for the presence of severe shrinkage porosity. It was concluded that the presence of shrinkage porosity in critical areas was the primary cause of fracture. Extremely high hardness indicating a lack of adequate tempering was the secondary cause.

The specially designed sand-cast low-alloy steel jaws that were implemented to stretch the wire used in prestressed concrete beams fractured. The fractures were found to be macroscale brittle and exhibited very little evidence of deformation. The surface of the jaws was disclosed by metallographic examination to be case carburized. The case was found to be martensite with small spheroidal carbides while the core consisted of martensite plus some ferrite. The fracture was revealed to be related to shrinkage porosity. Tempering was revealed to be probably limited to about 150 deg C by the hardness values (close to the maximum hardness values attainable) for the core. It was interpreted that the low tempering temperature used may have contributed to the brittleness. The procedures used for casting the jaws were recommended to be revised to eliminate the internal shrinkage porosity. Tempering at a slightly higher temperature to reduce surface and core hardness was recommended.

Cerclage wire, which was used with two screws and washers for a tension band in a corrective internal fixation, was found broken at several points and corroded after nine months in service. The material was examined using energy-dispersive x-ray analysis and determined not to be in compliance with standards (type 304 stainless steel without molybdenum). The screws and washers were found to be made of remelted implant-quality type 316L stainless steel and were intact. Signs of sensitization, characterized by chromium carbide precipitates at the grain boundaries, were revealed by the microstructure. Intercrystalline corrosion with pitted grains was indicated by SEM fractography. Improper heat treatment of the steel was interpreted to have led to intercrystalline corrosion and implant separation.

After being in service for ten years, two admiralty brass heat-exchanger tubes from a cooler in a refinery catalytic reforming unit cracked circumferentially in the area of U-bends. A blunt transgranular cracking with minimal branching propagating from the inside surface of the tube was revealed by metallography which was typical of cracking by corrosion fatigue mechanism. Corrosion deposits on both the inside- and outside-diam surfaces were found in the tubes. The presence of copper, zinc, iron, and small amounts of chloride, sulfur, silicon, tin, and manganese was revealed by energy-dispersive analysis of the deposits. It was interpreted by the hardness values (higher than typical for annealed copper tubing) that the tubes may not have been annealed after the U-bends were formed and thus the role of residual stresses in the crack was revealed. It was concluded that the tubes failed by corrosion fatigue initiated by pitting at the inside-diam surface. The tubes were recommended to be annealed after bending to reduce residual stresses from the bending operation to an acceptable level.

A tubular heat exchanger in a refinery reformer unit leaked after one month of service. The exchanger contained 167 type 304 stainless steel U-bent integral-finned tubes. Cracks in the tube wall were revealed during examination. Hardness of the tube was found to be 30 HRC at the inside surface and up to 40 HRC at the base of the fin midway between the roots which indicated that the fins were cold formed and not subsequently annealed thus susceptible to SCC because of a high residual stress level. It was revealed by metallographic examination that the fracture was predominantly by transgranular branched cracking and had originated from the inside surface. It was concluded that the tubes failed in SCC caused by chlorides in the presence of high residual stresses. The finned tubes were ordered in the annealed condition as a corrective measure.

U-shaped leaf springs, intended to serve as spacers between oil tank floats and the inner walls of the containers, broke while being fitted, or after a short time in use, in the bend of the U. The springs were made of tempered strip steel of type C 88 with 0.84 % C, bent at room temperature, and electroplated with cadmium for protection against corrosion. Each fracture showed seven or eight kidney-shaped cracks. At the origins of these cracks on the concave inner surface of the springs, crater-like depressions and beads of melted and resolidified material were found. Fracture of the springs was caused by stress cracks as a consequence of local hardening. The hardening caused by melting and resolidification, and therefore the cracks in the springs, was the result of a faulty procedure during cadmium electroplating.

A pushrod made by inertia welding two rough bored pieces of bar stock installed in a mud pump fractured after two weeks in service. The flange portion was made of 94B17 steel, and the shaft was made of 8620 steel. It was disclosed by visual examination that the fracture occurred in the shaft portion at the intersection of a 1.3 cm thick wall and a tapered surface at the bottom of the hole. The fatigue crack was influenced by one-way bending stresses initiated at the inner surface and progressed around the entire inner circumference. A heavily decarburized layer was detected on the inner surface of the flange portion and sharp corner was found at the intersection of the sidewall and bottom of the hole. It was concluded that the stress raiser due to the abrupt section change was accentuated by decarburized layer. As a corrective measure, the design of the pushrod was changed to a one-piece forging and circulation of atmosphere during heat treatment was permitted through a hole drilled in the flange end of the rod to avoid decarburization.

A bolt breaks along a change in cross section well below its rated capacity. An anchoring screw spins freely in place, having snapped at its first supporting thread. A motor unexpectedly disengages its load, its driveshaft having fractured near a keyway. Such failures – involving axles, leaf springs, engine rods, wing struts, bearings, gears, and more – can occur, seemingly without cause, due to vibrational fracture. Vibrational fractures begin as cracks that form under cyclic loading at nominal stresses which may be considerably lower than the yield point of the material. The fracture is proceeded by local gliding and the development of cracks along lattice planes favorably orientated with respect to the principal stress. This non-reversible process is often misleadingly called “fatigue” and presents significant challenges to engineering teams that ill-advisedly take to searching for material faults. Several examples of notch-induced vibrational fractures are presented along with guidelines for investigating their cause.

Two diesel engine crankshafts of similar dimensions, the journal diam being approximately 7 in., failed due to cracking originating in the fillet at the junction between the crankpin and the web nearest to the flywheel. The cracks were discovered before rupture occurred. Several small cracks originated in the fillet, ran together and developed as two main crack fronts that ultimately merged into one, a typical example of a fatigue failure. Electromagnetic crack detection revealed the presence of a number of discontinuities which were located at a position that would correspond to the vertical axis of the original ingot. The crankshaft had not been stress-relieved after a welding operation had been carried out. The only satisfactory course to follow when dealing with a highly stressed part in which defects of the type in question are revealed during machining is to scrap the forging.

Three radiant tubes, made of three different high-temperature alloys, were removed from a carburizing furnace after approximately eight months of service when they showed evidence of failure by collapsing (telescoping) in a region 30 cm (12 in.) from the tube bottoms in the vicinity of the burners. The tubes had an original wall thickness of 3.0 mm (0.120 in.) and were made of three different alloys: the first was Hastelloy X; the second alloy was RA 333, a wrought nickel-base heat-resistant alloy; and the third was experimental alloy 634, which contained 72% Ni, 4% Cr, and 3.5% Si. The three radiant tubes had been operated at a temperature of about 1040 deg C (1900 deg F) to maintain furnace temperatures of 900 to 925 deg C (1650 to 1700 deg F). Analysis (visual inspection and micrographic examination) supported the conclusion that all three tubes failed by corrosion. Recommendations included replacing the material with an alloy, such as RA 333, with a higher chromium content and with an additional element, like silicon, resistant to carburization-oxidation.

High-chromium steel pipes 42.25 x 3.25 mm from a blast furnace gas fired recuperator for the preheating of air were heavily oxidized and perforated in places. It was found that the blast furnace gas had a high sulfur content. Both the carburization and the formation of sulfide proved that in addition, from time to time at least, combustion was incomplete and the operation was carried out in a reducing atmosphere, with the result that oxygen deficiency prevented the formation or maintenance of a protective surface layer on the external surface of the pipes. The sulfur would probably not have damaged the nickel-free steel used here at the given temperatures if it had been present as sulfur dioxide in an oxidizing atmosphere. The damage was therefore caused primarily by an incorrectly conducted combustion process.

Severely reduced wall thickness was encountered at the liquid line of a lead-bath pan that was used in a continuous strip or wire oil-tempering unit. Replacement of the pan was necessary after six months of service. The pan, 6.9 m (22.5 ft) long, 0.6 m (2 ft) wide, and 38 cm (15 in.) deep with a 2.5-cm (1-in.) wall thickness, was a type 309 stainless steel weldment. Operating temperatures of the lead bath in the pan ranged from 805 deg C (1480 deg F) at the entry end to 845 deg C (1550 deg F) at the exit end. Analysis (visual inspection. metallographic analysis, moisture testing, and etched micrographs using Murakami's reagent) supported the conclusions that thinning of the pan walls at the surface of the molten lead resulted from using coke of high moisture content and from the low fluctuating coke level. Recommendations included reducing the supply of oxygen attacking the grain boundaries and the hydrogen that readily promoted decarburization with the use of dry (2 to 3% moisture content) coke. Maintaining a thick layer of coke over the entire surface of molten lead in the pan would exclude atmospheric oxygen from the grain boundaries.

Three radially-cracked disks that circulated the protective gases in a bell-type annealing furnace were examined. During service they had been heated in cycles of 48 h to 720 deg C for 3 h each time, then were kept at temperature for 15 h followed by cooling to 40 deg C in 30 h, while rotating at 1750 rpm. Two disks were cracked at the inner face of the sheet metal rim while the rim of the third was completely cracked through. An analysis of the sheet metal rim of one of the disks showed the following composition: 0.06C, 1.98Si, 25.8Cr, and 35.8Ni. A steel of such high chromium content was susceptible to s-phase formation when annealed under 800 deg C. The material selected was therefore unsuitable for the stress to be anticipated. In view of the required oxidation resistance, a chromium-silicon or chromium-aluminum steel with 6 or 13% Cr would have been adequate. If the high temperature strength of these steels proved inadequate, an alloy lower in chromium would have been preferable.

Heating elements, consisting of strips, 40 mm x 2 mm, of the widely used 80Ni-20Cr resistance heating alloy, and designed to withstand a temperature of 1175 deg C, were rendered unusable by scaling after a few months service in a through-type annealing furnace, Although the temperature supposedly did not exceed 1050 deg C. Structural observations indicated a special case of internal oxidation. The required conditions for this were apparently provided by the moist hydrogen atmosphere of the annealing furnace, in which the chromium was oxidized, while the oxides of iron and nickel were reduced. Even the carbon suffered incomplete combustion and was enriched in the core. Thus, no protective layer could form or be maintained. The intergranular advancement of the oxidation may have been favored by the precipitation of chromium-rich carbides on the austenite grain boundaries. This form of internal oxidation is, in the case of Ni-Cr alloys, known as green rot. Alloys containing iron should be more resistant. As a preventive measure it was recommended to reduce the operating temperature of the strip sufficiently to allow the use of Fe-Ni-Cr alloys.