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Nickel-chromium-molybdenum steel
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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001787
EISBN: 978-1-62708-241-9
Abstract
A masonry type drill bit, designed for impact drilling in rock, fractured after a short time in service. Samples of the failed bit were analyzed using optical and scanning electron microscopy, quantitative metallography, and chemical analysis. The composition was found to be that of 18CrNi3Mo steel. Investigators also found evidence of inclusions and prior austenite grain size, although it was determined that neither played a role in the failure. Rather, according to test data, the failure occurred because of stress concentration (due to geometric discontinuities along the tooth profiles) and the cumulative effect of torque and force loading (the byproduct of continuous twisting and axial impact). Cracks readily initiate under these conditions then propagate quickly through what was found to be networks of tempered martensite, thus resulting in premature failure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001790
EISBN: 978-1-62708-241-9
Abstract
The failure of a high-speed pinion shaft from a marine diesel engine was investigated. The shaft, which had been in service for more than 30 years, failed shortly after the bearings were replaced. Examination of the shaft revealed cyclic fatigue, with a substantial distribution of nonmetallic inclusions near the fracture initiation site. Fracture mechanics analysis indicated that, if stresses acting on the shaft were induced only by normal service loads, there was little likelihood that the inclusions served as failure initiation sites. Further examination of the bearing elements revealed an abnormal wear pattern, consistent with the application of elevated bending loads. The root cause of failure was determined to be an increase in service stresses after bearing replacement along with the presence of nonmetallic inclusions in the shaft.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001792
EISBN: 978-1-62708-241-9
Abstract
Two shafts that transmit power from the engine to the propeller of a container ship failed after a short time in service. The shafts usually have a 25 year lifetime, but the two in question failed after only a few years. One of the shafts, which carries power from a gearbox to the propeller, is made of low alloy steel. The other shaft, part of a clutch mechanism that regulates the transmission of power from the engine to the gears, is made of carbon steel. Fracture surface examination of the gear shaft revealed circumferential ratchet marks with the presence of inward progressive beach marks, suggesting rotary-bending fatigue. The fracture surfaces on the clutch shaft exhibited a star-shaped pattern, suggesting that the failure was due to torsional overload which may have initiated at corrosion pits discovered during the examination. Based on the observations, it was concluded that rotational bending stresses caused the gear shaft to fail due to insufficient fatigue strength. This led to the torsional failure of the corroded clutch shaft, which was subjected to a sudden, high level load when the shaft connecting the gearbox to the propeller failed.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001814
EISBN: 978-1-62708-241-9
Abstract
A pressure vessel failed causing an external fire on a nine-story coke gasifier in a refinery power plant. An investigation revealed that the failure began as cracking in the gasifier internals, which led to bulging and stress rupture of the vessel shell, and the escape of hot syngas, setting off the fire. The failure mechanisms include stress relaxation cracking of a large diameter Incoloy 825 tube, stress rupture of a 4.65 in. thick chromium steel shell wall, and the oxidation of chromium steel exposed to hot syngas. The gasifier process and operating conditions that contributed to the high-temperature degradation were also analyzed and are discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001256
EISBN: 978-1-62708-218-1
Abstract
There was a large incidence of surface defects on the crank pins and journals and other areas of crank shafts of a high power automotive engine. The steel used was a Cr-Mo type of nitriding steel. Metallographic observations conclusively proved that the defective areas were entrapment of foreign bodies, resulting from steel making/deoxidizing/teeming stages. The occasionally globular nature of the foreign particles suggested these were formed at the liquid condition of the steel. The ratio of Mn-Si as seen on electron probe microanalysis also suggested the globules high in Mn content might have resulted in deoxidizing stage. Particularly the absence of Fe in some areas in the inclusion was indicative of precipitation deoxidation by ferromanganese/ferrosilicon. The defects apparently did not have time to coalesce and rise up to the top.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0047846
EISBN: 978-1-62708-218-1
Abstract
An 8640 steel shaft installed in a fuel-injection-pump governor that controlled the speed of a diesel engine used in trucks and tractors broke after few days of operation. The mechanism that drove the shaft was designed to include a slip clutch to protect the governor shaft from shock loading. It was revealed by visual examination that the fracture had initiated in the sharp corner at the bottom of a longitudinal hole which was part of a force feed lubricating system. Beach marks were observed on the fracture surfaces. It was revealed by further examination that the slip clutch was removed in an effort to reduce cost and hence the shaft was subjected to increased vibration and shock loading. Insufficient fatigue limit of the shaft was revealed by fatigue testing of the shafts taken from stock in a rotating-beam machine. As a corrective measure, the fatigue limit of shafts was increased to 760 MPA by nitriding for 10 h at 515 deg C.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001498
EISBN: 978-1-62708-218-1
Abstract
One end of an axle shaft containing the integral spur pinion was submitted for examination, along with the report of a tooth pitting failure. The spur pinion, integral to the axle shaft, operated in a medium-size, off-highway truck at an open-pit mine, for “a relatively short time.” Only the pinion head had been returned. The shaft portion had been torch-cut away. Chemical analysis along with the microstructure confirmed the specified material was SAE 43BV12 Ni-Cr-Mo alloy steel. The mode of failure was surface contact fatigue through the shear plane subsurface at the lowest point of single-tooth contact. The cause of failure was tooth-tip interference from the mating gear teeth. Because the mating parts within the assembly had not been returned or examined, unanswered questions remained.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0046870
EISBN: 978-1-62708-217-4
Abstract
A hollow, splined alloy steel aircraft shaft (machined from an AMS 6415 steel forging – approximately the same composition as 4340 steel – then quenched and tempered to a hardness of 44.5 to 49 HRC) cracked in service after more than 10,000 h of flight time. The inner surface of the hollow shaft was exposed to hydraulic oil at temperatures of 0 to 80 deg C (30 to 180 deg F). Analysis (visual inspection, 15-30x low magnification examination, 4x light fractograph, chemical analysis, hardness testing) supported the conclusions that the shaft cracked in a region subjected to severe static radial, cyclic torsional, and cyclic bending loads. Cracking originated at corrosion pits on the smoothly finished surface and propagated as multiple small corrosion-fatigue cracks from separate nuclei. The originally noncorrosive environment (hydraulic oil) became corrosive in service because of the introduction of water into the oil. Recommendations included taking additional precautions in operation and maintenance to prevent the use of oil containing any water through filling spouts or air vents. Also, polishing to remove pitting corrosion (but staying within specified dimensional tolerances) was recommended as a standard maintenance procedure for shafts with long service lives.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001560
EISBN: 978-1-62708-217-4
Abstract
Military aircraft use a cartridge ignition system for emergency engine starts. Analysis of premature failures of steel (AISI 4340) breech chambers in which the solid propellant cartridges were burned identified corrosion as one problem with an indication that stress-corrosion cracking may have occurred. A study was made for stress-corrosion cracking susceptibility of 4340 steel in a paste made of the residues collected from used breech chambers. The constant extension rate test (CERT) technique was employed and SCC susceptibility was demonstrated. The residues, which contained both combustion products from the cartridges and corrosion products from the chamber, were analyzed using elemental analysis and x-ray diffraction techniques. Electrochemical polarization techniques were also utilized to estimate corrosion rates.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0006444
EISBN: 978-1-62708-217-4
Abstract
Helicopter rotor blade components that included the horizontal hinge pin, the associated nut, and the locking washer were examined. Visual examination of the submitted parts revealed that the hinge pin, fabricated from 4340 steel, was broken and that the fracture face showed a flat beach mark pattern indicative of a preexisting crack. The threaded area of the pin had an embedded thread that did not appear to come from the pin. A chemical analysis was conducted on the embedded thread and on an associated attachment to determine the origin of the thread. Analysis showed that the thread and nut were 4140 steel. Scanning electron fractographic examination of the fracture initiation site strongly suggested that the fracture progressed by fatigue. It was concluded that the failure of the horizontal hinge pin initiated at areas of localized corrosion pits. The pits in turn initiated fatigue cracks, resulting in a failure mode of corrosion fatigue. It was recommended that all of the horizontal hinge pins be inspected. Those pins determined to be satisfactory for further use should be stripped of cadmium, shot peened, and coated with cadmium to a minimum thickness of 0.0127 mm (0.0005 in.).
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001538
EISBN: 978-1-62708-217-4
Abstract
Examination of a cracked nose landing gear cylinder made of AISI 4340 Cr-Mo-Ni alloy steel proved that the part started to fail on the inside diam. When the nucleus of the stress-corrosion crack was studied in detail, iron oxide was found on the fracture surface. A 6500x micrograph revealed this area also displayed an intergranular texture. One of a group of small grinding cracks on the ID of the cylinder nucleated the failure. Other evidence indicated the cracks developed when the cylinder was ground during overhaul.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001145
EISBN: 978-1-62708-217-4
Abstract
Cartridge-pneumatic starter systems are used on military aircraft. In the cartridge mode used for alert starts, the starter turbine is driven by hot gases produced through the controlled burning of a solid propellant cartridge within a closed chamber (the breech chamber/cartridge chamber assembly). Premature failures of steel breech chambers have been prevalent enough to cause serious concern. The breech chamber is fabricated from a 4340 Ni-Cr-Mo steel forging heat treated to a hardness in the range HRC 40 to 45. The failures have taken several forms, including fracture and unzipping of the chamber dome, burn-through of the dome, and shearing of bayonet locking lugs. Factors identified as significant in the failures are the pressure developed in the chamber and internal corrosion of the chamber in an environment that can produce stress-corrosion cracking. The interior configuration of the chamber and the stress distribution also have a bearing upon the failure modes. Several failures are reviewed to illustrate the problems.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001540
EISBN: 978-1-62708-217-4
Abstract
Ground maintenance personnel discovered hydraulic fluid leaking from two small cracks in a main landing gear cylinder made from AISI 4340 Cr-Mo-Ni alloy steel. Failure of the part had initiated on the ID of the cylinder. Numerous cracks were found under the chromium plate. A 6500x electron fractograph showed cracking was predominantly intergranular with hairline indications. Leaking had occurred only 43 h after overhaul of the part. Total service time on the part was 9488 h. It was concluded that cracking on the ID was caused by hydrogen embrittlement which occurred during or after overhaul. The specific source of hydrogen which produced failure was not ascertainable.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001542
EISBN: 978-1-62708-217-4
Abstract
A nose landing gear cylinder made from AISI 4340 Ni-Cr-Mo alloy steel was found cracked and leaking, causing partial depressurization. Investigation revealed the crack to be a stress-corrosion type, judging by the 6500x electron fractograph. It had started in a region of concentrated, large non-metallic inclusions near the chromium-plated ID of the cylinder. Also, there were breaks in the chromium plate and pits in the underlying base metal. The cylinder had been in service for 18,017 h, and 5948 h had passed since the first and only overhaul. Substandard plating of the ID at this time ultimately resulted in pitting of the metal. The combination of surface pitting and stress concentration at the nearby inclusions resulted in stress-corrosion cracking.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0047835
EISBN: 978-1-62708-217-4
Abstract
An articulated rod (made from 4337 steel (AMS 6412) forging, quenched and tempered to 36 to 40 HRC) used in an overhauled aircraft engine was fractured after being in operation for 138 h. Visual examination revealed that the rod was broken into two pieces 6.4 cm from the center of the piston-pin-bushing bore. The fracture was nucleated at an electroetched numeral 5 on one of the flange surfaces. A notch, caused by arc erosion during electroetching, was revealed by metallographic examination of a polished-and-etched section through the fracture origin. A remelted zone and a layer of untempered martensite constituted the microstructure of the metal at the origin. Small cracks, caused by the high temperatures developed during electro-etching, were observed in the remelted area. It was concluded that fatigue fracture of the rod was caused by the notch resulting from electroetching and thus electroetched marking of the articulated rods was discontinued as a corrective measure.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0047856
EISBN: 978-1-62708-217-4
Abstract
The master connecting rod of a reciprocating aircraft engine revealed cracks during routine inspection. The rods were forged from 4337 (AMS 6412) steel and heat treated to a specified hardness of 36 to 40 HRC. H-shaped cracks in the wall between the knuckle-pin flanges were revealed by visual examination. The cracks were originated as circumferential cracks and then propagated transversely into the bearing-bore wall. No inclusions in the master rod were detected by magnetic-particle and x-ray inspection. Three large inclusions lying approximately parallel to the grain direction and fatigue beach marks around two of the inclusions were revealed by macroscopic examination of the fracture surface. Large nonmetallic inclusions that consisted of heavy concentrations of aluminum oxide (Al2O3) were revealed by microscopic examination of a section through the fracture origin. The forging vendors were notified about the excess size of the nonmetallic inclusions in the master connecting rods and a nondestructive-testing procedure for detection of large nonmetallic inclusions was established.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001731
EISBN: 978-1-62708-217-4
Abstract
Service failures have occurred in a number of aircraft parts made of quenched and tempered steel heat treated to ultimate tensile strengths of 260,000 to 280,000 psi. Some of these failures have been attributed to “delayed cracking” as a result of hydrogen embrittlement or to stress-corrosion. Because of the serious nature of the failures and because the mechanism of the fracture initiation is not well understood, unusually complete laboratory investigations have been conducted. Three of these investigations are reviewed to illustrate the methods used in studying failures in aircraft parts. The results of the laboratory studies indicate that unusual care is necessary in the processing and fabrication of ultra-high-strength steel and in the design and maintenance of the structures in which it is used.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001552
EISBN: 978-1-62708-217-4
Abstract
This report covers case histories of failures in fixed-wing light aeroplane and helicopter components. A crankshaft of AISI 4340 Ni-Cr-Mo alloy steel, heat treated and nitrided all over, failed in bending fatigue. The nitrided layer was ground too rapidly causing excessive heat generation which induced grinding cracks and grinding burn. Tensional stresses resulting from grinding developed in a thin surface layer. On another crankshaft, chromium plating introduced undesirable residual tensile stresses. Such plating is an unsatisfactory finish for crankshafts of aircraft engines. Aircraft engine manufacturers and aeronautical standards require magnetic particle inspection to detect grinding cracks after reconditioning. Renitriding after any grinding is needed also, regardless of the amount of undersize as it introduces beneficial residual compressive stresses.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001504
EISBN: 978-1-62708-217-4
Abstract
Despite extensive aircraft landing gear design analyses and tests performed by designers and manufacturers, and the large number of trouble-free landings, aircraft users have experienced problems with and failures of landing gear components. Different data banks and over 200 failure analysis reports were surveyed to provide an overview of structural landing gear component failures as experienced by the Canadian Forces over the last 20 years on more than 20 aircraft types, and to assess trends in failure mechanisms and causes. Case histories were selected to illustrate typical problems, troublesome failure mechanisms, the role of high strength aluminum alloys and steels, and situations where fracture mechanics analyses provided insight into the failures. The two main failure mechanisms were: fatigue occurring mainly in steel components, and corrosion related problems with aluminum alloys. Very few overload failures were noted. A number of causes were identified: design deficiencies and manufacturing defects leading mainly to fatigue failures, and poor materials selection and improper maintenance as the principal causes of corrosion-related failures. The survey showed that a proper understanding of the failure mechanisms and causes, by thorough failure analysis, provides valuable feedback information to designers, operators and maintenance personnel for appropriate corrective actions to be taken.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001746
EISBN: 978-1-62708-217-4
Abstract
Brittle intergranular fracture, typical of a hydrogen-induced delayed failure, caused the failure of an AISI 4340 Cr-Mo-Ni landing gear beam. Corrosion resulting from protective coating damage released nascent hydrogen, which diffused into the steel under the influence of sustained tensile stresses. A second factor was a cluster of non-metallic inclusions which had ‘tributary’ cracks starting from them. Also, eyebolts broke when used to lift a light aircraft (about 7000 lb.). The bolt failure was a brittle intergranular fracture, very likely due to a hydrogen-induced delayed failure mechanism. As for the factors involved, cadmium plating, acid pickling, and steelmaking processes introduce hydrogen on part surfaces. As a second contributing factor, both bolts were 10 Rc points higher in hardness than specified (25 Rc), lessening ductility and notch toughness. A third factor was inadequate procedure, which resulted in bending moments being applied to the bolt threads.
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