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Journal Articles
Raman Spectroscopy Optimizes Graphene Characterization
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AM&P Technical Articles (2012) 170 (4): 35–38.
Published: 01 April 2012
...Mark Wall Raman spectroscopy is an indispensable tool in laboratories conducting research in the nascent field of carbon nanomaterials. It provides comprehensive information about the structure and layer thickness of graphene samples with high levels of sensitivity, stability, and control...
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View articletitled, <span class="search-highlight">Raman</span> <span class="search-highlight">Spectroscopy</span> Optimizes Graphene Characterization
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for article titled, <span class="search-highlight">Raman</span> <span class="search-highlight">Spectroscopy</span> Optimizes Graphene Characterization
Raman spectroscopy is an indispensable tool in laboratories conducting research in the nascent field of carbon nanomaterials. It provides comprehensive information about the structure and layer thickness of graphene samples with high levels of sensitivity, stability, and control.
Journal Articles
Cold Spray: Advanced Characterization Methods—Raman Spectroscopy, Oxygen Analysis, and Surface Roughness Measurement
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AM&P Technical Articles (2021) 179 (5): 53–54.
Published: 01 July 2021
... analysis Raman spectroscopy surface roughness measurement httpsdoi.org/10.31399/asm.amp.2021-05.p053 JTST HIGFHFELEAIAGTTUHURTRSEE iTSSe TSS COLD SPRAY: ADVANCED CHARACTERIZATION METHODS RAMAN SPECTROSCOPY, OXYGEN ANALYSIS, AND SURFACE ROUGHNESS MEASUREMENT This article series explores...
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View articletitled, Cold Spray: Advanced Characterization Methods—<span class="search-highlight">Raman</span> <span class="search-highlight">Spectroscopy</span>, Oxygen Analysis, and Surface Roughness Measurement
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for article titled, Cold Spray: Advanced Characterization Methods—<span class="search-highlight">Raman</span> <span class="search-highlight">Spectroscopy</span>, Oxygen Analysis, and Surface Roughness Measurement
This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.
Journal Articles
How Residual Stresses are Measured: An Overview
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AM&P Technical Articles (2024) 182 (8): 12–19.
Published: 01 November 2024
... a discussion of measurement planning and execution considerations. Copyright © ASM International® 2024 2024 ASM International diffraction magnetic techniques mechanical techniques piezo-spectroscopy Raman spectroscopy residual stress measurement ultrasound techniques A D V A N C E D M...
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View articletitled, How Residual Stresses are Measured: An Overview
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for article titled, How Residual Stresses are Measured: An Overview
Residual stress is generally defined as the stress that is retained in equilibrium in a body or material after manufacturing or processing operations or component usage in the absence of any external forces. This article provides an overview of residual stress measurement methods, including diffraction-based, piezo-spectroscopic/Raman, mechanical, ultrasound, and magnetic techniques. It includes a discussion of measurement planning and execution considerations.
Journal Articles
Cold Spray: Advanced Characterization Methods, Part I
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AM&P Technical Articles (2016) 174 (4): 48.
Published: 01 April 2016
... of the coating 13 Raman spectroscopy Phase transitions in the coating 14 Oxygen analysis Feedstock powder characterization As-sprayed coating, distinguishing 15 Surface roughness between process parameters, gas type 16 Microhardness Screening tool for coating 17 Nanoindentation Coating characterization...
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View articletitled, Cold Spray: Advanced Characterization Methods, Part I
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for article titled, Cold Spray: Advanced Characterization Methods, Part I
This new article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coatings development. This article provides a list of techniques to be covered in subsequent articles.
Journal Articles
Evaluating Biofilms on Material Surfaces: A New International Standard
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AM&P Technical Articles (2024) 182 (1): 24–27.
Published: 01 January 2024
... concentration of bacteria increases to some extent, and it becomes clear that the water is fully hydrated due to the discharge of polysaccharides. Therefore, confirmation of EPS is the most important indicator of a true biofilm. Confocal laser microscopy, Raman spectroscopy, and Fourier transform infrared...
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View articletitled, Evaluating Biofilms on Material Surfaces: A New International Standard
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for article titled, Evaluating Biofilms on Material Surfaces: A New International Standard
A new ISO standard could help spur development of new surface treatments and innovative products that can help defend against harmful bacteria and biofilms. This article describes the successful development and adoption of a new standard, ISO 4768:2023, that addresses measurement of anti-biofilm activity on plastic and other nonporous surfaces.
Journal Articles
Trust But Verify
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AM&P Technical Articles (2017) 175 (8): 23–24.
Published: 01 November 2017
... on test equipment and began running a battery of tests on incoming metals, including x-ray fluorescence and optical emission spectroscopy, also known as spark testing. And for plastics, we began to do RoHS testing and started using Raman spectroscopy. No matter where you are, it is essential to verify all...
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View articletitled, Trust But Verify
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With today’s sophisticated measurement technology and testing equipment, manufacturers need never be in doubt over the quality of their starting materials and any property changes that occur in process. This interview addresses some of the key processes and technologies used to verify material stocks.
Journal Articles
Discovery of Q-Phases and Direct Coversion of Carbon into Diamond and h-BN into c-BN
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AM&P Technical Articles (2016) 174 (3): 24–28.
Published: 01 March 2016
... | MARCH 2016 26 Fig. 2 SEM micrographs: (a) nucleation of microdiamond from the Q-carbon (mechanism of carbon into diamond conversion), (b) mixture of nanodiamond and microdiamond, (c) entire area covered with microdiamond, and (d) diamond nanoneedles and microneedles. Fig. 3 Raman spectroscopy...
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View articletitled, Discovery of Q-Phases and Direct Coversion of Carbon into Diamond and h-BN into c-BN
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for article titled, Discovery of Q-Phases and Direct Coversion of Carbon into Diamond and h-BN into c-BN
The discovery of new phases of carbon and direct conversion of carbon into diamond and diamond-like materials—at ambient conditions and without a catalyst—is a breakthrough with tremendous potential for electronics and hard-materials applications.
Journal Articles
Archaeometallurgical Materials Characterization
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AM&P Technical Articles (2025) 183 (1): 22–24.
Published: 01 January 2025
... to cracked, and corroded. It was investigated by x-ray radiography, inductively coupled plasma mass spectroscopy (ICP-MS) for metal analysis, metallography (optical and SEM), x-ray diffraction (XRD), micro-Raman spectroscopy, and SEM + EDS for corrosion product analyses. The vessel proved to be made from two...
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View articletitled, Archaeometallurgical Materials Characterization
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for article titled, Archaeometallurgical Materials Characterization
This article summarizes the more common analytical techniques for studying ancient metal artifacts, illustrated by case histories. There are two main classifications: noninvasive and invasive techniques. This distinction is of prime importance because some heritage objects may be too rare or valuable for invasive sampling, or there may be ethical objections to certain types of examination. Noninvasive examination of ancient metal artifacts is important, yet it cannot provide the detailed information obtainable from invasive techniques. This is especially true when artifacts contain “hidden” damage and there is also a need for accurate quantitative analyses.
Journal Articles
Historic Monel, Part II: Testing and Analysis of Atmospheric Corrosion Products
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AM&P Technical Articles (2020) 178 (8): 24–30.
Published: 01 November 2020
..., with the addition of x-ray diffraction (XRD), Raman spectroscopy, and gas chromatography mass spectrometry (GC-MS) to help qualify corrosion compounds *Member of ASM International and identify, where possible, organic coatings. Samples in this testing session included two historic Monel sheets from the Metropolitan...
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View articletitled, Historic Monel, Part II: Testing and Analysis of Atmospheric Corrosion Products
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for article titled, Historic Monel, Part II: Testing and Analysis of Atmospheric Corrosion Products
A look at Monel after decades of exposure to the environment shows more work is needed to address the lack of scientific research and information in the conservation literature. Three case studies are presented related to the analysis of Monel artifacts.
Journal Articles
The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
Available to PurchaseHassina Z. Bilheux, R. Aaron Hanks, Jean-Christophe Bilheux, Harley Skorpenske, Mary-Ellen Donnelly ...
AM&P Technical Articles (2023) 181 (8): 18–23.
Published: 01 November 2023
... microscopy[13], transmission electron microscopy[14], optical spectroscopy[15], and Raman spectroscopy[16]. Recently, a novel nondestructive capability called wavelength-dependent or hyperspectral imaging has emerged in the field of neutron radiography and computed tomography. Unlike reactor-based neutron...
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View articletitled, The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
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for article titled, The VENUS Imaging Beamline at the Oak Ridge National Laboratory Spallation Neutron Source
Wavelength-dependent or hyperspectral imaging is a novel nondestructive characterization technique in the field of neutron radiography and computed tomography. A dedicated facility named VENUS is currently being built at Oak Ridge National Laboratory to provide these characterization capabilities for academia, industry, and other national laboratories. This feature article describes the VENUS capabilities for materials science and engineering, provides a quick overview of the modes of access of the facility, and illustrates the nondestructive measurements and interpretation of results.
Journal Articles
Noninvasive µ-XRF Analysis of Ancient Silver Object
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AM&P Technical Articles (2023) 181 (7): 18–21.
Published: 01 October 2023
... PIXE), laser induced breakdown spectroscopy LIBS), and molecular phase analysis, e.g., µ-Raman spectroscopy and micro-x-ray diffraction XRD). This article presents a case study of the application of noninvasive µ-XRF to identify the alloy composition in a 5000-year-old silver-base object from Iran...
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View articletitled, Noninvasive µ-XRF Analysis of Ancient Silver Object
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for article titled, Noninvasive µ-XRF Analysis of Ancient Silver Object
This case study details the noninvasive analysis of an 5000-year-old silver figurine from Iran, now in the collection of The Metropolitan Museum of Art. The The object of this study, a figure of a kneeling bull clothed in a robe with a stepped linear pattern and holding up a spouted vessel, is composed of 15 pieces of worked silver joined together with silver solder. The aim of the study is to apply noninvasive micro-xray fluorescence spectroscopy (μ-XRF) analysis to characterize the silver alloy compositions and compare the new data with previously obtained results from invasive chemical analyses of samples performed by thermal neutron activation.
Journal Articles
Nondestructive Variable Temperature Materials Characterization for Semiconductor Research
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AM&P Technical Articles (2014) 172 (10): 20–22.
Published: 01 October 2014
... impurities in materials will continue to be an important step in the development of next-generation semiconductor devices. Various measurement techniques for Hall conductivity, carrier concentration, and mobility measurements, as well as Raman and x-ray spectroscopy, help to understand these materials...
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View articletitled, Nondestructive Variable Temperature Materials Characterization for Semiconductor Research
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for article titled, Nondestructive Variable Temperature Materials Characterization for Semiconductor Research
To meet the rigorous demands of next-generation computer technology, new approaches to nondestructive measurement for early stage, temperature dependent materials characterization are needed. Terahertz spectroscopy bypasses the limitations of other characterization techniques by enabling nondestructive measurement under variable temperature and high magnetic field conditions.
Journal Articles
Modified Bond Coatings Improve Service Life of Plasma Sprayed Thermal Barrier Coatings and Protective Performance of Overlay Coatings
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AM&P Technical Articles (2018) 176 (5): 40–43.
Published: 01 July 2018
... Distribution in Plasma Sprayed MCrAlY-Coatings Studied by SEM with a Cathodoluminescence Detector and Raman Spectroscopy, Surf. & Coat. Technol., 204, p 531-538, 2009. 15. T. Mori, et al., Effects of Initial Oxidation on Phase Depletion and Oxidation of CoNiCrAlY Bond Coatings Fabricated by Warm Spray...
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View articletitled, Modified Bond Coatings Improve Service Life of Plasma Sprayed Thermal Barrier Coatings and Protective Performance of Overlay Coatings
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for article titled, Modified Bond Coatings Improve Service Life of Plasma Sprayed Thermal Barrier Coatings and Protective Performance of Overlay Coatings
New thermal and cold spray technologies are being developed to extend the lifespan of thermal barrier coating (TBC) systems at elevated temperatures. This article describes the relevant attributes of coating technologies such as high velocity air fuel, high velocity air plasma spray, and high pressure cold spray for use in TBC systems.
Journal Articles
Fabricating Metal Nanostructures with Pulsed Laser Dewetting Self-Assembly
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AM&P Technical Articles (2013) 171 (7): 22–26.
Published: 01 July 2013
... nanostructures that result in resonant interactions with electromagnetic waves at characteristic frequencies of the material[1]. The plasmonic behavior of metals is central to biological and chemical sensing based on techniques such as localized surface plasmon resonance and surface enhanced raman scattering[2,3...
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View articletitled, Fabricating Metal Nanostructures with Pulsed Laser Dewetting Self-Assembly
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for article titled, Fabricating Metal Nanostructures with Pulsed Laser Dewetting Self-Assembly
This article provides an overview of pulsed laser dewetting self-assembly (PLDSA) and its use in the production of silver and cobalt films with desired nanostructure.
Journal Articles
Advanced Designs Pose Challenges for Electronic System Failure Analysis
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AM&P Technical Articles (2014) 172 (8): 23–25.
Published: 01 August 2014
... sophisticated equipment may also be necessary, so failures can be localized down to a single transistor. Materials analysis using various spectroscopy techniques (EDS, Raman) or x-ray (diffraction, reflectivity, or fluorescence) may be useful to characterize materials issues as well. Another critical aspect...
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View articletitled, Advanced Designs Pose Challenges for Electronic System Failure Analysis
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for article titled, Advanced Designs Pose Challenges for Electronic System Failure Analysis
As today's electronics systems continue to shrink and become more complex and pervasive, failures can cause costly downtime, product delays and recalls, and debilitating reputational damage. Finding and fixing failures before they do damage is important, but becomes increasingly challenging when devices are built using ever more complex designs. The solution is to employ a comprehensive, multidisciplinary approach to electronic system failure analysis. In addition, many failures can be avoided altogether by thorough testing, coupled with the latest focused ion beam circuit edit techniques. These advanced methods quickly and inexpensively debug and validate design fixes or explore design optimization opportunities in integrated circuits without having to commit to costly and time-consuming full mask spins.
Journal Articles
ASM News for September 2015
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AM&P Technical Articles (2015) 173 (8): 59–67.
Published: 01 September 2015
..., and x-ray and neutron diffraction. Contributors are also needed to update existing articles on spectroscopy (optical emission, atomic absorption, infrared, Raman); mass and ion spectrometry (spark source, gas analysis, low-energy ion-scattering, Rutherford back scattering, gas, liquid and ion...
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View articletitled, ASM News for September 2015
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News about ASM members, chapters, events, awards, conferences, affiliates, and other society activities. Topics include: 2015 class of ASM Fellows; ASM holds its first-ever Affiliate Summit in July 2015; spotlight for ASM Handbook, Volume 7 editors Prasan Samal and Joseph Newkirk.
Journal Articles
ASM News for March 2025
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AM&P Technical Articles (2025) 183 (2): 45–58.
Published: 01 March 2025
... techniques like SEM, optical profilometry, and Raman spectroscopy. I also oversee the QCM-D and XRD equipment at ICMT, which includes maintaining the systems and training graduate and undergraduate students. My workday often includes research project update meetings and, as with any experimental work...
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View articletitled, ASM News for March 2025
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News about ASM members, chapters, events, awards, conferences, affiliates, and other society activities. Topics include: Frederick Schmidt chairs 2025 nominating committee; affiliate societies name committee chairs for 2024-2025 term; updates from ASM President Navin Manjooran and Executive Director Veronica Becker; President Manjooran visits India chapters; Hani Henein recognized for research transfer success; In memoriam for Gordon W. Powell.
Journal Articles
ASM News for October 2021
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AM&P Technical Articles (2021) 179 (7): 53–65.
Published: 01 October 2021
... are at the time when electrochemical measurements can be performed from the nano to macro-scale in either atmospheric or high-temperature conditions. Nevertheless, electrochemistry encompasses its own complex array of theories that need to be coupled with analytical measurements (e.g., SEM, XPS, Raman) so...
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View articletitled, ASM News for October 2021
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for article titled, ASM News for October 2021
News about ASM members, chapters, events, awards, conferences, affiliates, and other society activities. Topics include: ASM Materials Education Foundation announces 2021 scholarship winners; ASM Constitutional Amendments approved by the ASM Board in September 2021; ASM Acting Executive Director Ron Aderhold recaps the IMAT and Heat Treating events held in September 2021; updates to the ASM volunteer structure to encourage the formation of new technical communities and committees; celebrating 50 years of ASM Historical Landmarks; Briana Richardson and Scott Spohler announced as recipients of the 2021 Kishor M. Kulkarni Distinguished High School Teacher Award; professional profile for Ingrid M. Padilla Espinosa.