This article presents a failure analysis of an aluminum cylinder head on an automotive engine. During an endurance test, a crack initiated from the interior wall of a hole in the center of the cylinder head, then propagated through the entire thickness of the component. Metallurgical examination of the crack origin revealed that casting pores played a role in initiating the crack. Stress components, identified by finite element analysis, also played a role, particularly the stresses imposed by the bolt assembly leading to plastic strain. It was concluded that the failure can be prevented by eliminating the bolt hole, using a different type of bolt, or adjusting the fastening torque.

A commercial hybrid-iron golf club fractured during normal use. The club fractured through its cast aluminum alloy hosel. Optical analysis revealed casting pores through 20% of the hosel thickness. Mechanical properties were determined from characterization results, then used to construct a finite element model to analyze material performance under failure conditions. In addition, a full scale structural test was conducted to determine failure strength. It was concluded that the club failed not from ground impact but from a force reversal at the bottom of the downswing. Large moments generated during the downswing aggravated by manufacturing defects and stress concentration combined to create an overload condition.

A very large diameter worm gear that had been in service in a dam for more than 60 years exhibited cracks and was removed. It was reported that the high-strength, low-ductility cast bronze gear was only rarely stressed during service, associated with infrequent opening and closing of gates. Due to the age of the gear and the time frame of its manufacture, no original material specifications or strength requirements could be located. Likewise, no maintenance records of possible repairs to the gear were available. Investigation (visual inspection, chemical analysis, tension and hardness testing, 119x SEM images, and potassium dichromate etched 297x metallographic images) supported the conclusion that the bronze gear cracked via mixed-mode overload, rather than by a progressive mechanism such as fatigue or stress-corrosion cracking. The cracking was not associated with regions that would be highly stressed and did not appear to be consistently correlated to casting imperfections, repair welds, or associated heat-affected zones. Cracking across the gear face suggested that bending forces from misalignment were likely responsible for the cracking. Recommendations included further review of the potential root cause.

The bone cement failed at the distal end of the prosthesis stem of femoral head prosthesis six months after implantation. A small indentation on the lateral contour of the stem was visible where the stem had broken. The degree of loosening (gap between the lateral stem contour and the bone or cement) and implant loading was revealed by the dislocation of fragments of the prosthesis. Secondary cracks that had originated at the lateral aspect of the stem were revealed by metallographic examination of a section parallel to the stem surface and perpendicular to the fracture surface of the distal fragment. Gas pores are apparent in the grain and at the grain boundaries were revealed by a transverse section. Fine parallel line structures that run diagonally through the fractograph may be slip traces were revealed by scanning electron microscopy. One of the cracks was revealed to have propagated through a larger gas pore by a ruptured gas pore. The stresses created through the fatigue process activated glide systems which served the formation of secondary cracks along glide planes.

Two steam-methane reformer furnaces were subjected to short-time heat excursions because of a power outage, which resulted in creep bulging in the Incoloy 800 outlet pigtails, requiring complete replacement. Each furnace had three cells, consisting of 112 vertical tubes per cell, each filled with a nickel catalyst. The tubes were centrifugally cast from ASTM A297, grade HK-40 (Fe-25Cr-20Ni-0.40C), heat-resistant alloy. The tube was concluded after metallurgical inspection to have failed from creep rupture (i.e., stress rupture). A project for detecting midwall creep fissuring was instigated as a result of the failure. It was concluded after laboratory radiography and macroexamination that if the fissure were large enough to show on a radiograph, either with or without the catalyst, the tube could be expected to fail within one year. The set up for in-service radiograph examination was described. The tubes of the furnace were radiographed during shut down and twenty-four tubes in the first furnace and 53 in the second furnace showed significant fissuring. Although, radiography was concluded to be a practical technique to provide advance information, it was limited to detecting fissures caused by third-stage creep in tubes because of the cost involved in removing the catalysts.

Two water pumps were taken out of service because of reduced output. Visual inspection revealed considerable material loss in both impellers, which were 25.4 cm (10 in.) in diam x 1.3 cm (0.5 in.) wide and made from a cast bronze alloy. Several similar water pumps operating under nearly identical conditions, drawing water from an open tank through a standpipe, had no observable failures. Etched micrographs 100x of samples taken from the impellers showed clean, pockmarked, severely eroded surfaces, characteristic of cavitation damage. Investigation also revealed that considerable quantities of air were being drawn into the system when water in the supply tank dropped below a certain level. It was concluded that cavitation erosion (due to the uptake of air) caused metal removal and microstructural damage in the impellers. Recommendations included adding a water-level control to the piping system and excluding air from the pump inlet.

Stator vanes (cast from a Cu-Mn-Al alloy) in a hydraulic dynamometer used in a steam-turbine test facility were severely eroded. The dynamometer was designed to absorb up to 51 MW (69,000 hp) at 3670 rpm, and constituted an extrapolation of previous design practices and experience. Its stator was subject to severe erosion after relatively short operating times and initially required replacement after each test program. Although up to 60 cu cm (3.7 cu in.) of material was being lost from each vane, it only reduced the power-absorption capacity by a small amount. Analysis supported the conclusion that the damage was due to liquid erosion, but it could not be firmly established whether it was caused by cavitation or by liquid impact. Recommendations included making a material substitution (to Mo-13Cr-4Ni stainless steel) and doing a redesign to reduce susceptibility to erosion as well as erosion-producing conditions.

A failure analysis was conducted in late 1996 on two rolls that had been used in the production of iron and steel powder. The rolls had elongated over their length such that the roll trunnions had impacted with the furnace wall refractory. The result was distortion and bowing of the roll bodies which necessitated their removal from service. The initial analysis found large quantities of nitrogen had been absorbed by the roll shell. Further research indicated nitrogen pickup accounted for 3% volumetric growth for every 1% by weight nitrogen absorption. This expansion was sufficient to account for the dimensional change observed in the failed rolls. This paper details the failure analysis and resulting research it inspired. It also provides recommendations for cast material choice in highly nitriding atmospheres.

A microstructural analysis has been made of a burner nozzle removed from service in a coal gasification plant. The nozzle was a casting of a Co-29wt%Cr-19wt%Fe alloy. Extensive hot corrosion had occurred on the surface. There was penetration along grain boundaries, and corrosion products in these regions were particularly rich in S, and also contained Al, Si, O, and Cl. The grain boundaries contained Cr-rich particles which were probably Cr23-C6 type carbides. In the matrix, corrosion occurred between the Widmanstatten plates. Particles were found between these plates, most of which were rich in Cr and O, and probably were Cr2-O3 oxides. Other matrix particles were found which were rich in Al, O, and S. The corrosion was related to these grain boundary and matrix particles, which either produced a Cr-depleted zone around them or were themselves attacked.

During periodic inspection of the tubes of a reformer furnace, a soapy water leak test with the tubes pressurized with nitrogen was being carried out by site personnel in a manner contrary to the policy of the organization when one of the tubes suddenly disintegrated with explosive violence. The tube approximately 30 ft. long by 6 in. diam, was constructed of three spun cast sections butt welded together. The material specified for tubes for this service was basically a 25% chromium, 20% nickel, cast stainless steel containing 0.4% carbon to optimize creep resistance. Failure initiated in the region of the tube where the dark fracture surface and columnar grain structure were evident. These features indicated the presence of a defective zone or progressive cracking which had occurred during service. Microscopic examination of sections through the zone revealed extensive creep cracking. The cracking was intergranular and followed the interdendritic columnar structure adjacent to the outer surface.

Chain link, a part of a mechanism for transferring hot or cold steel blooms into and out of a reheating furnace, broke after approximately four months of service. The link was cast from 2% Cr austenitic manganese steel and was subjected to repeated heating to temperatures of 455 to 595 deg C (850 to 1100 deg F). Examination included visual inspection, macrograph of a nital-etched specimen from an as-received chain link 1.85x, micrographs of a nital-etched specimen from an as-received chain link 100x/600x, normal microstructure of as-cast standard austenitic manganese steel 100x, micrograph of a nital-etched specimen that had been austenitized 20 min at 1095 deg C (2000 deg F) and air cooled 315x, and micrograph of the same specimen after annealing 68 h at 480 deg C (900 deg F) 1000x). Investigation supported the conclusions that the chain link failed in a brittle manner, because the austenitic manganese steel from which it was cast became embrittled after being reheated in the temperature range of 455 to 595 deg C (850 to 1100 deg F) for prolonged periods of time. The alloy was not suitable for this application, because of its metallurgical instability under service conditions.

A sample tube was removed from a reformer furnace for life assessment after 69,000 h of service. Sections were cut from the tube, which was a spindle cast A297 Grade HK 40 (25 Cr, 20 Ni, 0.4 C) austenitic steel of 122.5 mm OD and 10.5 mm nominal wall thickness. They were examined metallographically on transverse sections and on longitudinal sections through the butt welds joining the separate cast segments of the tube. Creep damage was mainly concentrated within the inner one third of the wall thickness. The use of damage assessment parameters in evaluating the reformer tube remaining life showed the welds to be inadequate, and to have a strength and creep resistance below those of the base metal.

This investigation involved two AISI 304L acid storage tanks and one AISI 304L spent solvent tank from a sewage treatment facility. After installation, these tanks were hydrostatically tested using sewage effluent. No leaks were found and after a year or two, the tanks were drained and filled with nitric acid in preparation for service. Three weeks later the two acid tanks were found to be leaking from the bottom. Samples from the spent solvent tank revealed that pitting was located in a depressed area near a suction hole, beneath a black residue. It was concluded that the acid tanks failed by chloride-induced pitting initiated by microbial activity. Further, the spent solvent tank failed by a similar, but anaerobic mechanism. The use of the effluent for the hydrostatic test and the failure to remove it and clean and dry the tanks was the primary cause of failure. Localized carbide segregation in the original plate served as preferential corrosion sites. Had the tanks been hydrostatically tested in a proper manner, the pitting may not have occurred.

Microstructural examinations on transverse cross sections of a steam reformer tube, showed the presence of large macrovoids elongated in the radial direction and emanating from the internal surface of the tube. The macrovoids were located at the interdendritic regions, and were partially filled by a Mn-Fe bearing chromium oxide film. The areas adjacent to the oxide film were chemically depleted in C, Cr and Mn and rich in Fe and Ni. Associated with this depletion were a large concentration of microvoids. It was suggested that the dissolution of carbides in areas surrounding the macrovoids and the concentration of stresses at their tips, caused extensive localized plastic deformation which led to the formation of microvoids and subsequently to the spalling of the oxide film. The non-protective character of the film induced a progressive deterioration of the grain boundaries properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube.

To determine the effect of severe service on cast 357 aluminum pistons, a metallurgical evaluation was made of four pistons removed from the engine of the Hawk-Offenhauser car which had been driven by Rich Muther in the first Ontario, California 500 race. The pistons were studied by visual inspection, hardness traverses, radiography, dye penetrant inspection, chemical analysis, macrometallography, optical microscopy, and electron microscopy. The crown of one piston had a rough, crumbly deposit, which was detachable with a knife. Two pistons had remains of carbonaceous deposits. The fourth was severely hammered. It was concluded that the high temperatures developed in this engine created an environment too severe for 357 aluminum. Surfaces were so hot that the low-melting constituent melted. Then, the alloy oxidized rapidly to form Al2O3, an abrasive which further aggravated problems. The temperature in much of the piston was high enough to cause softening by overaging, lowering strength.

After 14 months of service, cracks were discovered in castings and bolts used to fasten together braces, posts, and other structural members of a cooling tower, where they were subjected to externally applied stresses. The castings were made of copper alloys C86200 and C86300 (manganese bronze). The bolts and nuts were made of copper alloy C46400 (naval brass, uninhibited). The water that was circulated through the tower had high concentrations of oxygen, carbon dioxide, and chloramines. Analysis (visual inspection, bend tests, fractographs, 50x unetched micrographs, 100x micrographs etched with H4OH, and 500x micrographs) supported the conclusions that the castings and bolts failed by SCC caused by the combined effects of dezincification damage and applied stresses. Recommendations included replacing the castings with copper alloy C87200 (cast silicon bronze) castings. Replacement bolts and nuts should be made from copper alloy C65100 or C65500 (wrought silicon bronze).

A desuperheater diffuser nozzle in the steam supply line failed within nine months of service in an 8.25 MN/sq m (1200 psig) steam line. The nozzle was an austenitic stainless steel casting in conformance to material. The nozzle had numerous cracks on the inside and outside surfaces, and the cracks had penetrated through the wall thickness in several areas. The fracture surfaces had distinct beach markings delineating the crack front, representative of crack propagation stages. The cracks were transgranular and, unlike classical corrosion-fatigue cracks, exhibited branching, characteristic of chloride-induced SCC in austenitic stainless steels. The failure resulted from chloride-induced SCC, possibly assisted by cyclic stress. The recommendation for alternate material for the desuperheater nozzle included nickel base alloys per ASTM B 564, Grades 600 or 800 titanium alloy per ASTM B 367, Grades C3/C4, or ferritic stainless steel alloy per ASTM 182, Grade FXM27.

In the EMD-2 Joint Directed Attack Munition (JDAM), the A357 aluminum alloy housing had been redesigned and cast via permanent mold casting, but did not meet the design strength requirements of the previous design. Mechanical tests on thick and thin sections of the forward housing assembly revealed tensile properties well below the allowable design values. Radiology and CT evaluations revealed no casting defects. Optical microscopy revealed porosity uniformly distributed throughout the casting on the order of 0.1 mm pore diam. Scanning electron microscopy revealed elongated pores, which indicated turbulent filling of the mold. Spherical pores would have indicated the melt had been improperly degassed. Based on these findings, it was recommended that the manufacturer analyze and redesign the gating system to eliminate the turbulent flow problem during the permanent mold casting process.

A new supplier for aluminum die castings was being evaluated, and the castings failed to meet the durability test requirements. Specifically, the fatigue life of the castings was low. Initial inspection of the fatigue fracture surfaces revealed large-scale porosity visible to the naked eye. New castings with reduced porosity also failed the durability tests. The fatigue fracture surfaces of additional casting fragments were very rough and contained multiple ratchet marks along the inner fillet. These observations indicated the fatigue process was heavily influenced by the presence of surface imperfections. Improving the surface finish or choosing a stronger alloy, were more likely to improve part durability than reducing the porosity.

Cluster bomb tailcone assemblies each containing two aluminum die-cast components were rejected because of the poor surface condition of the die castings. Numerous heat checks were found on the surfaces of the tailcones and radiographic inspection revealed inclusions, gas holes, and shrinkage defects in the castings. Most of the components failed to meet required mechanical properties because of these casting defects.