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Corrosion fatigue
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Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006813
EISBN: 978-1-62708-329-4
Abstract
Heat exchangers are devices used to transfer thermal energy between two or more fluids, between a solid surface and a fluid, or between a solid particulate and a fluid at different temperatures. This article first addresses the causes of failures in heat exchangers. It then provides a description of heat-transfer surface area, discussing the design of the tubular heat exchanger. Next, the article discusses the processes involved in the examination of failed parts. Finally, it describes the most important types of corrosion, including uniform, galvanic, pitting, stress, and erosion corrosion.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006779
EISBN: 978-1-62708-295-2
Abstract
Fatigue failures may occur in components subjected to fluctuating (time-dependent) loading as a result of progressive localized permanent damage described by the stages of crack initiation, cyclic crack propagation, and subsequent final fracture after a given number of load fluctuations. This article begins with an overview of fatigue properties and design life. This is followed by a description of the two approaches to fatigue, namely infinite-life criterion and finite-life criterion, along with information on damage tolerance criterion. The article then discusses the characteristics of fatigue fractures followed by a discussion on the effects of loading and stress distribution, and material condition on the microstructure of the material. In addition, general prevention and characteristics of corrosion fatigue, contact fatigue, and thermal fatigue are also presented.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001828
EISBN: 978-1-62708-241-9
Abstract
A heat transport pump in a heavy water reactor failed (exhibiting excessive vibration) during a restart following a brief interruption in coolant flow due to a faulty valve. The pump had developed a large crack across the entire length of a bearing journal. An investigation to establish the root cause of the failure included chemical and metallurgical analysis, scanning electron fractography, mechanical property testing, finite element analysis of the shrink fitted journal, and a design review of the assembly fits. The journal failure was attributed to corrosion fatigue. Corrective actions to make the journals less susceptible to future failures were implemented and the process by which they were developed is described.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001830
EISBN: 978-1-62708-241-9
Abstract
An 18-MW gas turbine exploded unexpectedly after three hours of normal operation. The catastrophic failure caused extensive damage to the rotor, casing, and nearly all turbo-compressor components. Based on their initial review, investigators believed that the failure originated at the interface between two shaft sections held together by 24 marriage bolts. Visual and SEM examination of several bolts revealed extensive deterioration of the coating layer and the presence of deep corrosion pits. It was also learned that the bolts were nearing the end of their operating life, suggesting that the effects of fatigue-assisted corrosion had advanced to the point where one of the bolts fractured and broke free. The inertial unbalance produced excessive vibration, subjecting the remaining bolts to overload failure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001803
EISBN: 978-1-62708-241-9
Abstract
Metallurgical SEM analysis provides many insights into the failure of biomedical materials and devices. The results of several such investigations are reported here, including findings and conclusions from the examination a total hip prosthesis, stainless steel and titanium compression plates, and hollow spinal rods. Some of the failure mechanisms that were identified include corrosive attack, corrosion plus erosion-corrosion, inclusions and stress gaps, production impurities, design flaws, and manufacturing defects. Failure prevention and mitigation strategies are also discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001459
EISBN: 978-1-62708-234-1
Abstract
Fundamentals of fatigue failure are outlined. Addressed are fatigue crack characteristics, basic crack types, unidirectional bending, alternate bending, rotary bending, torsion, direct stress, and combined stress. Stress cycle, endurance limits, under and overstressing, stress concentration, and surface condition are discussed. Sections are devoted to fatigue crack assessment, corrosion relation to fatigue failure, and the micro-mechanisms of fatigue failure. Materials considered include steels. Photographs of service failures are used to illustrate features alluded to in the text.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c0065826
EISBN: 978-1-62708-233-4
Abstract
The wires used in a wet precipitator for cleaning the gases coming off a basic oxygen furnace failed. The system consisted of six precipitators, three separate dual units, each composed of four zones. Each zone contained rows of wires (cold drawn AISI 1008 carbon steel) suspended between parallel collector plates. It was determined that the 1008 wires failed because of corrosion fatigue. It was decided to replace all of the wires in the two zones with the highest rates of failure with cold-drawn type 304 austenitic stainless steel wire. These expensive wires, however, failed after a week by transgranular SCC. Annealed type 430 ferritic stainless steel was subsequently suggested to prevent further failures.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0047917
EISBN: 978-1-62708-227-3
Abstract
The support bearing of a hydrofoil vessel failed after only 220 h of operation. The bearing consisted of an outer ring made of chromium-plated AISI type 416 stainless steel and an inner ring with a spherical outer surface made of AISI type 440C stainless steel, with a plastic material, bonded to the outer ring, between the two. The inner ring was found to have failed in four places. The two metallic rings were allowed to come in contact with each other by the disappearance of the plastic material. It was revealed by examination of the fracture surfaces of the inner ring that the failure was caused by fatigue initiated in corrosion pits (caused by seawater). The fracture was found to be transgranular. It was recommended that the inner and outer rings should both be made from the more corrosion resistant 17-4 PH (AISI type 630) stainless steel.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c9001141
EISBN: 978-1-62708-227-3
Abstract
During a refit of a twenty-year-old Naval destroyer, two cracks were found on the inside of the killed carbon-manganese steel hull plate at the forward end of the boiler room. The cracks coincided with the location of the top and bottom plates of the bilge keel. Metallurgical examination of sections cut from the cracked area identified lamellar tearing as the principle cause of the cracking. This was surprising in 6 mm thick hull plates. Corrosion fatigue and general corrosion also contributed to hull plate perforation. Although it is probable that more lamellar tears exist near the bilge keel in other ships and may be a nuisance in the future, the hull integrity of the ships is not threatened and major repairs are not needed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c9001703
EISBN: 978-1-62708-227-3
Abstract
This paper describes the metallurgical investigation of a broken spindle used to attach an antenna to the mast of a naval vessel. Visual inspections of both failed and intact fastener assemblies were carried out both on-board ship and in the laboratory followed by metallographic and fractographic examinations. Simulations were also performed on stressed material in a suitable environment to assess the relative importance of postulated failure mechanisms. Factors contributing to this failure including assembly procedures and applied preloads, service loading and environment, and material selection and specification. The discussion considers whether this failure was an isolated incident or is likely to be a fleet-wide problem, and suggests ways to prevent reoccurrence.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0051292
EISBN: 978-1-62708-225-9
Abstract
Type 302 stainless steel springs used in a printing operation failed by breaking into several pieces after two months in service. The springs were operating over a very small deflection and were regulating the flow of ink, in which they were constantly immersed. Fatigue fractures on every piece of the spring were revealed by visual examination. Each of the fractures was found to be oriented at 45 deg to the wire axis. Clear evidence of pitting corrosion at the fatigue fracture origin was also observed. Free chloride ions were revealed to be present in the ink in which the spring was operating. An alternative ink that contained no free chloride ions was recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0051293
EISBN: 978-1-62708-225-9
Abstract
Majority of the water feeders in a new chicken house had stopped working. The water feeders were found to be operated on the principle that when the chickens pecked a plastic bowl, a compressed spring released a squirt of water. The small compression springs were made from type 302 stainless steel, and the operating stresses were safely within the design limits given by the Goodman diagram. The springs were revealed by scanning electron microscopy to contain numerous cracks on their inside surface, and these cracks were all at 45 deg to the wire axis. The solution was recommended as to select a grade of spring steel that would be more corrosion resistant than 302 stainless.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c9001243
EISBN: 978-1-62708-225-9
Abstract
A needle bearing from a filling and seating machine for milk cartons became unusable due to corrosion and fracture of a ring after only four weeks of operation of the machine in a Finnish milk packing plant. These bearings were subject to corrosion by water condensates in this type of environment because of constant temperature changes, and they normally are replaced after eight months. The bearings were lubricated by a molybdenum sulfide paste. Judging by their structure the needles probably consisted of ball bearing steel. They showed corroded initial cracks of the pitting type, i.e., shear-fatigue fractures due to excessive surface pressure. The needles too were overstressed by compression. It seemed that the higher pressure necessary for the pressing of thicker paper accelerated the corrosion, which lead to the crack initiations of the parts and possibly also to impaired lubrication. The machine manufacturer therefore switched to bearings with shells of a complex bronze.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c9001614
EISBN: 978-1-62708-225-9
Abstract
The damage to a screw on the head of a 1.8 liter personal car engine was nucleated as the result of common disadvantageous environmental influences and reversed loads leading to corrosion fatigue.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001420
EISBN: 978-1-62708-220-4
Abstract
A hydroextractor installed new for the drying of sugar massecuite consisted of a metal basket fixed to a vertical spindle. Disruption occurred just after the machine had been run up to speed and was not preceded by any abnormal behavior. The basket assembly consisted of a Ni-Cr-Mo steel shell and two end plates. It was designed to spin at 2200 rpm, using centrifugal force to expel liquids through nearly 3000 drilled holes in the shell wall. Investigators found that the shell separated completely from the bottom plate. The top plate, though it cracked radially, remained attached over most of its circumference. The basket also contained a 22-gauge Monel metal liner that had been perforated by stabbing, raising pronounced burrs that faced each hole. Apart from the local spots of corrosion due to the lining, the inner surface of the basket showed little evidence of general corrosion. What caused the basket to fail was the presence of corrosion-fatigue cracks or fissures radiating from the holes. A secondary cause was that the scantlings of the basket were too light.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001652
EISBN: 978-1-62708-220-4
Abstract
Three separate corrosion mechanisms were involved in the failure of an AISI type 304 stainless steel pipe elbow. The major cracks, including the one that penetrated the wall, tend to be wide-mouthed, tapering to a blunt tip, with corrosion products filling much of the crack space. This was characteristic of corrosion fatigue. The second type of cracking originated at some of the major cracks. These cracks were branched and transgranular, which is characteristic of stress-corrosion caused by chlorides. The third crack mode, an intergranular network, was most probably the result of hydrogen sulphide attack. The 13-year service life of the elbow made it difficult, if not impossible, to determine the order of the corrosion mechanisms or the length of time it took to reach the present state of degradation after the initiation of corrosion. Based on the long service life the present material has given, it was recommended that it be used again.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001421
EISBN: 978-1-62708-235-8
Abstract
The bottom flange of a vertical pipe coupled to an isolating valve in a steam supply line to a turbine failed. Steam pressure was 1,500 psi and the temperature 416 deg C (780 deg F). Multiple cracking occurred in the bore of the flange. A quarter-segment was cut out and examined. The cracks were located in the part of the flange that formed a continuation of the pipe bore. The majority of them originated at the end of the flange bore and extended axially along the pipe and radially across the flange face. Magnetic crack detection revealed a further number of cracks in the weld deposit. While the fracture in the weld metal was of the ductile type exhibiting a fine fibrous appearance, that in the flange material was of the cleavage type. Microscopic examination revealed that the cracks were blunt-ended fissures of the type characteristic of corrosion-fatigue. It was concluded that cracking was due to corrosion-fatigue, which arose from the combined effect of a fluctuating tensile stress in the presence of a mildly corrosive environment.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c9001579
EISBN: 978-1-62708-226-6
Abstract
Stainless steel is frequently used for bone fracture fixation in spite of its sensitivity to pitting and cracking in chloride containing environments (such as organic fluids) and its susceptibility to fatigue and corrosion fatigue. A 316L stainless steel plate implant used for fixation of a femoral fracture failed after only 16 days of service and before bone callus formation had occurred. The steel used for the implant met the requirements of ASTM Standard F138 but did contain a silica-alumina inclusion that served as the initiation point for a fatigue/corrosion fatigue fracture. The fracture originated as a consequence of stress intensification at the edge of a screw hole located just above the bone fracture; several fatigue cracks were also observed on the opposite side of the screw hole edge. The crack propagated in a brittle-like fashion after a limited number of cycles under unilateral bending. The bending loads were presumably a consequence of leg oscillation during assisted perambulation.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c9001664
EISBN: 978-1-62708-226-6
Abstract
A compression hip screw is a device designed to hold fractures in the area of the femur in alignment and under compression. A side plate, which is an integral part of the device, is attached by screws to the femur, and it holds the compression screw in position. The device analyzed had broken across the eighth hole (of nine holes) from the end of the plate. The detailed metallurgical failure analysis of the device, including metallography and fractography, is reported here. It was found that the device had adequate metallurgical integrity for the application for which it was intended. It is believed that failure was caused by the lack of a screw in the ninth hole. Evidence is also presented which indicates that the device was bent prior to insertion, and the local plastic deformation may have caused structural changes leading to premature crack initiation.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c0048728
EISBN: 978-1-62708-228-0
Abstract
After being in service for ten years, two admiralty brass heat-exchanger tubes from a cooler in a refinery catalytic reforming unit cracked circumferentially in the area of U-bends. A blunt transgranular cracking with minimal branching propagating from the inside surface of the tube was revealed by metallography which was typical of cracking by corrosion fatigue mechanism. Corrosion deposits on both the inside- and outside-diam surfaces were found in the tubes. The presence of copper, zinc, iron, and small amounts of chloride, sulfur, silicon, tin, and manganese was revealed by energy-dispersive analysis of the deposits. It was interpreted by the hardness values (higher than typical for annealed copper tubing) that the tubes may not have been annealed after the U-bends were formed and thus the role of residual stresses in the crack was revealed. It was concluded that the tubes failed by corrosion fatigue initiated by pitting at the inside-diam surface. The tubes were recommended to be annealed after bending to reduce residual stresses from the bending operation to an acceptable level.
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