Search Results for in situ lift-out

This article discusses the practice of FIB-based in situ lift-out, a sample preparation method that has proven particularly useful for failure analysis. It explains how samples are now being made for a wide range of TEM techniques, including holography, tomography, high-angle annular dark-field scanning, and electron energy-loss spectroscopy. In most cases, achieving optimal quality requires the use of alternate FIB milling angles, as in plan-view, sideways, and backside milling, all of which are discussed.

Ex-situ lift out (EXLO) techniques rely on van der Waals forces to transfer FIB milled specimens to various types of carriers using a glass probe micromanipulator. This article describes some of the latest EXLO techniques for site specific scanning transmission electron microscopy, including the use slotted half-grids and vacuum-assisted lift out for plan-view analysis.

This is the story of how the mainstream Omniprobe FIB lift-out solution was invented and delivered to the market.

This article compiles summaries of User Group meetings held at ISTFA 2013, including the Contactless Fault Isolation User’s Group, the Focused Ion Beam User’s Group, the Sample Prep/3D Package User’s Group, and the Nanoprobing User’s Group. For each meeting, a brief synopsis of the presentations and subsequent dialog is provided.

This article provides a summary of the presentations given at the four User’s Group meetings at ISTFA 2012. Each user group focused on one of the following topics: nanoprobing, contactless fault isolation, focused ion beam, and sample preparation.

This article discusses sample preparation challenges that have impeded progress in producing bias-enabled TEM samples from electronic components, as well as strategies to mitigate these issues.

TEM specimens prepared using a Ga FIB are susceptible to artifacts, such as surface amorphization and ion-implanted layers, that can be problematic in advanced technology nodes, particularly for FinFETs. As this article shows, however, post-FIB cleaning via concentrated argon ion milling makes for a fast and effective specimen preparation process for FinFET devices controlled to a thickness of less than 20 nm. Although the results presented here are based on 14 nm node FinFETs, the method is also applicable to the 10 and 7 nm FinFET technologies currently in production.

FIB milling is difficult if not impossible with III-V compound semiconductors and certain interconnect metals because the materials do not react well with the gallium used in most FIB systems. This article discusses the nature of the problem and explains how cryogenic FIB-SEM techniques provide a solution. It describes the basic setup of a FIB-SEM system and provides examples of its use on InN nanocrystals, GaN films, and copper-containing multilayer photovoltaic materials.

Xenon plasma focused ion beam specimen preparation is ideal for preparing plan view TEM specimens due to its large-volume-milling capabilities. This article describes concentrated Ar ion beam milling using low energy as a post-pFIB final thinning step of plan view TEM specimens from a phase change memory device. Precise control of specimen thinning is achieved, which results in high-quality specimens with pristine surfaces and a large field of view for TEM characterization.

This article discusses the basic procedures involved in atom probe tomography (APT) and demonstrates its use on complex material stacks. Although still a relatively new technique, APT has moved to the forefront of semiconductor failure analysis because it can provide 3D chemical composition of a wide range of materials on a near-atomic scale.

The tools of the trade in semiconductor failure analysis have advanced rapidly over the past few decades, bringing major improvements in imaging, deprocessing, and materials analysis. In contrast to the progress made in physical FA, little attention has been given to the failure analysis process itself. This article shows through case studies how simple oversights and misunderstandings can lead to costly mistakes. It also defines basic FA concepts and presents a failure analysis sequence, describing each step along with common pitfalls and best practices.

Sample preparation is a critical step for dopant profiling of FinFET devices, especially when targeting individual fins. This article describes a sample-preparation technique based on low-energy, shallow-angle ion milling and shows how it minimizes surface amorphization and improves scanning capacitance microscopy (SCM) signals representative of local active dopant concentration.

The sixth FIB-SEM workshop was held March 1, 2013, in Cambridge, Mass. This article provides a summary of the event along with highlights from the 18 paper presentations.

Long-term stability studies indicate that cathode degradation is one of the main failure mechanisms in anode-supported SOFCs. In order to better understand the microstructural degradation mechanisms of the cathode and the influence of oxygen partial pressure at relevant operating temperatures, the authors of this article acquired TEM samples from technological cells to study cation interdiffusion mechanisms and LSM-YSZ interactions, particularly in areas where LSM grains are in contact with YSZ electrolyte. Here they present and interpret the results.

The ability to discern the composition and placement of atoms in a sample makes TEM one of the most powerful characterization tools for microelectronic components. For many devices, however, the dynamics underlying normal operation do not displace atoms. Device function is, instead, mediated by electronic and thermal processes that have little effect on physical structure, necessitating additional tools to determine the causes of failure. In this article, the author presents results indicating that STEM EBIC, with the new SEEBIC mode, can provide electronic contrast that complements the physical-based contrast of STEM imaging. By identifying device features at higher risk of failure, the two methods may open a path to predictive failure analysis.

The 42nd International Symposium for Testing and Failure Analysis (ISTFA 2016) was held in Fort Worth, Texas, November 6-10, 2016. This article provides a summary of the keynote presentation, technical program, panel discussion, tutorials, and User’s Group meetings.

Scanning microwave impedance microscopy is a nearfield technique using microwaves to probe the electrical properties of materials with nanoscale lateral resolution.

New materials integration and improved design can be promoted by using atom probe tomography (APT) as an analysis technique. This article provides an overview of APT principles and setups and provides diverse examples that focus on its use to characterize electronic devices.

This article discusses the primary differences between electrostatic discharge (ESD) and electrical overstress (EOS) and the circumstances under which they occur. It also explains how to differentiate ESD from EOS during failure analysis and how to avoid common misunderstandings and mistakes.

Trapped ion systems are one of the leading technology platforms for quantum computing. This article describes the construction and operation of ion trap devices and the various modes of failure that have been observed. Examples of failure in either the rendering or use of packaged trap chips are presented, including electrode shorts and opens, detached bond wires, and RF breakdown damage.