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Journal Articles
How Specimen Geometry and Microstructure Influence Fracture Toughness Properties of Ferritic Materials
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AM&P Technical Articles (2013) 171 (11): 13–18.
Published: 01 November 2013
... transition regime and test specimen geometries when measuring the toughness of weld metal and heat-affected zones. This article identifies several factors that are not fully addressed in most fracture toughness test standards and explains how they may influence calculated values obtained from ferritic...
Abstract
View articletitled, How <span class="search-highlight">Specimen</span> <span class="search-highlight">Geometry</span> and Microstructure Influence Fracture Toughness Properties of Ferritic Materials
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for article titled, How <span class="search-highlight">Specimen</span> <span class="search-highlight">Geometry</span> and Microstructure Influence Fracture Toughness Properties of Ferritic Materials
This article identifies several factors that are not fully addressed in most fracture toughness test standards and explains how they may influence calculated values obtained from ferritic steels. Of particular consequence are test temperatures within the ductile-to-brittle transition regime and test specimen geometries when measuring the toughness of weld metal and heat-affected zones.
Journal Articles
Quantifying and Propagating Uncertainty in Superelasticity Simulation Inputs
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AM&P Technical Articles (2022) 180 (7): 38–41.
Published: 01 October 2022
... is shown in Fig. 1. The method essentially has three components: (1) a standard tensile test specimen geometry and a test protocol to obtain the surface strain fields in the test specimen using digital image correlation (DIC); (2) a library of simulations of the tensile test specimen loading protocol using...
Abstract
View articletitled, Quantifying and Propagating Uncertainty in Superelasticity Simulation Inputs
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for article titled, Quantifying and Propagating Uncertainty in Superelasticity Simulation Inputs
Digital image correlation data and Bayesian inference used together facilitate rigorous quantification of the uncertainty in material input parameters for finite element simulations of superelastic deformation.
Journal Articles
Using Automated J-R Curve Analysis to Simplify Testing and Save Time
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AM&P Technical Articles (2019) 177 (2): 27–30.
Published: 01 February 2019
... of the normalization method in J-R curve testing, the authors developed an open source software with a user-friendly graphic interface to perform automated J-R curve analysis. The software can analyze the four most commonly used fracture toughness specimen geometries; i.e., compact tension (C(T disk compact tension...
Abstract
View articletitled, Using Automated J-R Curve Analysis to Simplify Testing and Save Time
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for article titled, Using Automated J-R Curve Analysis to Simplify Testing and Save Time
Recently developed open-source software based on standard test and normalization methods simplifies the process of generating J-integral versus crack-growth resistance (J-R) curves to evaluate fracture toughness in the ductile region.
Journal Articles
NASA's Orion Crew Vehicle Sports 3D-Printed Vents
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AM&P Technical Articles (2016) 174 (1): 18–21.
Published: 01 January 2016
... the exact part geometry. It is possible that specimen size (and subsequent microstructure, heating, and cooling rates) affects material properties. No work was done to correlate the effect of specimen size or geometry. Vents were nonstructural parts made from a high-strength alloy, so the effects...
Abstract
View articletitled, NASA's Orion Crew Vehicle Sports 3D-Printed Vents
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for article titled, NASA's Orion Crew Vehicle Sports 3D-Printed Vents
Orion’s Exploration Flight Test 1 vehicle used four additively manufactured vent assemblies to equalize pressure between unpressurized portions of the spacecraft and the external environment.
Journal Articles
Computer Modeling Solves Practical Problems in NDE
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AM&P Technical Articles (2013) 171 (10): 18–21.
Published: 01 October 2013
... with a beam angle of 60°. Plate weld Fig. 9 Comparison of a 52° beam angle on flat geometry (top) and cylinder geometry (bottom). 52° beam Pipe seam weld 52° beam ber of experimental specimens and mock-ups needed for technique and procedure validation, completely eliminating these in certain cases...
Abstract
View articletitled, Computer Modeling Solves Practical Problems in NDE
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for article titled, Computer Modeling Solves Practical Problems in NDE
Modeling and simulation are proving to be an effective alternative to the trial-and-error practices often used when developing and evaluating nondestructive tests for materials characterization. This article demonstrates the benefits of modeling in different cases where eddy current and ultrasonic inspection methods are employed.
Journal Articles
Solving Testing Challenges in Powder Metallurgy
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AM&P Technical Articles (2015) 173 (4): 18–21.
Published: 01 April 2015
... principle to enable fatigue testing of metal specimens. Testing at high frequencies may be done rapidly, enabling greater overall test throughput. component-specific gripping arrangements and fixturing, while component geometries often result in specimens with small final dimensions. For these small...
Abstract
View articletitled, Solving Testing Challenges in Powder Metallurgy
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for article titled, Solving Testing Challenges in Powder Metallurgy
Powder metallurgy offers distinct advantages for the production of certain alloys. The degree to which contents of the alloy may be prescribed represents tremendous potential and supports alloy use in new applications. However, robust testing of powder metallurgy alloys is required to assess their potential and quality. Fatigue testing via the resonance principle enables metallurgists to achieve greater throughput in testing programs, while novel hardness testing platforms support analysis of individual phases in porous powder metallurgy specimens.
Journal Articles
Controlled Rotation and Collection of Electron Backscattered Diffraction Patterns from Complex Test Samples
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AM&P Technical Articles (2013) 171 (10): 15–17.
Published: 01 October 2013
... diameter of 12.5 mm a typical geometry often used in tensile tests. The second geometry was a round bar sample of a nickel alloy (IN100) with a gage diameter of 4.8 mm, to test the ability to provide EBSD data from a curved surface. The specimen was 145 mm long (Fig. 2) with an outer bar di- ameter of 25...
Abstract
View articletitled, Controlled Rotation and Collection of Electron Backscattered Diffraction Patterns from Complex Test Samples
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for article titled, Controlled Rotation and Collection of Electron Backscattered Diffraction Patterns from Complex Test Samples
This article discusses the development and use of a nondestructive evaluation (NDE) method that allows researchers to compare surface crystallographic orientations before and after mechanical testing to determine the impact of surface orientation on material response. Two gage samples were tested, one rectangular (Ti-Al), the other round (IN100). The samples were placed in a SEM equipped with an EBSD detector and a motorized fixture that rotates the test piece as EBSD and imaging data are collected. Inverse pole figure maps of both gage samples are presented.
Journal Articles
High-Resolution Crack Imaging Reveals Degradation Processes in Nuclear Reactor Structural Materials
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AM&P Technical Articles (2012) 170 (4): 17–21.
Published: 01 April 2012
... and TEM specimen geometries the APT specimen is a sharp ~100-nm diameter needle, while the TEM specimen is a thin foil (~100-nm thick and 20 mm long). (a) Penetrative oxidation Cr carbide (b) Cr carbide Oxide filaments 50 nm (c) Cr2O3 platelets 50 nm Mo oxide sample (Fig. 2b) is cut out and extracted from...
Abstract
View articletitled, High-Resolution Crack Imaging Reveals Degradation Processes in Nuclear Reactor Structural Materials
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for article titled, High-Resolution Crack Imaging Reveals Degradation Processes in Nuclear Reactor Structural Materials
Researchers at Pacific Northwest National Laboratory (PNNL) use a combination of scanning and transmission electron microscopy, atom probe tomography, and focused ion beam milling to analyze corrosion and crack structures in light-water reactor components with near-atomic spatial resolution.
Journal Articles
Best Practices for Metallography in a Powder Testing Laboratory
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AM&P Technical Articles (2025) 183 (2): 17–20.
Published: 01 March 2025
... of polish, in the aspolished condition. This inspection reveals the frequency and distribution of specimen defects (pores). The shape, size, orientation, and location of these is essential to understand the effect of machine parameters, which in turn guide the development process. If trying to calibrate...
Abstract
View articletitled, Best Practices for Metallography in a Powder Testing Laboratory
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for article titled, Best Practices for Metallography in a Powder Testing Laboratory
This article highlights some of the best metallographic practices from a laser powder bed fusion laboratory and provides practical observations of the more universal aspects of powder testing.
Journal Articles
Additive Manufacturing Presents New Challenges for Metal Components
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AM&P Technical Articles (2022) 180 (5): 24–26.
Published: 01 July 2022
... to confirm satisfactory performance in service. processes and parts, AM components need not only more data points through testing greater sample sizes, but also require more 25 comprehensive data from each specimen. This requires both a quantitative increase in mechanical tests and a qualitative improvement...
Abstract
View articletitled, Additive Manufacturing Presents New Challenges for Metal Components
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for article titled, Additive Manufacturing Presents New Challenges for Metal Components
A look at how companies in regulated industries can test materials to produce higher quality metal components with additive manufacturing.
Journal Articles
Profilometry-Based Indentation Plastometry Brings Speed and Accuracy to Metallurgical R&D
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AM&P Technical Articles (2022) 180 (3): 19–24.
Published: 01 April 2022
...) was developed and commercialized by Plastometrex required for PIP testing per stress-strain curve is 72 mm3, whereas an ASTM E8 sub-size specimen (prior to machin- in the U.K. This unique testing meth- ing to test coupon geometry) requires od offers the materials science, engi- a volume of 2100 mm3 per stress...
Abstract
View articletitled, Profilometry-Based Indentation Plastometry Brings Speed and Accuracy to Metallurgical R&D
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for article titled, Profilometry-Based Indentation Plastometry Brings Speed and Accuracy to Metallurgical R&D
This unique testing method offers economic benefits, sustainability advantages, and the potential to slash the time required to develop new alloys and processing recipes.
Journal Articles
Producing Hybrid Composites By Combining Additive Manufacturing and Casting
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AM&P Technical Articles (2017) 175 (7): 16–21.
Published: 01 October 2017
... offer engineers new tools with which to select materials and geometries for specific applications, through the ability to create unique geometries that are unable to be machined or cast, exploiting novel material properties, and enabling new composite materials to add flexibility to their designs...
Abstract
View articletitled, Producing Hybrid Composites By Combining Additive Manufacturing and Casting
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for article titled, Producing Hybrid Composites By Combining Additive Manufacturing and Casting
Additive manufacturing by itself provides many benefits, but by combining different materials processing techniques like traditional casting with additive manufacturing to create hybrid processes, custom materials can be tailor-made and mass produced for applications with specific performance needs. This article reports on research to create metal-metal interpenetrating phase composite materials using additive manufacturing and casting methods in combination.
Journal Articles
Fabricating Copper Components with Electron Beam Melting
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AM&P Technical Articles (2014) 172 (7): 20–24.
Published: 01 July 2014
... conductivity of copper presents challenges for direct AM processes, fully dense copper components with complex geometries have been demonstrated. Of particular interest is the ability to use AM methods to fabricate internal cooling channels and mesh structures to optimize thermal management. This article...
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View articletitled, Fabricating Copper Components with Electron Beam Melting
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for article titled, Fabricating Copper Components with Electron Beam Melting
The ability to make components from copper and copper alloys via additive manufacturing is spurring a range of novel applications. Although the high thermal conductivity of copper presents challenges for direct AM processes, fully dense copper components with complex geometries have been demonstrated. Of particular interest is the ability to use AM methods to fabricate internal cooling channels and mesh structures to optimize thermal management. This article describes feasibility studies to evaluate AM processing of copper parts.
Journal Articles
Advanced EDS Detectors Drive Nanoparticle Research
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AM&P Technical Articles (2019) 177 (8): 29–31.
Published: 01 November 2019
... the nucleus of the atom. Under normal conditions, the electrons in a specific shell have discrete pieces and detector distance and height have been optimized to place the detector as close as possible to the specimen terials characterization and is common- energies. As an electron beam strikes for the highest...
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View articletitled, Advanced EDS Detectors Drive Nanoparticle Research
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for article titled, Advanced EDS Detectors Drive Nanoparticle Research
The rapid ability of next-generation EDS detectors to characterize beam sensitive materials is leading to breakthroughs in nanoparticle research.
Journal Articles
Toward Integrated Wearable Devices: Shape Memory Alloy Textiles
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AM&P Technical Articles (2020) 178 (3): 63–66.
Published: 01 April 2020
... textiles can be a monofilament, a single-ply yarn spun from microfilaments, and multi-ply yarns. (b) The contractile knitted textile consists of interlacing courses of knit and purl loops. The loop geometry is defined by the loop enclosed area (Al) and the wire diameter (d). (c) Force-knit length profiles...
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View articletitled, Toward Integrated Wearable Devices: Shape Memory Alloy Textiles
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for article titled, Toward Integrated Wearable Devices: Shape Memory Alloy Textiles
Shape memory alloy textiles provide complex deformation and force profiles for novel wearable applications.
Journal Articles
Quantitative Analysis of Phase Transformation in Ni-Ti Shape Memory Alloys
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AM&P Technical Articles (2013) 171 (4): 21–24.
Published: 01 April 2013
... by typical optical imaging elements. However, applying DIC to scanning electron images requires consideration of the more complex distortions created by rastering of the electron beam, the time-dependent nature of image capture, the complex geometry *Joint Student Member of ASM International ** Member of ASM...
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View articletitled, Quantitative Analysis of Phase Transformation in Ni-Ti Shape Memory Alloys
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for article titled, Quantitative Analysis of Phase Transformation in Ni-Ti Shape Memory Alloys
Researchers at the University of Michigan are investigating the complex heterogeneous phase transformations associated with deformation in shape memory alloys by means of in-situ tensile loading in combination with SEM, EBSD, and digital image correlation. This article describes the general approach and presents and interprets test results.
Journal Articles
Nondestructive Testing: A Developing Tool in Science and Engineering
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AM&P Technical Articles (2013) 171 (4): 17–20.
Published: 01 April 2013
... developed after the Tensile sample Displacement field 1980s also advanced NDT technology. Digital image correlation (DIC), comparing images of the same specimen before and after deforma- tion, allows measuring displacement and strain fields without contacting the specimen surface and provides high...
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View articletitled, Nondestructive Testing: A Developing Tool in Science and Engineering
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for article titled, Nondestructive Testing: A Developing Tool in Science and Engineering
This article provides an overview of nondestructive test methods and their application in the study of material properties and structures. It covers the most widely used NDT technologies, including optical examination, radiography, acoustic emission, and ultrasonic testing, and discusses the impact of recent advancements.
Journal Articles
Breakthroughs in Nondestructive Measuring Techniques
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AM&P Technical Articles (2014) 172 (11): 40.
Published: 01 November 2014
...-treated parts, explains Sisson. treating industry needs rapid, accurate nondestructive techniques to measure surface hardness and case depth on carburized steels for process verification and control. Current measurement methods require destructive testing with traveler specimens that cannot always...
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View articletitled, Breakthroughs in Nondestructive Measuring Techniques
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for article titled, Breakthroughs in Nondestructive Measuring Techniques
The Center for Heat Treating Excellence (CHTE) at Worcester Polytechnic Institute (WPI) in Massachusetts is conducting a cutting-edge research project aimed at measuring the surface hardness and case depth on carburized steels for process verification and control. The results will enable companies to improve the quality of heat-treated products faster and more cost-effectively. Nondestructive techniques being evaluated initially include eddy current, meandering winding magnetometer (MWM), Barkhausen noise testing, and alternating current potential drop.
Journal Articles
Research Progress: Nondestructive Measurement Techniques
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AM&P Technical Articles (2016) 174 (6): 30–31.
Published: 01 June 2016
... Another challenge with the traveler specimen measurement method is that it often requires periodic production part cut-ups to validate the hardness and case depth of parts The Center for Heat Treating Excellence (CHTE) at after carburization, especially for critical shaft and gear teeth Worcester...
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View articletitled, Research Progress: Nondestructive Measurement Techniques
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for article titled, Research Progress: Nondestructive Measurement Techniques
This article provides an update on a three-year three research project by the Center for Heat Treating Excellence aimed at establishing nondestructive techniques for measuring surface hardness and case depth on carburized steels for process verification and control.
Journal Articles
Cold Spray: Advanced Characterization Methods—Microhardness and Nanoindentation
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AM&P Technical Articles (2022) 180 (3): 37–39.
Published: 01 April 2022
... beneath the specimen surface is measured as the load is applied to the indenter. From the known geometry of the indenter, the size of the area of contact is determined. FEATURE iTSSe TSS 39 ADVANCED MATERIALS & PROCESSES | APRIL 2022 A nanoindentation test is usually performed as a depth-sensing...
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View articletitled, Cold Spray: Advanced Characterization Methods—Microhardness and Nanoindentation
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for article titled, Cold Spray: Advanced Characterization Methods—Microhardness and Nanoindentation
This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.
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