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Ductile iron
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Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006831
EISBN: 978-1-62708-329-4
Abstract
The information provided in this article is intended for those individuals who want to determine why a casting component failed to perform its intended purpose. It is also intended to provide insights for potential casting applications so that the likelihood of failure to perform the intended function is decreased. The article addresses factors that may cause failures in castings for each metal type, starting with gray iron and progressing to ductile iron, steel, aluminum, and copper-base alloys. It describes the general root causes of failure attributed to the casting material, production method, and/or design. The article also addresses conditions related to the casting process but not specific to any metal group, including misruns, pour shorts, broken cores, and foundry expertise. The discussion in each casting metal group includes factors concerning defects that can occur specific to the metal group and progress from melting to solidification, casting processing, and finally how the removal of the mold material can affect performance.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c0047343
EISBN: 978-1-62708-236-5
Abstract
An experimental high-temperature rotary valve was found stuck due to growth and distortion after approximately 100 h. Gas temperatures were suspected to have been high due to overfueled conditions. Both the rotor and housing in which it was stuck were annealed ferritic ductile iron similar to ASTM A395. Visual examination of the rotor revealed unusually heavy oxidation and thermal fatigue cracking along the edge of the gas passage. Material properties, including microstructure, composition, and hardness, of both the rotor and housing were evaluated to determine the cause of failure. The microstructure of the rotor was examined in three regions. The shaft material, the heavy section next to the gas passage and the thin edge of the rotor adjacent to the gas passage. The excessive gas temperatures were responsible for the expansion and distortion that prevented rotation of the rotor. Actual operating temperatures exceeded those intended for this application. The presence of transformation products in the brake-rotor edge indicated that the lower critical temperature had been exceeded during operation.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c0089657
EISBN: 978-1-62708-233-4
Abstract
The gun mount used in two types of self-propelled artillery consists of an oil-filled recoil cylinder and a sand-cast (MIL-I-11466, grade D7003) ductile-iron piston that connects to the gun tube through a threaded rod. The piston contains several orifices through which oil is forced as a means of absorbing recoil energy. During operation, the piston is stressed in tension, pulled by oil pressure on one end and the opposing force of the gun tube on the other. The casting specification stipulated that the graphite be substantially nodular and that metallographic test results be provided for each lot. Investigation (visual inspection, fatigue testing, 0.25x/0.35x/50x magnifications, 2% nital etched 60x/65x magnifications, and SEM views) showed that most of the service fractures occurred in pistons containing vermicular graphite. Recommendations included ultrasonic testing of pistons already in the field to identify and reject those containing vermicular graphite. In addition, metallographic control standards were suggested for future production lots.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001532
EISBN: 978-1-62708-232-7
Abstract
Work rolls made of indefinite chill double-poured (ICDP) iron are commonly used in the finishing trains of hot-strip mills (HSMs). In actual service, spalling, apart from other surface degeneration modes, constitutes a major mechanism of premature roll failures. Although spalling can be a culmination of roll material quality and/or mill abuse, the microstructure of a broken roll can often unveil intrinsic inadequacies in roll material quality that possibly accentuate failure. This is particularly relevant in circumstances when rolls, despite operation under similar mill environment, exhibit variations in roll life. The paper provides an insight into the microstructural characteristics of spalled ICED HSM work rolls, which underwent failure under similar mill operating environment in an integrated steel plant under the Steel Authority of India Limited. Microstructural features influencing ICDP roll quality, viz. characteristics of graphite, carbides, martensite, etc., have been extensively studied through optical microscopy, quantitative image analysis (QIA), and electron-probe microanalysis (EPMA). These are discussed in the context of spalling propensity and roll life.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c0089617
EISBN: 978-1-62708-232-7
Abstract
A forged 4130 steel cylindrical permanent mold, used for centrifugal casting of gray- and ductile-iron pipe, was examined after pulling of the pipe became increasingly difficult. In operation, the mold rotated at a predetermined speed in a centrifugal casting machine while the molten metal, flowing through a trough, was poured into the mold beginning at the bell end and ending with the spigot end being poured last. After the pipe had cooled, it was pulled out from the bell end of the mold, and the procedure was repeated. Investigation supported the conclusion that failure of the mold surface was the result of localized overheating caused by splashing of molten metal on the bore surface near the spigot end. In addition, the mold-wash compound (a bentonite mixture) near the spigot end was too thin to provide the proper degree of insulation and to prevent molten metal from sticking to the bore surface. Recommendations included reducing the pouring temperatures of the molten metal and spraying a thicker insulating coating onto the mold surface.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0047312
EISBN: 978-1-62708-224-2
Abstract
A ductile iron T-hook hook was reported to have fractured in service. It was further reported that the hook had been subjected to a load that did not exceed 5900 kg (13,000 lb) at the time of fracture. No information was provided regarding the type of metal used to manufacture the hook. A failure analysis was requested to determine the cause of fracture. Two hooks were submitted for examination. Analysis (visual inspection, 2.7x light fractography, chemical analysis, 110x SEM fractography, 27x/110x/215x nital-etched micrographs) supported the conclusions that this component fractured in service as a consequence of ductile tensile overload. Evidence indicates that the fractured region was subjected to a load exceeding the capacity of the material. Because the information available from the service application indicated that the component had not been subjected to a stress that exceeded 5900 kg (13,000 lb), the observations made in this investigation suggested that either the load was underestimated or that the indicated load was applied at a more rapid rate (perhaps with a jerk), which would tend to increase the effective force of the load.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0047321
EISBN: 978-1-62708-224-2
Abstract
A 58.4 cm (23 in.) diam heavy-duty brake drum component of a cable-wound winch broke into two pieces during a shutdown period. Average service life of these drums was two weeks; none had failed by wear. The drums were sand cast from ductile iron. During haul-out, the cable on the cable drum drove the brake drum, and resistance was provided by brake bands applied to the outside surface of the brake drum. Friction during heavy service was sufficient to heat the brake drum, clutch mount, and disk to a red color. Examination of the assembly indicated that the brake drum would cool faster than its mounts and would contract onto them. Brittle fracture of the brake drum occurred as a result of thermal contraction of the drum web against the clutch mount and the disk. The ID of the drum web was enlarged sufficiently to allow for clearance between the web and the clutch mount and disk at a temperature differential of up to 555 deg C (1000 deg F). With the adoption of this procedure, brake drums failed by wear only.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0089633
EISBN: 978-1-62708-220-4
Abstract
A stuffing box (sand cast from ASTM A 536, grade 60-45-10, ductile iron) began leaking water after two weeks of service. The machine was operating at 326 rpm with a discharge water pressure of 21.4 MPa (3100 psi). Investigation (visual inspection, mechanical analysis, and nital etched 100x magnification) supported the conclusion that the crack initiated at the inner edge of a lubrication hole and had propagated toward both the threaded and flange ends of the casting. An appreciable residual-stress concentration must have been present and caused propagation of the crack. The residual stress might have been caused when a fitting was tightly screwed into the lubrication hole, and it might have been concentrated by notches at the inner end of the hole created when the drill broke through the sidewall to the stuffing box.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0047220
EISBN: 978-1-62708-220-4
Abstract
Two oil-pump gears broke after four months of service in a gas compressor that operated at 1000 rpm and provided a discharge pressure of 7240 kPa (1050 psi). The compressor ran intermittently with sudden starts and stops. The large gear was sand cast from class 40 gray iron with a tensile strength of 290 MPa (42 ksi) at 207 HRB. The smaller gear was sand cast from ASTM A536, grade 100-70-03, ductile iron with a tensile strength of 696 MPa (101 ksi) at 241 HRB. Analysis (metallographic examination) supported the conclusion that excessive beam loading and a lack of ductility in the gray iron gear teeth were the primary causes of fracture. During subsequent rotation, fragments of gray iron damaged the mating ductile iron gear. Recommendations included replacing the large gear material with ASTM A536, grade 100-70-03, ductile iron normalized at 925 deg C (1700 deg F), air cooled, reheated to 870 deg C (1600 deg F), and oil quenched. The larger gear should be tempered to 200 to 240 HRB, and the smaller gear to 240 to 280 HRB.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c0090965
EISBN: 978-1-62708-221-1
Abstract
The upper frame from a large cone crusher failed in severe service after an unspecified service duration. The ductile iron casting was identified as grade 80-55-06, signifying minimum properties of 552 MPa (80 ksi) tensile strength, 379 MPa (55 ksi) yield strength, and 6% elongation. Investigation (visual inspection, chemical analysis, unetched 30x images, and 2% nital etched 30x images) was difficult because the fracture surface of the frame section was obliterated by postfracture corrosion. Repeated attempts at cleaning using progressively stronger chemicals revealed that no telltale fracture morphology remained. However, the investigation supported the conclusion that the crusher frame failed via brittle overload fracture, likely due to excessive service stresses and substandard mechanical properties. Recommendations included additional quality-control measures to provide better spheroidal graphite morphology at the frame surface.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c9001633
EISBN: 978-1-62708-221-1
Abstract
Failure analysis of a mobile harbor crane wheel hub that included SEM and EDS analyses demonstrated that the mechanism of failure was fatigue. The wheel hub was a ductile cast iron component that had been subjected to cyclic loading during a ten-year service period. The fracture surface of the fatigue failure also contained corrosion deposit, suggesting that cracking occurred over a period of time sufficient to allow corrosion of the cracked surfaces. Replacement and alignment of the failed wheel hub was recommended along with inspection of the nonfailed wheel hubs that remained on the crane.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0089646
EISBN: 978-1-62708-235-8
Abstract
Nodular cast iron crankshafts and their main-bearing inserts were causing premature failures in engines within the first 1600 km (1000 mi) of operation. The failures were indicated by internal noise, operation at low pressure, and total seizing. Concurrent with the incidence of engine field failures was a manufacturing problem: the inability to maintain a similar microfinish on the cope and drag sides of a cast main-bearing journal. Investigation supported the conclusion that the root cause of the failure was carbon flotation due to the crankshafts involved in the failures showing a higher-than-normal carbon content and/or carbon equivalent. Larger and more numerous cope side graphite nodules broke open, causing ferrite caps or burrs. They then became the mechanism of failure by breaking down the oil film and eroding the beating material. A byproduct was heat, which assisted the failure. Recommendations included establishing closer control of chemical composition and foundry casting practices to alleviate the carbon-flotation form of segregation. Additionally, some nonmetallurgical practices in journal-finishing techniques were suggested to ensure optimal surface finish.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003508
EISBN: 978-1-62708-180-1
Abstract
This article focuses on the general root causes of failure attributed to the casting process, casting material, and design with examples. The casting processes discussed include gravity die casting, pressure die casting, semisolid casting, squeeze casting, and centrifugal casting. Cast iron, gray cast iron, malleable irons, ductile iron, low-alloy steel castings, austenitic steels, corrosion-resistant castings, and cast aluminum alloys are the materials discussed. The article describes the general types of discontinuities or imperfections for traditional casting with sand molds. It presents the international classification of common casting defects in a tabular form.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001087
EISBN: 978-1-62708-214-3
Abstract
The repeated failure of rubber-covered rotors and volute liners in a flue gas desulfurization system after conversion from lime slurry reagent to limestone slurry reagent was investigated. The pump was a horizontal 50 x 65 mm (2 x 2.5 in.) Galiger pump with a split cast iron case and open rotor (impeller). Both the case and the ductile iron rotor core were covered by natural rubber. Analyses conducted included surface examination of wear patterns, chemical analysis of materials, measurement of mechanical properties, and in-place flow tests. It was determined that the proximate cause of failure was cavitation and vortexing between the rotor and the lining. The root cause of the failure was the conversion from lime to limestone slurry without appropriate modification of the pump. Conversion to the limestone slurry resulted in fluid dynamics outside the operational limits of the pump. The recommended remedial action was replacement with a pump appropriately sized for the desired pressures and flow rates for limestone slurry.