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Chromium steel
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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001764
EISBN: 978-1-62708-241-9
Abstract
High failure rates in the drive shafts of 40 newly acquired articulated buses was investigated. The drive shafts were fabricated from a low-carbon (0.45%) steel similar to AISI 5046. Investigators examined all 40 buses, discovering six different drive shaft designs across the fleet. All of the failures, a total of 14, were of the same type of design, which according to finite-element analysis, produces a significantly higher level of stress. SEM examination of the fracture surface of one of the failed drive shafts revealed fatigue striations near the OD and ductile dimpling near the ID, evidence of high-cycle fatigue. Based on the failure rate and fatigue life predictions, it was recommended to discontinue the use of drive shafts with the inferior design.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001785
EISBN: 978-1-62708-241-9
Abstract
A maintenance worker was injured when his 3/4 in. (19 mm) open-ended wrench failed, fracturing in overload fashion along the jaw. The failed wrench was unavailable for testing, but an identical one that failed in the same manner was acquired and subjected to hardness, chemistry, SEM, and metallurgical analyses. SEM imaging revealed microvoid coalescence within the fracture zone. The microvoids were flat and smooth edged indicating insufficient bonding. In addition, a cross sectional sample, mounted and etched using alkaline chromate, revealed an oxygen-rich zone in the jaw. It was concluded that the failures stemmed from forging laps in the jaw that broaching failed to remove.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001792
EISBN: 978-1-62708-241-9
Abstract
Two shafts that transmit power from the engine to the propeller of a container ship failed after a short time in service. The shafts usually have a 25 year lifetime, but the two in question failed after only a few years. One of the shafts, which carries power from a gearbox to the propeller, is made of low alloy steel. The other shaft, part of a clutch mechanism that regulates the transmission of power from the engine to the gears, is made of carbon steel. Fracture surface examination of the gear shaft revealed circumferential ratchet marks with the presence of inward progressive beach marks, suggesting rotary-bending fatigue. The fracture surfaces on the clutch shaft exhibited a star-shaped pattern, suggesting that the failure was due to torsional overload which may have initiated at corrosion pits discovered during the examination. Based on the observations, it was concluded that rotational bending stresses caused the gear shaft to fail due to insufficient fatigue strength. This led to the torsional failure of the corroded clutch shaft, which was subjected to a sudden, high level load when the shaft connecting the gearbox to the propeller failed.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001795
EISBN: 978-1-62708-241-9
Abstract
A ball bearing in a military jet engine sustained heavy damage and was analyzed to determine the cause. Almost all of the balls and a portion of the outer race were found to be flaking, but there were no signs of damage on the inner race and cage. Tests (chemistry, hardness, and microstructure) indicated that the bearing materials met the specification requirements. However, closer inspection revealed areas of discoloration, or nonuniform contact marks, on the ID surface of the inner ring. The unusual wear pattern suggested that the bearing was not properly mounted, thus subjecting it to uneven or eccentric loading. This explains the preferential nature of the flaking on the outer race and points to an assembly error as the root cause of failure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001844
EISBN: 978-1-62708-241-9
Abstract
A cylindrical spiral gear, part of a locomotive axle assembly, cracked ten days after it had been press-fit onto a shaft, after which it sat in place as other repairs were made. Workers at the locomotive shop reported hearing a sound, and upon inspecting the gear, found a crack extending radially from the bore to the surface of one of the tooth flanks. The crack runs the entire width of the bore, passing through an oil hole in the hub, across the spoke plate and out to the tip of one of the teeth. Design requirements call for the gear teeth to be carburized, while the remaining surfaces, protected by an anti-carburizing coating, stay unchanged. Based on extensive testing, including metallographic examination, microstructural analysis, microhardness testing, and spectroscopy, the oil hole was not protected as required, evidenced by the presence of a case layer. This oversight combined with the observation of intergranular fracture surfaces and the presence of secondary microcracks in the case layer point to hydrogen embrittlement as the primary cause of failure. It is likely that hydrogen absorption occurred during the gas carburizing process.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001811
EISBN: 978-1-62708-241-9
Abstract
A deformed steel tube was received for failure analysis after buckling during a heat-treat operation. The tube was subjected to various metallurgical tests as well as nondestructive testing to confirm the presence of residual stresses. The microstructure of the tube was found to be homogenous and had no banded structure. However, x-ray diffraction analysis confirmed the presence of up to 6% retained austenite which likely caused the tube to buckle during the 910 °C heat treating procedure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001821
EISBN: 978-1-62708-241-9
Abstract
A fire in a storage yard engulfed several propane delivery trucks, causing one of them to explode. A series of elevated-temperature stress-rupture tears developed along the top of the truck-mounted tank as it was heated by the fire. Unstable fracture then occurred suddenly along the length of the tank and around both end caps, following the girth welds that connect them to the center portion of the tank. The remaining contents of the tank were suddenly released, aerosolized, and combusted, creating a powerful boiling liquid expanding vapor explosion (BLEVE). Based on the metallography of the tank pieces, the approximate tank temperature at the onset of explosion was determined. Metallurgical analysis provided additional insights as well as a framework for making tanks less susceptible to this destructive failure mechanism.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001831
EISBN: 978-1-62708-241-9
Abstract
An air blower in an electric power plant failed unexpectedly when a roller bearing in the drive motor fractured along its outer ring. Both rings, as well as the 18 rolling elements, were made from GCr15 bearing steel. The bearing also included a machined brass (MA/C3) cage and was packed with molybdenum disulfide (MoS 2 ) lithium grease. Metallurgical structures and chemical compositions of the bearing’s matrix materials were inspected using a microscope and photoelectric direct reading spectrometer. SEM/EDS was used to examine the local morphology and composition of fracture and contact surfaces. Chemical and thermal properties of the bearing grease were also examined. The investigation revealed that the failure was caused by wear due to dry friction and impact, both of which worsened as a result of high-temperature degradation of the bearing grease. Fatigue cracks initiated in the corners of the outer ring and grew large enough for a fracture to occur.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001833
EISBN: 978-1-62708-241-9
Abstract
The failure of a boiler operating at 540 °C and 9.4 MPa was investigated by examining material samples from the near-failure region and by thermodynamic analysis. A scanning Auger microprobe, SEM, and commercial thermodynamic software codes were used in the investigation. Results indicated that the boiler failure was caused by grain-boundary segregation of phosphorous, tin, and nitrogen and the in-service formation of carbide films and granules on the grain boundaries.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001835
EISBN: 978-1-62708-241-9
Abstract
Wind turbine blades are secured by a number of high-strength bolts. The failure of one such bolt, which caused a turbine blade to detach, was investigated to determine why it fractured. Based on the results of a detailed analysis, consisting of stress calculations, chemical composition testing, metallurgical examination, mechanical property testing, and fractographic analysis, it was determined that the bolt failed by fatigue accelerated by stress concentration at low temperatures. The investigation also provided suggestions for avoiding similar failures.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0089456
EISBN: 978-1-62708-223-5
Abstract
A cross-recessed die of D5 tool steel fractured in service. The die face was found to be subjected to shear and tensile stresses as a result of the forging pressures from the material being worked. The presence of numerous slag stringers was revealed by microscopic examination of an unetched longitudinal section taken through the die. The pattern was microscopically revealed after etching with 5 % nital to be due to severe chemical segregation or banding. Considerable variation in the hardness, corresponding to the banded and non-banded regions across the face of the specimen was observed. The fracture was found to have originated near the high-stress region of the die face examination of the fracture surface. Failure of the die was concluded to have originated in an area of abnormally high hardness which is prone to microcracking during heat treatment for this grade of tool steel
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0047154
EISBN: 978-1-62708-223-5
Abstract
The head of a socket spanner made of heat-treated 0.40C-0.34Cr steel cracked in service. The pronounced fibrous structure of the component became evident as soon as it was etched with 2% nital. Folds in the material originating from the shaping process were visible, and the micrograph showed that cracks ran along these folds oriented according to the fiber. The fissures, with the exception of the hardening crack, were partly filled with oxide and showed signs of decarburization at the edges. From this it could be assumed that parts of the external skin had been forced into the folds during forging. This evidence supported the conclusion that even through there was some indication of chemical segregation, the folds made during forging initiated the main crack. Furthermore, even if the steel had been more homogeneous, hardening cracks would probably have been promoted by the coarse fissures at the fold zones.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c9001155
EISBN: 978-1-62708-223-5
Abstract
Milling machine arbors were inserted with satellite spindles having a maximum speed of 1500 rpm, and broke out between the groove and the flange. The appearance of the fracture surface was the same on both arbors. The pronounced scan lines characterized the fractures as fatigue fractures. The appearance of the fracture in the arbors indicated ductile fatigue fracture which had its origin in the radii between groove and flange. These radii of 0.15 and 0.2 mm were too small for the load on the milling machine. In addition there were grooves at the base of the radii which had an unfavorable effect on the life of the component by acting as notches with their resulting stress concentration. Considering the great hardness of the case, the small radii would have been critical even without grooves. Measures were taken so that the critical radius of the milling machine was increased and the surface roughness measured more precisely.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c9001572
EISBN: 978-1-62708-236-5
Abstract
Extensive slipper/wobbler failures occurred in the integrated drive generators that incorporated TiN coated wobblers, during the production acceptance test. Similar coated wobblers had passed the application tests. The nature of the failure was extensive gouging of the wobbler surface with discoloration and coating removal. The substrate material was E52100 which was through-hardened to HRC 55-60. The slippers that were in contact with the coated wobbler surface were made of AISI 06 material. A synthetic oil was used as the hydraulic fluid in the application. The failure in the wobblers was caused by lack of temperature control during application which resulted in localized surface rehardening. It was established that there was a significant difference in the grade of the hydraulic fluid that was used in the two test programs. Use of superior grade of hydraulic fluid was recommended in this case for the production acceptance tests.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c0048397
EISBN: 978-1-62708-226-6
Abstract
A large portion of the four-hole Lane plate disintegrated and consisted mainly of corrosion products after remaining in the body for 26 years. Transformation structures and carbides were exhibited by the plate which was made from chromium steel. Minimal corrosion was exhibited by the soft austenitic 304 stainless steel used to make the screws. The corrosion products of the plate were revealed by microprobe analysis to impregnate the surrounding tissues. Improper material selection was concluded to be the reason for the general corrosion behavior.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001193
EISBN: 978-1-62708-229-7
Abstract
When a steam turbine was put out of service, cracks were noticed on many of the blades in the low pressure section round the stabilization bolts and perpendicular to the blade axis. The blades were made from chrome alloy steel X20-Cr13 (Material No. 1.402). When the bolts were brazed into the blades inadmissible localized overheating of the steel must have occurred, which resulted in transformation stresses and hence reduced deformability. The cracks arose as a consequence of careless brazing. Whether the cracks should be considered as stress cracks over their entire extent or partially as fatigue cracks produced by vibration in the operation of the turbine as a result of steplike growing of microcracks could not be deduced from the fracture surfaces. Microfractography showed that the cracks developed in stages.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c9001259
EISBN: 978-1-62708-233-4
Abstract
A bolt manufacturer observed that products made from certain shipments of steel 41 Cr4 wire were prone to the formation of quench cracks in their rolled threads. The affected wire was tested and found to be highly sensitive to overheating because of the metallurgical method by which it was produced. A stronger decarburization of the case was a contributing factor that could not be prevented by working because the thread was rolled. Hardening tests conducted by the bolt manufacturer showed that quench cracks did not occur in specimens that were turned down before hardening and when notches were machined instead of beaten with a chisel.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001557
EISBN: 978-1-62708-234-1
Abstract
A number of machined end frame steel forgings made of Cr-Si-Mn alloy showed tiny cracks during magnetic particle inspection after heat treatment. The cracks were mostly confined to base edges and fillet radius. No significant abnormality was observed in chemical composition and microstructure. SEM, optical microscopy, and gas analysis revealed that the subsurface discontinuous cracks at the bore edges and in the fillet radius of the heat-treated end frame component had occurred due to hydrogen embrittlement, and not because of faulty heat treatment. This conclusion was supported by the presence of cracklike indications in machined bore surface of the annealed part.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001192
EISBN: 978-1-62708-234-1
Abstract
The fracture cause had to be determined in a three-cylinder crankshaft made of chrome steel 34Cr4 (Material No. 1.7033) according to DIN 17200. The fracture occurred after only 150 h of operation. The fracture was of the bend fatigue type which originated in the fillet of the main bearing and ran across the jaw almost to the opposite fillet of the adjoining connecting rod bearing. The fillet was well rounded and smoothly machined. Thus, no reason for the fracture of the crankshaft could be found externally. No material defects were discernible in the origin or anywhere else. No cause for the crank fracture could be established from material testing. Probably the load was too high for the strength of the crank. Tensile strength could have been increased for the same material by tempering at lower temperature. Additionally, the resistance against high bend fatigue stresses or torsion fatigue stresses could have been increased substantially by including the fillet in the case hardening process.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0091893
EISBN: 978-1-62708-218-1
Abstract
An automotive front-wheel outer angular-contact ball bearing generated considerable noise shortly after delivery of the vehicle. The inner and outer rings were made of seamless cold-drawn 52100 steel tubing, the balls were forged from 52100 steel, and the retainer was stamped from 1008 steel strip. The inner ring, outer ring, and balls were austenitized at 845 deg C (about 1550 deg F), oil quenched, and tempered to a hardness of 60 to 64 HRC. Investigation (visual inspection) supported the conclusion that failure was caused by fretting due to vibration of the stationary vehicle position without bearing rotation. Recommendations included improving methods of securing the vehicle during transportation to eliminate vibrations.
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