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Journal Articles
Ebook Preview: STEM-in-SEM Imaging Techniques for Microelectronics Failure Analysis
Available to Purchase
EDFA Technical Articles (2020) 22 (1): 26–27.
Published: 01 February 2020
...Jason D. Holm; Benjamin W. Caplins This article describes an ebook titled STEM-in-SEM: Introduction to Scanning Transmission Electron Microscopy for Microelectronics Failure Analysis , intended as an introductory tutorial for those with little or no transmission imaging experience and as a source...
Abstract
View articletitled, Ebook Preview: STEM-in-<span class="search-highlight">SEM</span> <span class="search-highlight">Imaging</span> Techniques for Microelectronics Failure Analysis
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for article titled, Ebook Preview: STEM-in-<span class="search-highlight">SEM</span> <span class="search-highlight">Imaging</span> Techniques for Microelectronics Failure Analysis
This article describes an ebook titled STEM-in-SEM: Introduction to Scanning Transmission Electron Microscopy for Microelectronics Failure Analysis , intended as an introductory tutorial for those with little or no transmission imaging experience and as a source of ideas for SEM users looking to expand the imaging and diffraction capabilities of their equipment.
Journal Articles
3-D Analysis of a Copper Flip-Chip Interconnection Using FIB-SEM Slice and View
Available to Purchase
EDFA Technical Articles (2016) 18 (1): 14–20.
Published: 01 February 2016
...Mototaka Ito; Jun Kato A detailed analysis based on FIB etching and SEM image capture was conducted on a flip-chip solder joint deep inside a tablet PC. 3D views reconstructed from SEM images show what appears to be a copper pillar with a solder cap connected to a copper trace on the substrate...
Abstract
View articletitled, 3-D Analysis of a Copper Flip-Chip Interconnection Using FIB-<span class="search-highlight">SEM</span> Slice and View
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for article titled, 3-D Analysis of a Copper Flip-Chip Interconnection Using FIB-<span class="search-highlight">SEM</span> Slice and View
A detailed analysis based on FIB etching and SEM image capture was conducted on a flip-chip solder joint deep inside a tablet PC. 3D views reconstructed from SEM images show what appears to be a copper pillar with a solder cap connected to a copper trace on the substrate. The investigators believe the joint was formed by thermal compression bonding with a preapplied underfill. The analysis also revealed the presence of voids and intermetallic compounds along with signs of filler entrapment.
Journal Articles
Breaking the Resolution Barrier in the Scanning Electron Microscope
Available to Purchase
EDFA Technical Articles (2004) 6 (4): 32–40.
Published: 01 November 2004
...William Vanderlinde This article describes two innovative methods that can significantly improve the resolution of SEM imaging: scanning transmission electron microscopy in a scanning electron microscope (STEM-in-SEM) and forward-scattered electron imaging (FSEI). Both methods can be implemented...
Abstract
View articletitled, Breaking the Resolution Barrier in the Scanning Electron Microscope
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for article titled, Breaking the Resolution Barrier in the Scanning Electron Microscope
This article describes two innovative methods that can significantly improve the resolution of SEM imaging: scanning transmission electron microscopy in a scanning electron microscope (STEM-in-SEM) and forward-scattered electron imaging (FSEI). Both methods can be implemented in any SEM using special sample holders. No other modifications are required. Test results presented in the article show that 1 to 2 nm resolution is possible in thin sections, uncoated polysilicon gates, and photoresist.
Journal Articles
Supervised Feature Extraction and Synthesis of Integrated Circuits Micrographs for Physical Assurance
Available to Purchase
EDFA Technical Articles (2022) 24 (3): 12–22.
Published: 01 August 2022
...Md. Mahfuz Al Hasan; Md. Tahsin Mostafiz; Navid Asadizanjani This article proposes a design for a real-time Trojan detection system and explores possible solutions to the challenge of large-scale SEM image acquisition. One such solution, a deep-learning approach that generates synthetic micrographs...
Abstract
View articletitled, Supervised Feature Extraction and Synthesis of Integrated Circuits Micrographs for Physical Assurance
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for article titled, Supervised Feature Extraction and Synthesis of Integrated Circuits Micrographs for Physical Assurance
This article proposes a design for a real-time Trojan detection system and explores possible solutions to the challenge of large-scale SEM image acquisition. One such solution, a deep-learning approach that generates synthetic micrographs from layout images, shows significant promise. Learning-based approaches are also used to both synthesize and classify cells. The classification outcome is matched with the design exchange format file entry to ensure the purity of the underlying IC.
Journal Articles
Nanoprobing at Low Beam Energy, Addressing Current and Future Nodes
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EDFA Technical Articles (2022) 24 (2): 12–15.
Published: 01 May 2022
...Andreas Rummel; Andrew Jonathan Smith This article discusses the challenges associated with nanoprobing advanced technology node devices and explains how to optimize SEM images for beam voltages of 100 eV or less. This article discusses the challenges associated with nanoprobing advanced...
Abstract
View articletitled, Nanoprobing at Low Beam Energy, Addressing Current and Future Nodes
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for article titled, Nanoprobing at Low Beam Energy, Addressing Current and Future Nodes
This article discusses the challenges associated with nanoprobing advanced technology node devices and explains how to optimize SEM images for beam voltages of 100 eV or less.
Journal Articles
Theory of SEM Voltage Contrast and Applications to IC Failure Analysis
Available to Purchase
EDFA Technical Articles (2001) 3 (3): 15–18.
Published: 01 August 2001
...Valluri Rao Voltage contrast, a phenomenon that occurs in scanning electron microscopes, produces brightness variations in SEM images that correspond to potential variations on the test sample. Through appropriate processing, voltage contrast signals can reveal an extensive amount of information...
Abstract
View articletitled, Theory of <span class="search-highlight">SEM</span> Voltage Contrast and Applications to IC Failure Analysis
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for article titled, Theory of <span class="search-highlight">SEM</span> Voltage Contrast and Applications to IC Failure Analysis
Voltage contrast, a phenomenon that occurs in scanning electron microscopes, produces brightness variations in SEM images that correspond to potential variations on the test sample. Through appropriate processing, voltage contrast signals can reveal an extensive amount of information about the functionality of ICs. Voltage contrast can be used, for example, to map electrical logic levels and timing waveforms from internal nodes of the chip as it operates inside the SEM chamber. This article describes the fundamentals of voltage contrast and its applications in IC failure analysis.
Journal Articles
A Sample Preparation Workflow for Delayering a 45 nm Node Serial Peripheral Interface Module
Available to Purchase
EDFA Technical Articles (2021) 23 (4): 4–13.
Published: 01 November 2021
... imaging and subsequent feature extraction. By combining polygon sets representing each layer, the full design of the device was reconstructed as shown in one of the images. Further development of SEM-based feature extraction tools for design validation and failure analysis is contingent on reliable...
Abstract
View articletitled, A Sample Preparation Workflow for Delayering a 45 nm Node Serial Peripheral Interface Module
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for article titled, A Sample Preparation Workflow for Delayering a 45 nm Node Serial Peripheral Interface Module
Further development of SEM-based feature extraction tools for design validation and failure analysis is contingent on reliable sample preparation methods. This article describes how a delayering framework for 130 nm technology was adapted and used on a 45 nm SPI module consisting of 11 metal layers, 10 via layers, two layers of polysilicon, and an active silicon layer. It explains how different polishing and etching methods are used to expose each layer with sufficient contrast for SEM imaging and subsequent feature extraction. By combining polygon sets representing each layer, the full design of the device was reconstructed as shown in one of the images.
Journal Articles
Mechanical Milling and Polishing of Cross Sections using a Micro CNC Machine for Failure Analysis
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EDFA Technical Articles (2020) 22 (1): 14–19.
Published: 01 February 2020
..., and clearly illustrate the differences. SEM images of a manually polished sample show process-induced cracking, chipping, and delamination at the die-C4 interface. In contrast, the CNC-milled sample is artifact-free and the C4 bumps are uniformly exposed along the entire length of the cross-section...
Abstract
View articletitled, Mechanical Milling and Polishing of Cross Sections using a Micro CNC Machine for Failure Analysis
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for article titled, Mechanical Milling and Polishing of Cross Sections using a Micro CNC Machine for Failure Analysis
In this article, the authors evaluate micro CNC milling as an alternative to manual parallel lapping for mechanical cross-sectioning of flip-chip packaged samples. They describe both processes, and how they compare to other cross-sectioning techniques, and clearly illustrate the differences. SEM images of a manually polished sample show process-induced cracking, chipping, and delamination at the die-C4 interface. In contrast, the CNC-milled sample is artifact-free and the C4 bumps are uniformly exposed along the entire length of the cross-section.
Journal Articles
Full Chip Backside Delayering of 10 nm Node Integrated Circuits with Chemically Assisted Focused Ion Beam Deprocessing
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EDFA Technical Articles (2025) 27 (1): 3–7.
Published: 01 February 2025
... advantage of chemically assisted focused ion beam processing with ultraviolet spectroscopy to destructively delayer integrated circuits starting from the shallow trench isolation layer, enabling high-resolution SEM imaging at each layer. Copyright © ASM International® 2025 2025 ASM International...
Abstract
View articletitled, Full Chip Backside Delayering of 10 nm Node Integrated Circuits with Chemically Assisted Focused Ion Beam Deprocessing
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for article titled, Full Chip Backside Delayering of 10 nm Node Integrated Circuits with Chemically Assisted Focused Ion Beam Deprocessing
Advanced 10 nm device delayering is a critical process for verifying and validating the circuit design layout and extracting the structures buried inside the chip. The work featured in this article takes advantage of chemically assisted focused ion beam processing with ultraviolet spectroscopy to destructively delayer integrated circuits starting from the shallow trench isolation layer, enabling high-resolution SEM imaging at each layer.
Journal Articles
Voltage Contrast within Electron Microscopy: From a Curious Effect to Debugging Modern ICs
Available to Purchase
EDFA Technical Articles (2023) 25 (4): 28–34.
Published: 01 November 2023
..., routinely inspect devices extracted from modern ICs, and can resolve, for instance, the lattice of silicon atoms that form transistor channels. Meanwhile, scanning electron microscopes (SEMs) and focused-ion beam (FIB) microscopes routinely image IC features with low-nanometer resolution. Nanoscale features...
Abstract
View articletitled, Voltage Contrast within Electron Microscopy: From a Curious Effect to Debugging Modern ICs
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for article titled, Voltage Contrast within Electron Microscopy: From a Curious Effect to Debugging Modern ICs
A scanning electron microscope system measures voltage contrast on device-under-test surfaces. This article addresses a limited set of applications that rely on voltage contrast (VC) measurements in SEM systems, showing how VC measurements can probe electrical activity running at speeds as high as 2 GHz on modern active integrated circuits.
Journal Articles
Innovative Puck Design for the Mechanical Cross-Sectioning and Subsequent Analysis of Semiconductor Packaged Samples in Failure Analysis
Available to Purchase
EDFA Technical Articles (2020) 22 (2): 4–12.
Published: 01 May 2020
... brings attention to some of the drawbacks with the current approach and presents a solution in the form of a redesigned puck. As test results show, the new puck significantly reduces polishing time, and when cast with a conductive epoxy, minimizes charging artifacts and image distortion during SEM...
Abstract
View articletitled, Innovative Puck Design for the Mechanical Cross-Sectioning and Subsequent Analysis of Semiconductor Packaged Samples in Failure Analysis
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for article titled, Innovative Puck Design for the Mechanical Cross-Sectioning and Subsequent Analysis of Semiconductor Packaged Samples in Failure Analysis
The causes of failure in flip-chip packaged devices are often found at the interface between the die and package. Exposing the site of interest usually entails some form of mechanical cross-sectioning with the sample embedded in an epoxy puck. This article brings attention to some of the drawbacks with the current approach and presents a solution in the form of a redesigned puck. As test results show, the new puck significantly reduces polishing time, and when cast with a conductive epoxy, minimizes charging artifacts and image distortion during SEM analysis. It also facilitates easy sample removal for subsequent analysis.
Journal Articles
SRAM Physical Failure Analysis Challenges in Technology Nodes Beyond 14 nm
Available to Purchase
EDFA Technical Articles (2020) 22 (3): 4–7.
Published: 01 August 2020
... of the continuous downscaling of technology nodes. Of particular interest to failure analysis engineers is the ability to determine the root cause of defect mechanisms that may have physical characteristics beyond the imaging resolution limits of current scanning electron microscopy (SEM) toolsets...
Abstract
View articletitled, SRAM Physical Failure Analysis Challenges in Technology Nodes Beyond 14 nm
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for article titled, SRAM Physical Failure Analysis Challenges in Technology Nodes Beyond 14 nm
Three case studies involving 14 nm SRAM technology show how progressive FIB cross-sectioning and top-down analysis can be supplemented with nanoprobing and TEM tomography to determine the root cause of failure. In the first case, the memory failure is traced to an abnormal gate profile. In the second case, the failure is attributed to a metal line short, and in the third case, a gate defect.
Journal Articles
Detection of Gate Oxide Defects Using Electrochemical Wet Etching in KOH:H 2 O Solution
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EDFA Technical Articles (1998) 1 (1): 8–11.
Published: 01 November 1998
... technique for detecting gate oxide defects is described. This method is based on chemical and electrochemical wet etching of Si in KOH:H2O. KOH:H2O is well known as a solution for Si etching by the following chemical reaction: Si + 20H- + H2O ¨ SiO32- + 2H2 (1) Fig. 1: SEM cross sectional image of Si...
Abstract
View articletitled, Detection of Gate Oxide Defects Using Electrochemical Wet Etching in KOH:H 2 O Solution
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for article titled, Detection of Gate Oxide Defects Using Electrochemical Wet Etching in KOH:H 2 O Solution
A new way to detect gate oxide defects has been developed. The method, as the article explains, is based on wet chemical etching and is particularly effective for devices with floating gates. Test samples with exposed poly-Si gates are placed in a KOH:H 2 O solution and a voltage is applied to the silicon substrate. At a certain voltage, normal gates begin to etch, while those shorted to the substrate through gate oxide defects develop an anodic oxide and thus remain unetched. This method has proven effective in assessing gate oxide integrity without direct observation of the oxide, which requires complicated deprocessing and a lot of time. It also reveals electrical characteristics of gate oxides that are difficult to identify by conventional physical analysis.
Journal Articles
Large Area Automated Deprocessing of Integrated Circuits: Present and Future
Available to Purchase
EDFA Technical Articles (2019) 21 (3): 8–14.
Published: 01 August 2019
... of advancements in gas-assisted etching, ion source alternatives, compact spectroscopy, and high-speed lasers. Copyright © ASM International® 2019 2019 ASM International automated IC deprocessing large area delayering plasma FIB SEM imaging spectroscopy 8 httpsdoi.org/10.31399/asm.edfa.2019-3...
Abstract
View articletitled, Large Area Automated Deprocessing of Integrated Circuits: Present and Future
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for article titled, Large Area Automated Deprocessing of Integrated Circuits: Present and Future
This article discusses the current state of large area integrated circuit deprocessing, the latest achievements in the development of automated deprocessing equipment, and the potential impact of advancements in gas-assisted etching, ion source alternatives, compact spectroscopy, and high-speed lasers.
Journal Articles
A Brief Overview of Scanning Transmission Electron Microscopy in a Scanning Electron Microscope
Available to Purchase
EDFA Technical Articles (2021) 23 (4): 18–26.
Published: 01 November 2021
...Jason Holm This article provides a brief overview of STEM-in-SEM, discussing the pros and cons, recent advancements in detector technology, and the emergence of 4D STEM-in-SEM, a relatively new method that uses diffraction patterns recorded at different raster positions to enhance images offline...
Abstract
View articletitled, A Brief Overview of Scanning Transmission Electron Microscopy in a Scanning Electron Microscope
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for article titled, A Brief Overview of Scanning Transmission Electron Microscopy in a Scanning Electron Microscope
This article provides a brief overview of STEM-in-SEM, discussing the pros and cons, recent advancements in detector technology, and the emergence of 4D STEM-in-SEM, a relatively new method that uses diffraction patterns recorded at different raster positions to enhance images offline in selected regions of interest.
Journal Articles
Advanced Defect Isolation Utilizing Image Intensity Analysis
Available to Purchase
EDFA Technical Articles (2007) 9 (2): 14–18.
Published: 01 May 2007
.... However, inspection of that area with conventional techniques, such as secondary electron and backscattered electron (BSE) scanning electron microscopy (SEM), does not always lead to physical defects being readily apparent in the images obtained. In part, this is due to the human eye being inherently...
Abstract
View articletitled, Advanced Defect Isolation Utilizing <span class="search-highlight">Image</span> Intensity Analysis
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for article titled, Advanced Defect Isolation Utilizing <span class="search-highlight">Image</span> Intensity Analysis
Image enhancement has proven helpful for locating defects in ICs. This article discusses two image analysis techniques, image comparison and intensity profiling, and shows how they reveal defects that would otherwise be missed.
Journal Articles
MEMS Failure Analysis Engineer’s Toolbox (Part 1)
Available to Purchase
EDFA Technical Articles (2000) 2 (3): 4–7.
Published: 01 August 2000
... connections are more susceptible to failure than others. Video footage of operating engines can track the performance of micromachines during operating life tests6. Fig. 3: SEM image showing a thin 100 Å layer of silicon reduced tungsten conformal coating around all sides of a section of structural...
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View articletitled, MEMS Failure Analysis Engineer’s Toolbox (Part 1)
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for article titled, MEMS Failure Analysis Engineer’s Toolbox (Part 1)
Experiments to assess microelectromechanical systems (MEMS) test their functionality and materials properties. These experiments provide knowledge and insight into MEMS failure modes and potential pathways to improve the lifetime of MEMS devices. This article demonstrates the use of optical microscopy and SEM analysis to determine various causes of failure in MEMS devices.
Journal Articles
Failure Analysis of DC/DC Converters: A Case Study
Available to Purchase
EDFA Technical Articles (2017) 19 (4): 4–9.
Published: 01 November 2017
..., a cross section was performed with optical (Fig. 7) and scanning electron microscopy (SEM) imaging (Fig. 8). A crack was confirmed under one pin. The other side of the component was not affected. The solder material thickness between the pin and the pad was found to be very low. The SEM observation showed...
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View articletitled, Failure Analysis of DC/DC Converters: A Case Study
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for article titled, Failure Analysis of DC/DC Converters: A Case Study
In this case study, the author describes the investigation of a defective DC-DC converter retrieved from an aircraft following the report of abnormal system behavior. Electrical testing, local probing, X-ray imaging, and cross-sectional analysis led to the discovery of cracks on several pins and in some of the solder material. The cracks were caused by different rates of thermal expansion and were remedied with the help of thermomechanical analysis, EBSD imaging, and phase map comparisons for thick and thin solder joints.
Journal Articles
SEM for General Purpose Failure Analysis: "Little Used but Very Useful"
Available to Purchase
EDFA Technical Articles (1999) 1 (3): 21–24.
Published: 01 August 1999
... examples of the various ways they can be used. Copyright © ASM International® 1999 1999 ASM International backscattering charging emissive imaging scanning electron microscopes voltage contrast httpsdoi.org/10.31399/asm.edfa.1999-3.p021 SEM SEM for General Purpose Failure Analysis: Little...
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View articletitled, <span class="search-highlight">SEM</span> for General Purpose Failure Analysis: "Little Used but Very Useful"
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for article titled, <span class="search-highlight">SEM</span> for General Purpose Failure Analysis: "Little Used but Very Useful"
Scanning electron microscopes can be used to analyze almost anything that conducts electricity and is prone to failure, including relays, coils, inductors, capacitors, resistors, transistors, diodes, IGBTS, MOSFETS, and hybrid circuits. As the author of the article explains, SEMs are one of the most versatile tools for failure analysis if used to the full extent of their capabilities. Their operating modes include emissive imaging, backscattering, voltage contrast, EBIC or specimen current, and conductivity resistive mapping. The author describes each operating mode and presents examples of the various ways they can be used.
Journal Articles
Joint Integrity Characterization in Mixed and Lead-Free Soldering
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EDFA Technical Articles (2006) 8 (1): 16–24.
Published: 01 February 2006
... pad interface, Unstressed capacitors were selected for cross sectioning of the solder joint. Optical images and scanning electron microscopy (SEM) micrographs of the solder joints in all samples are shown in Fig. 4 to 7. indicating a very strong solder joint. After mechanical shock tests, up to 100 kg...
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View articletitled, Joint Integrity Characterization in Mixed and Lead-Free Soldering
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for article titled, Joint Integrity Characterization in Mixed and Lead-Free Soldering
This article presents a method for determining the integrity of solder joints made from mixed and lead-free solders. It discusses the procedures involved in sample preparation and testing and explains how to interpret the results, particularly the effect intermetallic formation, cracking, and voiding.
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