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Journal Articles
AM&P Technical Articles (2013) 171 (7): 28–30.
Published: 01 July 2013
... on surface nitrogen content and case depth in four martensitic stainless steels. Vacuum solution nitriding is a promising technique for increasing the surface hardness, load-bearing capability, and fatigue strength of martensitic stainless steels without sacrificing corrosion resistance. This article...
Abstract
View articletitled, Vacuum Solution Nitriding of Martensitic Stainless Steel Holds Promise
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for article titled, Vacuum Solution Nitriding of Martensitic Stainless Steel Holds Promise
Vacuum solution nitriding is a promising technique for increasing the surface hardness, load-bearing capability, and fatigue strength of martensitic stainless steels without sacrificing corrosion resistance. This article examines the effects of nitriding pressure and temperature on surface nitrogen content and case depth in four martensitic stainless steels.
Journal Articles
AM&P Technical Articles (2013) 171 (11): 52–53.
Published: 01 November 2013
... development High-temperature solution nitriding/carburizing Chromium nitrides/carbides Austenite Low temperature surface hardening log t Fig. 1 TTT diagram of austenite with a high nitrogen or carbon content. A low-temperature treatment of long duration or a high temperature treatment (>1050°C) combined...
Abstract
View articletitled, Low-Temperature <span class="search-highlight">Surface</span> Hardening of Stainless Steel
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for article titled, Low-Temperature <span class="search-highlight">Surface</span> Hardening of Stainless Steel
Low-temperature surface hardening of stainless steel by means of gaseous processing provides a high degree of tailorability of the hard surface case without affecting corrosion resistance. This article covers the fundamental and technological aspects of the process and examines the effect of different LTSH treatments on 304 and 316 austenitic stainless steel.
Journal Articles
AM&P Technical Articles (2013) 171 (2): 20–22.
Published: 01 February 2013
...N.R. Tailleart; F.J. Martin; R.J. Rayne; P.M. Natishan; H. Kahn; A.H. Heuer In this study, 316L stainless steel samples were plasma nitrided for 64 h at 370-420 °C then subjected to surface hardness and pitting corrosion testing. The results show that interstitial hardening with nitrogen...
Abstract
View articletitled, Interstitial Hardening with <span class="search-highlight">Nitrogen</span> for Improved Corrosion Resistance
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for article titled, Interstitial Hardening with <span class="search-highlight">Nitrogen</span> for Improved Corrosion Resistance
In this study, 316L stainless steel samples were plasma nitrided for 64 h at 370-420 °C then subjected to surface hardness and pitting corrosion testing. The results show that interstitial hardening with nitrogen significantly improved the surface hardness as well as the pitting corrosion resistance of the austenitic stainless steel.
Journal Articles
AM&P Technical Articles (2021) 179 (5): 53–54.
Published: 01 July 2021
... the oxygen content in the coating starting with the powders prior to any spraying. A LECO analyzer is specifically designed to estimate very minute (5 to 10 ppm) traces of oxygen, nitrogen, and hydrogen in samples. It is imperative to characterize for oxygen levels, especially with materials and alloys prone...
Abstract
View articletitled, Cold Spray: Advanced Characterization Methods—Raman Spectroscopy, Oxygen Analysis, and <span class="search-highlight">Surface</span> Roughness Measurement
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for article titled, Cold Spray: Advanced Characterization Methods—Raman Spectroscopy, Oxygen Analysis, and <span class="search-highlight">Surface</span> Roughness Measurement
This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.
Journal Articles
AM&P Technical Articles (2020) 178 (2): 43–47.
Published: 01 February 2020
... it into water. In the N2/H2O experiment, four different steels were exposed to a wet nitrogen atmosphere at 850oC. The (Table 1), the near-surface microstructure is very different although they met the same atmosphere. dew point of wet N2 atmosphere was monitored and controlled at -4oC. As each sample has...
Abstract
View articletitled, Understanding and Optimizing <span class="search-highlight">Nitrogen</span>-Hydrogen Furnace Atmospheres for Annealing
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for article titled, Understanding and Optimizing <span class="search-highlight">Nitrogen</span>-Hydrogen Furnace Atmospheres for Annealing
Proper specification, measurement, and control of annealing furnace atmospheres are critical to reduce sooting, oxidation, sticking, and distortion. This article describes how to effectively design and utilize a nitrogen-hydrogen annealing atmosphere.
Journal Articles
AM&P Technical Articles (2021) 179 (4): 62–65.
Published: 01 May 2021
... IMAGING TO UNDERSTAND SILICON EFFECTS IN NITRIDED STEELS Nitriding is a thermochemical process where nitrogen is introduced into the surface of a component via a heated gas, molten salt, or plasma. Increased amounts of nitrogen lead to solid solution strengthening and precipitation hardening if strong...
Abstract
View articletitled, The Case for Advanced Characterization to Better Understand <span class="search-highlight">Surface</span> Hardening of Steels
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for article titled, The Case for Advanced Characterization to Better Understand <span class="search-highlight">Surface</span> Hardening of Steels
Using advanced characterization techniques on surface hardened steels builds a richer understanding of the underlying metallurgical phenomena.
Journal Articles
AM&P Technical Articles (2019) 177 (8): 42–43.
Published: 01 November 2019
... for quantitative estimation of the elements present. All elements except hydrogen, helium, and lithium can be detected using XRF. It is possible to determine accurate values of elemental information using this method. Fig. 1 Comparison of surface characteristics of helium-sprayed versus nitrogen-sprayed titanium...
Abstract
View articletitled, Cold Spray: Advanced Characterization Methods—X-Ray Photoelectron Spectroscopy, X-Ray Fluorescence, and Auger Electron Spectroscopy
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for article titled, Cold Spray: Advanced Characterization Methods—X-Ray Photoelectron Spectroscopy, X-Ray Fluorescence, and Auger Electron Spectroscopy
This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.
Journal Articles
AM&P Technical Articles (2016) 174 (8): 42–45.
Published: 01 September 2016
... the hot and cooling zones for sinter hardening steel parts. Figure 1 shows a typical continuous sintering furnace design. surface hardness and strength, are affected if uncontrolled carburization or decarburization occurs. In a carbon-neutral atmosphere based on nitrogen with hydrogen addition, the actual...
Abstract
View articletitled, Continuous Dew Point Monitoring System for a Sintering Furnace
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for article titled, Continuous Dew Point Monitoring System for a Sintering Furnace
Accurate and continuous dew point measurement is key to maintaining the atmosphere required to achieve high quality and consistency of sintered products in powder metallurgy processing.
Journal Articles
AM&P Technical Articles (2014) 172 (6): 45.
Published: 01 June 2014
... content for the untreated wire, the addition and/or depletion of carbon in the heat treated wire can be accurately measured. The instrument provides a direct reading of percent carbon without the influence of gas composition. The measurement can be influenced by nitrogen absorption into the coil from...
Abstract
View articletitled, Application Note: Tool for Atmospheric Carbon Potential Analysis
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for article titled, Application Note: Tool for Atmospheric Carbon Potential Analysis
Heat treaters regularly seek ways to prevent and reduce rework and scrap loads by implementing procedures and tools to make sure the heat treating process meets customer expectations and specifications. One process parameter requirement is to ensure consistent atmosphere carbon content. Measuring carbon absorption into steel is commonly done to verify atmosphere consistency. This article describes an atmosphere carbon potential analyzer that provides a cost-effective way to measure carbon using a wire coil that functions in a way similar to using shim stock.
Journal Articles
AM&P Technical Articles (2022) 180 (5): 56–59.
Published: 01 July 2022
... SPECTROSCOPY (GDS) MEASUREMENTS As can be seen from the distribution of the elements in the near-surface region in Fig. 5, the sample is enriched 7 58 FEATURE ADVANCED MATERIALS & PROCESSES | JULY/AUGUST 2022 in nitrogen to an estimated 18 at.% in its peak value at a depth of approximately 0.33 to 0.5 µm...
Abstract
View articletitled, Practical Aspects of Plasma Nitriding Kinetics for 17-4 PH Stainless Steel
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for article titled, Practical Aspects of Plasma Nitriding Kinetics for 17-4 PH Stainless Steel
Plasma nitriding is very effective in removing the passive layer of chromium oxide formed naturally on the surface of stainless steel, but controlling the kinetics is key for optimal results.
Journal Articles
AM&P Technical Articles (2014) 172 (8): 37–38.
Published: 01 August 2014
... vehicle weight as well as improving engine efficiency by reducing internal friction losses. The surface structure of the composite coating created by the PTWA process promotes favorable lubrication, low friction, wear resistance, improved heat transfer, and decreased bore distortion in engine block...
Abstract
View articletitled, Plasma Transferred Wire Arc Process Fortifies Aluminum Engine Blocks
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for article titled, Plasma Transferred Wire Arc Process Fortifies Aluminum Engine Blocks
One of the most recent success stories for thermal spray in the automotive industry involves the development of plasma transferred wire arc (PTWA) for aluminum engine blocks. Driven by the demand to increase fuel efficiency, automakers are placing emphasis on decreasing overall vehicle weight as well as improving engine efficiency by reducing internal friction losses. The surface structure of the composite coating created by the PTWA process promotes favorable lubrication, low friction, wear resistance, improved heat transfer, and decreased bore distortion in engine block cylinders.
Journal Articles
AM&P Technical Articles (2014) 172 (3): 15–19.
Published: 01 March 2014
... and its contents bulence and greater entrainment of oxide films. Entrained are sectioned parallel to flow direction and examined with oxides are typically double oxide film defects (bifilms) com- an optical microscope. The amount of inclusions in the prised of folded MgO films[9]. A fresh melt surface...
Abstract
View articletitled, Finding and Removing Inclusions in Magnesium Alloys
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for article titled, Finding and Removing Inclusions in Magnesium Alloys
Understanding both the origin and procedures for removing inclusions in magnesium alloys results in castings with enhanced mechanical and corrosion properties. This article provides an overview of typical inclusions found in magnesium and its alloys, various techniques used to determine inclusion content, and methods employed to reduce inclusions and their influence on properties.
Journal Articles
AM&P Technical Articles (2023) 181 (1): 36–37.
Published: 01 January 2023
... is partially routed back into the intake air stream to reduce nitric oxide (NOx) content in exhaust emissions. The use of EGR in diesel engines can change engine combustion characteristics and consequently the valve and valve seat inset (VSI) working environment. In addition, engine exhaust gas contains...
Abstract
View articletitled, Sustainable Alloy Solution for Engine Valvetrain Applications
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for article titled, Sustainable Alloy Solution for Engine Valvetrain Applications
Cobalt alloys are widely used to meet the demanding performance requirements of diesal and natural gas engine valvetrain applications. Alloy J513 alloy was developed to lower costs and provide higher performance while also requiring substantially less cobalt usage.
Journal Articles
AM&P Technical Articles (2014) 172 (11): 41–44.
Published: 01 November 2014
... stages of the process to avoid oversaturating the surface with excessive carbon or nitrogen, which are responsible for carbide networking, excessive retained austenite, and/or nitride networking. Therefore, boriding to deeper case depths with a fixed high boron activity during the entire process...
Abstract
View articletitled, Deep Case Boriding for Extreme Wear Resistance
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for article titled, Deep Case Boriding for Extreme Wear Resistance
Boriding is performed by diffusing boron atoms into a metal surface and allowing the boron to react with elements present in the substrate to form metal-boride compounds. Upon diffusing enough boron into the surface, a metal-boride compound layer with high hardness precipitates and grows below the surface of the part. This article discusses boriding of ferrous alloys, including a new deep case boriding method that produces wear layer depths comparable to competitive processes such as carburizing, nitriding, thermal spray coatings, and hardfacing.
Journal Articles
AM&P Technical Articles (2012) 170 (7): 22–26.
Published: 01 July 2012
... resistance and reduce friction losses in engines. 5 V arious surface treatment methods are currently used on cylinder piston group (CPG) components to increase service life of internal combustion engines and improve efficiency. Galvanic chrome plating of piston rings is the most common way to improve engine...
Abstract
View articletitled, Advanced Chromium Carbide Coatings on Piston Rings by CVD: A Highly Adaptable New Method with Relatively Low Cost
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for article titled, Advanced Chromium Carbide Coatings on Piston Rings by CVD: A Highly Adaptable New Method with Relatively Low Cost
Chemical vapor deposition (CVD) of pyrolytic chromium carbide coatings (PCCCs) is proving to be a viable alternative to hard chrome plating used on cylinder piston group components. This article discusses the development and optimization of a CVD process for depositing PCCCs on piston rings and cylinder sleeves. It evaluates the coatings based on friction, wear, and adhesion properties in comparison with coatings produced by other methods.
Journal Articles
AM&P Technical Articles (2022) 180 (6): 15–21.
Published: 01 September 2022
... material examination through transmission and reflection geometries. Reference and sample scans must be performed under pure nitrogen atmosphere due to absorption of THz waves by water vapor[4-6]. THz-TDS sample requirements include having flat and pristine front and back surfaces, as incident THz waves...
Abstract
View articletitled, Examining Ceramics, Glasses and Composites with Nondestructive Terahertz Radiation
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for article titled, Examining Ceramics, Glasses and Composites with Nondestructive Terahertz Radiation
Terahertz time-domain spectroscopy is a powerful and nondestructive analytical characterization technique for investigating ceramics, glasses, and composites.
Journal Articles
AM&P Technical Articles (2024) 182 (7): 27–29.
Published: 01 October 2024
... of the metal/alloy. The stress level can be enhanced by stress raisers on the surface of the object. For example, if the metal is susceptible to attack by pitting or crevice corrosion, these surface features can enhance the localized stresses. Hence, stress cracks are frequently observed to originate from...
Abstract
View articletitled, Damage Caused by Stress Corrosion Cracking
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for article titled, Damage Caused by Stress Corrosion Cracking
Stress corrosion cracking is an insidious form of damage that can occur when a susceptible metal is subjected to a tensile stress in a specific environment. To relieve tensile stresses at welded joints, postweld heat treatment can be helpful in reducing the susceptibility of carbon steel fabrications to SCC. When planning to use stainless steels in chloride-containing environments, it is advisable to select alloys that have been specifically developed to resist stress chloride cracking such as ferritic-austenitic (duplex) alloys, low-carbon ferritic alloys, and 6% Mo austenitic alloys or to select high-nickel alloys.
Journal Articles
AM&P Technical Articles (2015) 173 (8): 20–27.
Published: 01 September 2015
... stiffness, predictable contraction when cooled to cryogenic temperatures, and the ability to be polished to a highly reflective surface. These characteristics were recognized and discussed as design parameters as early as 1966 by Barnes[1], while limitations of the available vacuum hot pressed (VHP) Be were...
Abstract
View articletitled, Beryllium Optics Enable Advanced Space Telescopes
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for article titled, Beryllium Optics Enable Advanced Space Telescopes
Beryllium won a lengthy competition as the material of choice for the mirrors on the James Webb Space Telescope, set to launch in 2018. This article documents the development history leading up to that decision. It took decades to perfect powder atomization and HIP'ing processes to make optical-grade beryllium components homogeneous, isotropic, polishable, thermally and dimensionally stable, and above all, predictable.
Journal Articles
AM&P Technical Articles (2013) 171 (9): 55–58.
Published: 01 September 2013
... of vacuum carburization at an austenitizing temperature of ~930°C followed by high pressure nitrogen gas quenching at 1 20 bar (Fig. 1a). Acetylene is supplied at low pressure in sev- eral boost intervals, because its decomposition is catalyzed by iron atoms at the gear surface, providing high carbon...
Abstract
View articletitled, ICME Tools Can Help Control Gear Distortion from Heat Treating
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for article titled, ICME Tools Can Help Control Gear Distortion from Heat Treating
Engineers at the Ford Motor Co. are using integrated computational materials engineering (ICME) tools, allowing them to accurately simulate the heat treatment of gears and predict phase transformation kinetics and distortion.
Journal Articles
AM&P Technical Articles (2014) 172 (4): 24–26.
Published: 01 April 2014
... concentrations of sulfur and phosphorus in steel. OES determines the nitrogen content and thereby identifies duplex steels. However, this technique is less portable, requires more calibration maintenance, typically uses an argon gas purge, and sometimes requires additional sample preparation. Handheld LIBS...
Abstract
View articletitled, Analyzing Metals with Handheld Laser-Induced Breakdown Spectroscopy (LIBS)
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for article titled, Analyzing Metals with Handheld Laser-Induced Breakdown Spectroscopy (LIBS)
Laser-induced breakdown spectroscopy (LIBS) is an established technology that provides nearly instantaneous and virtually nondestructive analysis with minimal or no sample preparation and without an ionizing radiation source. This article describes the capabilities of new handheld LIBS systems.
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