Search Results for EBSD characterization

An in-situ annealing technique combined with electron backscatter diffraction was used to characterize the microstructural evolution of ZE20 magnesium alloy as a function of temperature. This work sets the stage for future experiments to understand and control the recrystallization behavior of commercial alloys.

This article series explores the indispensable role of characterization in the development of cold spray coatings. Electron backscatter diffraction (EBSD) is a characterization technique that enables determination of crystal orientations, texture, boundary misorientations and deformation behavior, and bonding mechanism in cold spray coatings.

A microscale fatigue testing technique for characterizing mechanical response and relating it to microstructure promises to improve fatigue life prediction for turbine engine components.

This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.

By changing a setup and using electron transparent samples, hundreds of laboratories worldwide have access to a characterization technique, transmission Kikuchi diffraction, that measures grain sizes and orientations in nanocrystalline materials.

Advances in software algorithms and design enable automation of microstructure image analysis, leading to cost savings, reduction in measurement variability, and access to important metrics.

This article demonstrates the application of machine learning to the classification and segmentation of bainitic microstructures and compares three approaches for assigning the ground truth: correlative microscopy using EBSD as an additional information source, comparison with images obtained from specially produced reference samples, and unsupervised learning.

Researchers at the University of Michigan are investigating the complex heterogeneous phase transformations associated with deformation in shape memory alloys by means of in-situ tensile loading in combination with SEM, EBSD, and digital image correlation. This article describes the general approach and presents and interprets test results.

This article discusses the development and use of a nondestructive evaluation (NDE) method that allows researchers to compare surface crystallographic orientations before and after mechanical testing to determine the impact of surface orientation on material response. Two gage samples were tested, one rectangular (Ti-Al), the other round (IN100). The samples were placed in a SEM equipped with an EBSD detector and a motorized fixture that rotates the test piece as EBSD and imaging data are collected. Inverse pole figure maps of both gage samples are presented.

This article reviews the analytical techniques used for phase identification in components, including x-ray diffraction, metallography/microscopy, electron backscatter diffraction, trasmission electron microscopy,and atom probe tomography. The article addresses the advantages and disadvantages of each technique compared to the other approaches.

This study presents a comprehensive scale-bridging characterization approach to investigate acicular ferrite nucleation in electron beam welded S355 ML steel, demonstrating the critical role of titanium oxide particles in promoting fracture-resistant microstructures for offshore wind monopile applications. Using a multi-technique methodology spanning light microscopy, scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), energy dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM), and transmission Kikuchi diffraction (TKD), the researchers identified and analyzed particles that serve as nucleation sites for acicular ferrite formation. This entry won the prestigious 2024 Jacquet-Lucas Award for Excellence in Metallography at the International Metallographic Contest held during IMAT in Cleveland, October 2024.

Optimizing the integrity and performance of highly engineered surfaces and structures requires the ability to visualize and understand material behavior over multiple length and time scales from a three-dimensional perspective. The Electron Microscopy Centre at the University of Manchester is equipped for such work as demonstrated in problem-solving scenarios involving multiscale imaging and analysis of the progression of intergranular corrosion in Al alloy 2024, the catalytic effect of silver nanoparticles in seawater, recrystallization in a volume element of a bronze alloy, and defect progression on graphene surfaces.

The 15th World Conference on Titanium included papers on titanium alloy development, efforts to reduce Ti powder costs, additive manufacturing, and computational materials modeling tools. This article reviews some of the key advances reported at the conference.

In Germany, the Federal Institute for Materials Research and Testing (BAM) is addressing challenges in the implementation of additive manufacturing on the industrial landscape for safety-critical applications. This article provides an overview of BAM’s activities in additive manufacturing with a focus on safety (both for applications and the environment) and AM technology innovation for a wide range of materials and manufacturing locations.

This article describes research at Los Alamos National Laboratory that is aimed at building a coupled experimental and computational methodology that supports the development of predictive damage capabilities by: (1) capturing real distributions of microstructural features from real material and implementing them as digitally generated microstructures in damage model development, and (2) distilling structure-property information to link microstructural details to damage evolution under a multitude of loading states.

This article explains how SEM, TEM, and atom probe tomography are being used in the development of additively manufactured high-entropy alloys (HEAs), revealing critical features such as anisotropic microstructure and metallurgical defects. It also discusses ongoing efforts to improve the predictability and analysis of HEA microstructure using data-driven approaches.

Because the nature of grain size distribution can influence mechanical properties and service behavior, it is important to accurately characterize this parameter. This article demonstrates how to evaluate grain size distribution, which can be done using either grain area or intercept-length measurements.

An investigation into the chemistry and type of tungsten carbide powder used for drill bits has yielded a material with improved transverse rupture strength and interesting microstructural response to thermal cycling.

Development of wear-resistant hardfacing materials using powder metallurgy/hot isostatic pressing technology offers an alternative to today's cobalt-based materials and those that suffer delamination damage. Ongoing research and development at the Electric Power Research Institute (EPRI), detailed in this article, examines the application of wear-resistant hardfacing materials using the PM/HIP process. The hope is to eliminate weldability and residual stress challenges associated with some hardfacing alloys, as well as to provide a wider range of potential alloy solutions to reduce cobalt use and to address delamination issues with incumbent materials.

Enhancement of the diffusion bonding process for the development of compact heat exchangers (CHXs) provides an energy efficient solution for high-temperature applications in advanced nuclear reactors and other technologies. However, available information is limited concerning the diffusion bonding (and manufacturing) of CHXs in high temperature applications and associated selection of bonded materials, bonding conditions, mechanical performance, and thermo-fluid characteristics. This article reviews the available knowledge and the ongoing research being conducted to address gaps in information and application.