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Journal Articles
Advantages and Challenges of 3-D Atom Probe Tomography Characterization of FinFETs
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EDFA Technical Articles (2017) 19 (2): 22–30.
Published: 01 May 2017
...Andrew J. Martin; Ajay Kumar Kambham; Ahmad D. Katnani This article provides an overview of atom probe tomography (APT) and its use in semiconductor FA and new product development. It discusses the basic components in an atom probe, the making of APT tips, and the general approach for data...
Abstract
View articletitled, Advantages and Challenges of 3-D <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span> <span class="search-highlight">Tomography</span> Characterization of FinFETs
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for article titled, Advantages and Challenges of 3-D <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span> <span class="search-highlight">Tomography</span> Characterization of FinFETs
This article provides an overview of atom probe tomography (APT) and its use in semiconductor FA and new product development. It discusses the basic components in an atom probe, the making of APT tips, and the general approach for data collection and reconstruction. It also includes a case study in which 3D atom probe techniques are used to map dopant profiles and identify defects in the source-drain region of SiGe FinFET transistors.
Journal Articles
Advanced Characterization of Materials Using Atom Probe Tomography
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EDFA Technical Articles (2024) 26 (1): 14–21.
Published: 01 February 2024
...Jacob M. Garcia; Ann N. Chiaramonti New materials integration and improved design can be promoted by using atom probe tomography (APT) as an analysis technique. This article provides an overview of APT principles and setups and provides diverse examples that focus on its use to characterize...
Abstract
View articletitled, Advanced Characterization of Materials Using <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span> <span class="search-highlight">Tomography</span>
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for article titled, Advanced Characterization of Materials Using <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span> <span class="search-highlight">Tomography</span>
New materials integration and improved design can be promoted by using atom probe tomography (APT) as an analysis technique. This article provides an overview of APT principles and setups and provides diverse examples that focus on its use to characterize electronic devices.
Journal Articles
Analysis of Electronic Devices with a Three-Dimensional Atom Probe
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EDFA Technical Articles (2013) 15 (4): 4–11.
Published: 01 November 2013
...Sergej Mutas This article discusses the basic procedures involved in atom probe tomography (APT) and demonstrates its use on complex material stacks. Although still a relatively new technique, APT has moved to the forefront of semiconductor failure analysis because it can provide 3D chemical...
Abstract
View articletitled, Analysis of Electronic Devices with a Three-Dimensional <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span>
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for article titled, Analysis of Electronic Devices with a Three-Dimensional <span class="search-highlight">Atom</span> <span class="search-highlight">Probe</span>
This article discusses the basic procedures involved in atom probe tomography (APT) and demonstrates its use on complex material stacks. Although still a relatively new technique, APT has moved to the forefront of semiconductor failure analysis because it can provide 3D chemical composition of a wide range of materials on a near-atomic scale.
Journal Articles
Scanning Capacitance Microscopy (SCM) Applications in Failure Analysis
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EDFA Technical Articles (2011) 13 (4): 14–19.
Published: 01 November 2011
..., Phys. Rev. Lett., 2002, 89, p. 25502. 11. K. Thompson, P.L. Flaitz, P. Ronsheim, D.J. Larson, and T.F. Kelly: Imaging of Arsenic Cottrell Atmospheres Around Silicon Defects by Three-Dimensional Atom Probe Tomography, Science, 2007, 317(5843), pp. 1370-74. 12. K. Thompson, J.H. Bunton, T.F. Kelly...
Abstract
View articletitled, Scanning Capacitance Microscopy (SCM) Applications in Failure Analysis
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for article titled, Scanning Capacitance Microscopy (SCM) Applications in Failure Analysis
Scanning capacitance microscopy (SCM) has proven to be an effective tool for investigating doping-related failure mechanism in ICs. The examples in this article show how the author used SCM to solve various problems including premature breakdown due to pattern misalignment, threshold voltage variations caused by poly gate doping anomalies, and source-drain leakage due to channeling effects.
Journal Articles
A Short Summary of the First Chips Metrology Workshop on Failure Analysis and Reliability Testing
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EDFA Technical Articles (2024) 26 (2): 2–43.
Published: 01 May 2024
... challenges such as atom probe tomography and time-resolved emission microscopy. It became clear to me that NIST scientists showed a strong interest in learning more about FA challenges. This presents a unique opportunity for the FA community to collaborate with NIST in defining projects for a second round...
Abstract
View articletitled, A Short Summary of the First Chips Metrology Workshop on Failure Analysis and Reliability Testing
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for article titled, A Short Summary of the First Chips Metrology Workshop on Failure Analysis and Reliability Testing
The goals of the workshop were twofold: Give NIST researchers an industry perspective and evaluate the CHIPS Act Metrology R&D program industry relevance to plan to future projects. This guest editorial provides a brief overview of the February 2024 workshop and its outcomes.
Journal Articles
Electrical Characterizations Based on AFM: SCM and SSRM Measurements with a Multidimensional Approach
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EDFA Technical Articles (2022) 24 (3): 24–31.
Published: 01 August 2022
... distribution, the most accurate quantitative analysis method is secondary ion mass spectrometry (SIMS). For 3D tomography, time of flight secondary ion mass spectrometry (TOF-SIMS) can be deployed. Atom probe tomography (APT or 3D atom probe) also provides chemical composition with high mass resolution and ppm...
Abstract
View articletitled, Electrical Characterizations Based on AFM: SCM and SSRM Measurements with a Multidimensional Approach
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for article titled, Electrical Characterizations Based on AFM: SCM and SSRM Measurements with a Multidimensional Approach
This article demonstrates the value of atomic force microscopes, particularly the different electrical modes, for characterizing complex microelectronic structures. It presents experimental results obtained from deep trench isolation (DTI) structures using SCM and SSRM analysis with emphasis on the voltage applied by the AFM. From these measurements, a failure analysis workflow is proposed that facilitates AFM voltage optimization to reveal the structure of cross-sectioned samples, make comparisons, and determine the underlying cause of failures.
Journal Articles
Sixth FIB-SEM Workshop
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EDFA Technical Articles (2014) 16 (1): 18–23.
Published: 01 February 2014
... to an electropolished stub compatible with a Fischione on-axis tomography holder. The TEM sample is rough-cut to position the grain boundary near the end of the sample and then annular milled to shape the atom probe specimen. This procedure produces samples with a grain boundary near the tip, on a sample stub suitable...
Abstract
View articletitled, Sixth FIB-SEM Workshop
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for article titled, Sixth FIB-SEM Workshop
The sixth FIB-SEM workshop was held March 1, 2013, in Cambridge, Mass. This article provides a summary of the event along with highlights from the 18 paper presentations.
Journal Articles
Four-Dimensional Scanning Transmission Electron Microscopy: Part III, Ptychography
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EDFA Technical Articles (2024) 26 (4): 4–11.
Published: 01 November 2024
... Sciences: The Development of Z-Contrast and EFTEM Tomography, Ultramicroscopy, 2003, 96(3), p. 413-431. 44. W. Van den Broek, et al.: Correction of Non-Linear Thickness Effects in HAADF STEM Electron Tomography, Ultramicroscopy, 2012, 116, p. 8-12. 45. D.J. Chang, et al.: Ptychographic Atomic Electron...
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View articletitled, Four-Dimensional Scanning Transmission Electron Microscopy: Part III, Ptychography
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for article titled, Four-Dimensional Scanning Transmission Electron Microscopy: Part III, Ptychography
Four-dimensional scanning transmission electron microscopy (4D-STEM) is a spatially resolved electron diffraction technique that records the electron scattering distribution at each point of the electron beam raster, thereby producing a four-dimensional dataset. The final article in this series covers ptychography, a form of computational imaging that recovers the phase information imparted to an electron beam as it interacts with a specimen.
Journal Articles
EUFANET Workshop 2012 Report
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EDFA Technical Articles (2013) 15 (3): 20–23.
Published: 01 August 2013
... integration, such as throughsilicon vias (TSVs), and also described the limits and requirements for future integration challenges. unique information regarding the interfaces between the various material layers were obtained. The 3-D atom probe has repeatedly proven its capability to obtain reproducible...
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View articletitled, EUFANET Workshop 2012 Report
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for article titled, EUFANET Workshop 2012 Report
The third extended European Failure Analysis Network (EUFANET) workshop, “Smart FA for New Materials in Electronic Devices,” was held in Dresden, Germany, September 17-18, 2012. This article provides a summary of the event with highlights from presentations on flexible organic electronics, crystal defects in SiC, nanoprobing, and the capabilities of nano X-ray tomography.
Journal Articles
Variations on FIB in situ Lift-Out for TEM Sample Preparation
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EDFA Technical Articles (2011) 13 (3): 18–26.
Published: 01 August 2011
... for presenting a sample for TEM tomography and atom probe analysis. In summary, today s port-mounted nanomanipulators with closed-loop feedback control and a rotation axis enable efficient sample repositioning. This repositioning is achieved by implementing a combined stage and probe (CSP) reorientation method...
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View articletitled, Variations on FIB in situ Lift-Out for TEM Sample Preparation
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for article titled, Variations on FIB in situ Lift-Out for TEM Sample Preparation
This article discusses the practice of FIB-based in situ lift-out, a sample preparation method that has proven particularly useful for failure analysis. It explains how samples are now being made for a wide range of TEM techniques, including holography, tomography, high-angle annular dark-field scanning, and electron energy-loss spectroscopy. In most cases, achieving optimal quality requires the use of alternate FIB milling angles, as in plan-view, sideways, and backside milling, all of which are discussed.
Journal Articles
Making Connections: Challenges and Opportunities for In Situ TEM Biasing
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EDFA Technical Articles (2023) 25 (1): 4–8.
Published: 01 February 2023
... in Tungsten via Atom Probe Tomography, Ultramicroscopy, Vol. 228, p. 113334, Sep. 2021, doi: 10.1016/j.ultramic.2021.113334. 5. A. Zintler, et al.: FIB based Fabrication of TiN Device for Resistive Switching inside a an Operative Transmission PEtle/HctfrOo2n/ Microscope, Ultramicroscopy, Vol. 181, p. 144...
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View articletitled, Making Connections: Challenges and Opportunities for In Situ TEM Biasing
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for article titled, Making Connections: Challenges and Opportunities for In Situ TEM Biasing
This article discusses sample preparation challenges that have impeded progress in producing bias-enabled TEM samples from electronic components, as well as strategies to mitigate these issues.
Journal Articles
Four-Dimensional Scanning Transmission Electron Microscopy: Part I: Imaging, Strain Mapping, and Defect Detection
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EDFA Technical Articles (2023) 25 (3): 12–22.
Published: 01 August 2023
... Resolution, Ultramicroscopy, 2011, 111(8), p. 1111-1116. 17. Z. Chen, et al.: Practical Aspects of Diffractive Imaging using an Atomic-scale Coherent Electron Probe, Ultramicroscopy, 2016, 169, p. 107-121. 18. J.M. LeBeau, et al.: Quantitative Comparisons of Contrast in Experimental and Simulated Bright...
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View articletitled, Four-Dimensional Scanning Transmission Electron Microscopy: Part I: Imaging, Strain Mapping, and Defect Detection
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for article titled, Four-Dimensional Scanning Transmission Electron Microscopy: Part I: Imaging, Strain Mapping, and Defect Detection
Four-dimensional scanning transmission electron microscopy (4D-STEM) is a spatially resolved electron diffraction technique that records the electron scattering distribution at each sampling point. 4D-STEM provides researchers with information that can be analyzed in a multitude of ways to characterize a sample’s structure, including imaging, strain measurement, and defect analysis. This article introduces the basics of the technique and some areas of application with an emphasis on semiconductor materials.
Journal Articles
ISTFA 2013 User's Groups Summaries
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EDFA Technical Articles (2014) 16 (1): 31–48.
Published: 01 February 2014
...-and-answer panel session. The presentations covered a range of important industry topics, including the latest in TEM preparation techniques (in situ and ex situ), improving sputtering yield through incidence angle changes, novel chemistry, and atom probe sample creation. The presenters for the 2013 User s...
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View articletitled, ISTFA 2013 User's Groups Summaries
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for article titled, ISTFA 2013 User's Groups Summaries
This article compiles summaries of User Group meetings held at ISTFA 2013, including the Contactless Fault Isolation User’s Group, the Focused Ion Beam User’s Group, the Sample Prep/3D Package User’s Group, and the Nanoprobing User’s Group. For each meeting, a brief synopsis of the presentations and subsequent dialog is provided.
Journal Articles
An X-Ray Tomography Primer
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EDFA Technical Articles (2005) 7 (1): 26–32.
Published: 01 February 2005
... of approximately 13% is favored for application to tomography on theoretical grounds,[2] although the minimum is broad. The x-rays, here assumed to be monochromatic, are sent through the sample. Typically, they are imaged onto an array of detectors, although a scanning probe with a single channel detector may also...
Abstract
View articletitled, An X-Ray <span class="search-highlight">Tomography</span> Primer
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for article titled, An X-Ray <span class="search-highlight">Tomography</span> Primer
X-ray tomography has been rapidly gaining acceptance in the semiconductor industry since the first demonstration of its use on IC interconnect in 1999. As failure analysts are discovering, X-ray imaging is more powerful than visible light microscopy and can be used to analyze larger samples than those that fit in an electron microscope. This article provides an introduction to the physics, signal processing, and algorithms involved in X-ray imaging and tomography and the factors that affect resolution.
Journal Articles
ISTFA 2011 User’s Group Summaries
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EDFA Technical Articles (2012) 14 (1): 27–31.
Published: 01 February 2012
..., etc.) to failures that are physically challenging and need specialized tools for localization (atomic force probe, e-beam, passive voltage contrast, scanning probe microscopy, etc The message Vijay shared with the failure analysis (FA) community is that invisible failures must be inferred through...
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View articletitled, ISTFA 2011 User’s Group Summaries
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for article titled, ISTFA 2011 User’s Group Summaries
This article provides a summary of each of the four User’s Group meetings that took place at ISTFA 2011. The summaries cover key participants, presentation topics, and discussion highlights from each of the following groups: Group 1, Focused Ion Beam; Group 2, 3D Packaging and Failure Analysis; Group 3, Finding the Invisible Defect; and Group 4, Nanoprobing and Electrical Characterization.
Journal Articles
Nanoelectronics Failure Analysis
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EDFA Technical Articles (2003) 5 (2): 5–9.
Published: 01 May 2003
.... They have also been used in nanomanipulation of individual atoms and for very localized oxidation. Clearly such manual techniques are not tractable for mass production of millions of devices; however, arrays of scanning probes are in development that might provide a more parallel alternative. Top-down...
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View articletitled, Nanoelectronics Failure Analysis
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for article titled, Nanoelectronics Failure Analysis
This article discusses the emergence of nanoelectronics and the effect it may have on semiconductor testing and failure analysis. It describes the different types of quantum effect and molecular electronic devices that have been produced, explaining how they are made, how they work, and the changes that may be required to manufacture and test these devices at scale.
Journal Articles
Four-Dimensional Scanning Transmission Electron Microscopy: Part II, Crystal Orientation and Phase, Short and Medium Range Order, and Electromagnetic Fields
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EDFA Technical Articles (2024) 26 (1): 4–13.
Published: 01 February 2024
... of Medium Range Ordering and CLaryysetraDlleizpaotisoitnioonf,A mAPoLrpMhaotuersiaTlisO, 22U02lt3ra, 1th1i(n1)F.ilms Grown by Atomic 34. J. Hwang and P.M. Voyles: Variable Resolution Fluctuation Electron Microscopy on Cu-Zr Metallic Glass using a Wide Range of Coherent STEM Probe Size, Microscopy...
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View articletitled, Four-Dimensional Scanning Transmission Electron Microscopy: Part II, Crystal Orientation and Phase, Short and Medium Range Order, and Electromagnetic Fields
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for article titled, Four-Dimensional Scanning Transmission Electron Microscopy: Part II, Crystal Orientation and Phase, Short and Medium Range Order, and Electromagnetic Fields
Four-dimensional scanning transmission electron microscopy (4D-STEM) is a spatially resolved electron diffraction technique that records the electron scattering distribution at each point of the electron beam raster, thereby producing a four-dimensional dataset. This second installment of this series presents applications of 4D-STEM, including measurements of crystal orientation and phase, short- and medium-range order, and internal electromagnetic fields.
Journal Articles
Failure Analysis of DC/DC Converters: A Case Study
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EDFA Technical Articles (2017) 19 (4): 4–9.
Published: 01 November 2017
...Jérémie Dhennin In this case study, the author describes the investigation of a defective DC-DC converter retrieved from an aircraft following the report of abnormal system behavior. Electrical testing, local probing, X-ray imaging, and cross-sectional analysis led to the discovery of cracks...
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View articletitled, Failure Analysis of DC/DC Converters: A Case Study
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for article titled, Failure Analysis of DC/DC Converters: A Case Study
In this case study, the author describes the investigation of a defective DC-DC converter retrieved from an aircraft following the report of abnormal system behavior. Electrical testing, local probing, X-ray imaging, and cross-sectional analysis led to the discovery of cracks on several pins and in some of the solder material. The cracks were caused by different rates of thermal expansion and were remedied with the help of thermomechanical analysis, EBSD imaging, and phase map comparisons for thick and thin solder joints.
Journal Articles
Transforming an Industry: An Inventor’s Tale of FIB In Situ Lift-Out
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EDFA Technical Articles (2023) 25 (1): 20–27.
Published: 01 February 2023
... and transfer it to a support for atom probe analysis, all using only the e-beam.[24] Omniprobe also developed customized lift-out recipes for emerging applications, such as sample preparation for MEMS in situ holders. In 2011, I developed a patented cryo lift-out solution. By 2016, it was fully commercialized...
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View articletitled, Transforming an Industry: An Inventor’s Tale of FIB In Situ Lift-Out
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for article titled, Transforming an Industry: An Inventor’s Tale of FIB In Situ Lift-Out
This is the story of how the mainstream Omniprobe FIB lift-out solution was invented and delivered to the market.
Journal Articles
Probing the Future of Failure Analysis
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EDFA Technical Articles (2002) 4 (4): 5–9.
Published: 01 November 2002
... sized defects versus time. Diverging trends indicate increasing difficulty in isolating faults. A very promising alternative for high atomic number materials is X-rays. An emerging technique known as X-ray tomography (XRT) combines the material dependent contrast of X-ray microscopy with precision...
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View articletitled, <span class="search-highlight">Probing</span> the Future of Failure Analysis
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for article titled, <span class="search-highlight">Probing</span> the Future of Failure Analysis
A review of the 2001 edition of the International Technology Roadmap for Semiconductors indicates major obstacles ahead. Of the three basic failure analysis steps—inspection, deprocessing, and fault isolation—the latter is the most at risk, especially physical fault isolation.
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