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Search Results for light scattering detectors
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Journal Articles
AM&P Technical Articles (2012) 170 (11): 16–19.
Published: 01 November 2012
...Judit E. Puskas; Geof Wyatt Researchers at the University of Akron have developed a high-resolution characterization system that incorporates six gel permeation chromatography columns, two light scattering detectors, a refractive index sensor, and a viscometer. The new system facilitates the study...
Abstract
View articletitled, New Multidetector Solution Could Lead to Safer Alternatives to Faulty Silicone Breast Implants
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for article titled, New Multidetector Solution Could Lead to Safer Alternatives to Faulty Silicone Breast Implants
Researchers at the University of Akron have developed a high-resolution characterization system that incorporates six gel permeation chromatography columns, two light scattering detectors, a refractive index sensor, and a viscometer. The new system facilitates the study of separated macromolecules and is expected to play a role in the development of safer biopolymers for breast implants.
Journal Articles
AM&P Technical Articles (2016) 174 (8): 16–20.
Published: 01 September 2016
... and detector technologies include the spallation neutron source (SNS) at Oak Ridge National Laboratory (ORNL) and the microchannel plate (MCP) detector[6-8], respectively. These advances enable new contrast mechanisms using neutron scattering Bragg features for crystalline information, such as average lattice...
Abstract
View articletitled, Neutron Characterization of Additively Manufactured Inconel 718
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for article titled, Neutron Characterization of Additively Manufactured Inconel 718
Recent advances in neutron sources and detector technologies enable new contrast mechanisms to determine crystalline information for metal components. This new capability can help validate emerging additive manufacturing processes used to produce parts with complex geometries.
Journal Articles
AM&P Technical Articles (2014) 172 (2): 13–15.
Published: 01 February 2014
... on crystal lattice planes at the necessary Bragg angle for diffraction. The diffracted electrons form the Kikuchi bands that make up the diffraction pattern. However, those electrons that are scattered in the upper part of the sample are likely scattered further before exiting towards the detector, meaning...
Abstract
View articletitled, Transmission Kikuchi Diffraction in the Scanning Electron Microscope: Orientation Mapping on the Nanoscale
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for article titled, Transmission Kikuchi Diffraction in the Scanning Electron Microscope: Orientation Mapping on the Nanoscale
By changing a setup and using electron transparent samples, hundreds of laboratories worldwide have access to a characterization technique, transmission Kikuchi diffraction, that measures grain sizes and orientations in nanocrystalline materials.
Journal Articles
AM&P Technical Articles (2013) 171 (3): 23–27.
Published: 01 March 2013
... number Z). Con- olution at the sample position is approximately 75 µm. sequently, light elements such as hydrogen, boron, and The radiograph and nCT data in Fig. 3 indicate a rela- lithium make very little contribution to the overall scatter- tively low neutron attenuation through the blade itself, ing...
Abstract
View articletitled, Neutron Characterization for Additive Manufacturing
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for article titled, Neutron Characterization for Additive Manufacturing
Neutron-based imaging and measurement techniques are an ideal complement to x-ray methods for characterizing additively manufactured materials and components. This article presents examples showing how neutron radiography and residual strain measurements reveal the internal structure and stress distributions in highly engineered turbine blades produced by additive processes. It also discusses the development of neutron characterization tools at ORNL and a recent effort in which they were used to evaluate stress-relief treatments for large-scale metal AM structures.
Journal Articles
AM&P Technical Articles (2020) 178 (1): 32–34.
Published: 01 January 2020
... samples and recorded using a chargecoupled device detector. x-ray radiation with the same frequency. Thus, the electron is the basic unit scattering x-ray waves. EXPERIMENTAL PROCEDURE Each structural determination usually starts with a single crystal selection. A suitable crystal is generally...
Abstract
View articletitled, Single-Crystal X-Ray Diffraction
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for article titled, Single-Crystal X-Ray Diffraction
This excerpt from ASM Handbook, Volume 10: Materials Characterization describes the technique used to determine crystal structure and the arrangement of atoms in a unit cell.
Journal Articles
AM&P Technical Articles (2012) 170 (10): 14–18.
Published: 01 October 2012
..., in addition to affording large working distances at high resolution, can use variable objective magnification to change detector pixel size without moving the sample. This approach enables fast tuning of system resolution with a technique similar to imaging using a visible-light microscope, providing user...
Abstract
View articletitled, Functionality to Failure: Materials Engineering in the 4th Dimension
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for article titled, Functionality to Failure: Materials Engineering in the 4th Dimension
X-ray microscopy (XRM) offers long working distances and switchable magnification, facilitating time-resolved volumetric investigation of materials and structures. Examples show how XRM opens new windows into microstructure evolution processes in functional materials such as batteries, in response to charge state, and polymer foams, in response to compression loading.
Journal Articles
AM&P Technical Articles (2016) 174 (10): 16–21.
Published: 01 November 2016
... 0.005 <0.01 *S, O, N, and P contents at or below 10 ppm. fit the 4-mm-diameter aperture sizes and allow for sufficient scattering to maintain an adequate signal-to-noise ratio in the SANS data. Two dimensional diffractograms were collected at room temperature at three different detector configurations...
Abstract
View articletitled, Correlative Microscopy of Neutron-Irradiated Materials
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for article titled, Correlative Microscopy of Neutron-Irradiated Materials
Development of new, radiation-tolerant materials that maintain the structural integrity and safety margins over the course of a nuclear power reactor’s service life requires the ability to predict degradation phenomena. Modern post-irradiation examination methods make use of specialized high-flux test reactors and dedicated characterization facilities to limit occupational exposure and prevent the spread of radioactive contamination. This article illustrates the use of these advanced techniques to characterize precipitates in neutron-irradiated Fe-Cr-Al alloys.
Journal Articles
AM&P Technical Articles (2013) 171 (4): 17–20.
Published: 01 April 2013
... (CT) scanner was conceived by Godfrey Newbold Hounsfield[11], enabling the 3-D x-ray measurement method. Recently, synchrotron x-ray CT was used in in-situ ultrahigh temperature tensile tests at Lawrence Berkeley National Laboratory s Advanced Light Source in Calif. Three-dimensional CT scans were...
Abstract
View articletitled, Nondestructive Testing: A Developing Tool in Science and Engineering
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for article titled, Nondestructive Testing: A Developing Tool in Science and Engineering
This article provides an overview of nondestructive test methods and their application in the study of material properties and structures. It covers the most widely used NDT technologies, including optical examination, radiography, acoustic emission, and ultrasonic testing, and discusses the impact of recent advancements.