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Journal Articles
Archaeometallurgical Materials Characterization
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AM&P Technical Articles (2025) 183 (1): 22–24.
Published: 01 January 2025
... microscopy visual inspection X-ray radiography 2 2 httpsdoi.org/10.31399/asm.amp.2025-01.p022 ADVANCED MATERIALS & PROCESSES | JANUARY/FEBRUARY 2025 ARCHAEOMETALLURGICAL MATERIALS CHARACTERIZATION Combinations of descriptive and analytical techniques with case studies provide essential information about...
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View articletitled, Archaeometallurgical Materials Characterization
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This article summarizes the more common analytical techniques for studying ancient metal artifacts, illustrated by case histories. There are two main classifications: noninvasive and invasive techniques. This distinction is of prime importance because some heritage objects may be too rare or valuable for invasive sampling, or there may be ethical objections to certain types of examination. Noninvasive examination of ancient metal artifacts is important, yet it cannot provide the detailed information obtainable from invasive techniques. This is especially true when artifacts contain “hidden” damage and there is also a need for accurate quantitative analyses.
Journal Articles
Archaeometallurgical Study of an Ancient North-African Iron-Base Artifact
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AM&P Technical Articles (2021) 179 (8): 23–26.
Published: 01 November 2021
... of a broken tip of a parent nail, revealed that the basic structure of the nail may be pyramidal (Fig. 3a). X-ray radiography (Fig. 4) helped to define the internal structure of the nail (Fig. 5). At the surface, a layer, less dense than the core, was identified. Cross-section observation shows...
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View articletitled, Archaeometallurgical Study of an Ancient North-African Iron-Base Artifact
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A metallurgical study of a 10th century iron-base nail from the central-East coast of Tunisia reveals how early metallurgists without modern scientific knowledge created parts with engineered properties.
Journal Articles
Nondestructive Testing: A Developing Tool in Science and Engineering
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AM&P Technical Articles (2013) 171 (4): 17–20.
Published: 01 April 2013
..., and components tested typically are huge containers or vehicles up to 13 ft high ´ 8 ft wide ´ 100 ft long. Neutrons, which can be absorbed by hydrogen with a specific high ratio, complement the application of x-rays[11]. Neutron radiography provides more contrast for organic materials than x-ray radiography...
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View articletitled, Nondestructive Testing: A Developing Tool in Science and Engineering
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This article provides an overview of nondestructive test methods and their application in the study of material properties and structures. It covers the most widely used NDT technologies, including optical examination, radiography, acoustic emission, and ultrasonic testing, and discusses the impact of recent advancements.
Journal Articles
NDE of Electrical Generators using Radiographic Inspection
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AM&P Technical Articles (2019) 177 (6): 18–22.
Published: 01 September 2019
... to utilization of nuclear energy and licensed materials in the public interest[2, 3]. Four types of radiation are alpha, beta, neutron, and electromagnetic (gamma and x-ray) as shown in Fig. 4[4]. In industrial radiography, gamma rays and x-rays are commonly used to inspect metal components. These radiations...
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View articletitled, NDE of Electrical Generators using Radiographic Inspection
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Use of radiography to inspect insulated generator components without the need to strip insulation offers advantages over other inspection methods to assess serviceability and need for repair. This article outlines some of the considerations involved in using nondestructive radiography techniques to assess component integrity.
Journal Articles
Neutron Characterization for Additive Manufacturing
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AM&P Technical Articles (2013) 171 (3): 23–27.
Published: 01 March 2013
...Thomas Watkins; Hassina Bilheux; Ke An; Andrew Payzant; Ryan Dehoff; Chad Duty; William Peter; Craig Blue; Craig Brice Neutron-based imaging and measurement techniques are an ideal complement to x-ray methods for characterizing additively manufactured materials and components. This article presents...
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View articletitled, Neutron Characterization for Additive Manufacturing
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Neutron-based imaging and measurement techniques are an ideal complement to x-ray methods for characterizing additively manufactured materials and components. This article presents examples showing how neutron radiography and residual strain measurements reveal the internal structure and stress distributions in highly engineered turbine blades produced by additive processes. It also discusses the development of neutron characterization tools at ORNL and a recent effort in which they were used to evaluate stress-relief treatments for large-scale metal AM structures.
Journal Articles
The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
Available to PurchaseHassina Z. Bilheux, R. Aaron Hanks, Jean-Christophe Bilheux, Harley Skorpenske, Mary-Ellen Donnelly ...
AM&P Technical Articles (2023) 181 (8): 18–23.
Published: 01 November 2023
... available to study structural, chemical, and behavioral properties of materials. Among the most popular techniques are x-ray or neutron radiography and computed tomography[1-7], x-ray or neutron diffraction[8-10], small angle x-ray or neutron scattering[11], acoustic emission[12], scanning electron...
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View articletitled, The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
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for article titled, The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
Wavelength-dependent or hyperspectral imaging is a novel nondestructive characterization technique in the field of neutron radiography and computed tomography. A dedicated facility named VENUS is currently being built at Oak Ridge National Laboratory to provide these characterization capabilities for academia, industry, and other national laboratories. This feature article describes the VENUS capabilities for materials science and engineering, provides a quick overview of the modes of access of the facility, and illustrates the nondestructive measurements and interpretation of results.
Journal Articles
A Noncomprehensive Guide to Nondestructive Evaluation
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AM&P Technical Articles (2018) 176 (6): 26–29.
Published: 01 September 2018
... for dimensional anomalies, color variation, cracks, and pits Locating fabrication discontinuities, stress cracks Near-surface flaws are sensitive to magnetization; includes blow holes, laps, and cracks Online monitoring of magnetic material Penetrating radiation test (RT), computed tomography (CT), digital x-ray...
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View articletitled, A Noncomprehensive Guide to Nondestructive Evaluation
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for article titled, A Noncomprehensive Guide to Nondestructive Evaluation
Nondestructive evaluation comprises a large family of specific test disciplines including visual inspection, dimensional metrology, ultrasound, radiography, penetrant tests, magnetic particle tests, leak tests, eddy current tests, potential drop tests, flash and vibrothermography, shearography, acoustic emissions, and many other methods. This article offers an overview of NDE science and discusses some key considerations for choosing specific techniques.
Journal Articles
Neutron Characterization of Additively Manufactured Inconel 718
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AM&P Technical Articles (2016) 174 (8): 16–20.
Published: 01 September 2016
... components. Hard (high energy) x-rays offer similar penetration capability (depending on the material), but the relevant diffraction angles are very small, so gauge volumes are needle-like, which is problematic for measuring one component of the stress. Therefore, the two techniques are highly complementary...
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View articletitled, Neutron Characterization of Additively Manufactured Inconel 718
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Recent advances in neutron sources and detector technologies enable new contrast mechanisms to determine crystalline information for metal components. This new capability can help validate emerging additive manufacturing processes used to produce parts with complex geometries.
Journal Articles
Acoustic Micro Imaging of Large Objects
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AM&P Technical Articles (2012) 170 (8): 22–24.
Published: 01 August 2012
... Handbook, Vol 17, 9th Edition, ASM International, 1989, p 465-482. D.A. Gilmour, J.F. Reilly, and D. Calabrese, Comparison of Acoustic Microscope, X-ray Radiography, Dye Penetrant and Destructive Physical Analysis Data for Die Attachment Analysis , Proc. Intl. Acoustic Micro Imaging Symposium, 1997...
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View articletitled, Acoustic Micro Imaging of Large Objects
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Acoustic micro imaging is widely used for inspecting IC packages, but readily adapts for the detection of defects in parts and assemblies up to 1 m or more on a side. This article describes a typical imaging setup consisting of a scanning acoustic microscope and water tank and presents examples in which it was used to detect delaminations in solar panels and clogs in brazed aluminum-copper cooling-ring assemblies. It also explains how to deal with issues that arise when scanning large-area parts.
Journal Articles
Forensic Metallurgy in Archaeology and Aerospace
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AM&P Technical Articles (2025) 183 (4): 23–28.
Published: 01 May 2025
... or defect detection: e.g., x-radiography, acoustic emission SEM microscopy and fractography of small and nominally clean components Key: p/l = portable/laboratory equipment; SEM = scanning electron microscope; XRF = x-ray fluorescence. which also caused considerable surface corrosion[1,2]. The crack...
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View articletitled, Forensic Metallurgy in Archaeology and Aerospace
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for article titled, Forensic Metallurgy in Archaeology and Aerospace
Forensic metallurgy investigations in archaeology and aerospace engineering follow similar technical protocols but serve different objectives. Archaeometallurgical analyses focus on artifact provenance and cultural heritage management with minimal invasive sampling, while aerospace investigations prioritize rapid failure analysis for operational problems. Four case studies illustrate the approaches: noninvasive macrophotographic analysis of an ancient silver cup revealed stress corrosion cracking, noninvasive investigation of a Boeing 747 accident identified fatigue failure in fuse pins due to inadequate load knowledge, invasive lead isotope analysis successfully provenanced Chinese bronzes using kernel density methods, and comprehensive testing of F-16 wing bolts ruled out hydrogen embrittlement. Both fields employ similar analytical techniques, including microscopy, fractography, and chemical analysis, but differ in sampling constraints, time pressures, and reporting goals, with successful investigations in both domains requiring interdisciplinary teamwork.
Journal Articles
Additive Manufacturing at the BAM: Focus on Safety
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AM&P Technical Articles (2019) 177 (7): 22–26.
Published: 01 October 2019
... components in laser and arc-based AM processes. In situ techniques in addition to passive and active methods of thermography, include optical tomography (Fig. 1), optical emission spectroscopy, eddy current testing, particle emission spectroscopy, laminography (radiography), x-ray backscattering...
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View articletitled, Additive Manufacturing at the BAM: Focus on Safety
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In Germany, the Federal Institute for Materials Research and Testing (BAM) is addressing challenges in the implementation of additive manufacturing on the industrial landscape for safety-critical applications. This article provides an overview of BAM’s activities in additive manufacturing with a focus on safety (both for applications and the environment) and AM technology innovation for a wide range of materials and manufacturing locations.
Journal Articles
Development of Single Crystal Superalloys: A Brief History
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AM&P Technical Articles (2013) 171 (9): 26–30.
Published: 01 September 2013
...), refractory metals, ceramics, chemistry, x-ray diffraction, microscopy, and several other technical areas. Employees were encouraged to think long term, publish papers, and attend conferences. I was hired as one experienced with cobalt alloys, phase transformation kinetics, and x-ray diffraction. As engineers...
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View articletitled, Development of Single Crystal Superalloys: A Brief History
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An industry pioneer shares a historical overview of the early days of single crystal superalloy development.
Journal Articles
ASM News for May and June 2017
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AM&P Technical Articles (2017) 175 (4): 65–77.
Published: 01 May 2017
... and x-ray radiography (1991-1997 and 2007-present, respectively) and served 68 H I G H L I G H T S TBYOPAERD NOMINATIONS ADVANCED MATERIALS & PROCESSES | MAY/JUNE 2017 as a session chair for several years for Packaging, FIB, and Advanced Techniques. Moore was the general chair for ISTFA 2003...
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View articletitled, ASM News for May and June 2017
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News about ASM members, chapters, events, awards, conferences, affiliates, and other society activities. Topics include: ASM announces the nominees for ASM vice president and trustee for 2017-18 and three members of the Board of Trustees for 2017-2020; profiles for nominated officers; update on the ASM Renewal from ASM President William E. Frazier; the ASM Failure Analysis Society announces nominees for officers and directors; professional profile for Margaret Flury.
Journal Articles
ASM News for September 2015
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AM&P Technical Articles (2015) 173 (8): 59–67.
Published: 01 September 2015
... for all aspects of SEM and TEM imaging and analytical techniques, electron-probe microanalysis, atom probe, Auger electron spectroscopy, XPS, and more. Updated content and new application examples are also sought for other surface analysis methods, thermal analysis (DSC, TGA, DMA, TMA), x-ray spectroscopy...
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View articletitled, ASM News for September 2015
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News about ASM members, chapters, events, awards, conferences, affiliates, and other society activities. Topics include: 2015 class of ASM Fellows; ASM holds its first-ever Affiliate Summit in July 2015; spotlight for ASM Handbook, Volume 7 editors Prasan Samal and Joseph Newkirk.