As high-entropy alloys become more complex in terms of microstructure, phase stability, and intermetallics, the advent of sophisticated analytical instruments is helping scientists to develop new materials with the most desirable properties. The analysis techniques described in this article include electron energy loss spectroscopy, electron probe microanalysis, atom probe tomography, and x-ray absorption spectroscopy.

This article describes a metallographic and SEM study of a Spanish silver coin. The study verified the coin's authenticity and determined its alloy composition. The investigation is an example of a unique archaeometallurgical collaboration between a university and a museum.

Alloy developers worldwide have struggled to create creep-resistant alumina-forming, iron-based austenitic stainless steels for use as high-temperature structural alloys, but with limited success in balancing alloy cost, oxidation, and creep resistance. This article describes the research and development of a novel cast alumina-forming austenitic stainless steel. This work won the prestigious Engineering Materials Achievement Award presented at IMAT 2023 in Detroit.

Wavelength-dependent or hyperspectral imaging is a novel nondestructive characterization technique in the field of neutron radiography and computed tomography. A dedicated facility named VENUS is currently being built at Oak Ridge National Laboratory to provide these characterization capabilities for academia, industry, and other national laboratories. This feature article describes the VENUS capabilities for materials science and engineering, provides a quick overview of the modes of access of the facility, and illustrates the nondestructive measurements and interpretation of results.

This article describes the development of applications of phosphate-based materials and characterizes five non-apatite phosphate minerals using 3D optical profilometry. The results reveal the suitability of these materials for new uses in energy storage and conversion as well as medical applications.

This article explores one of the most commonly used analytical techniques in plastic component failure analysis—Fourier transform infrared spectroscopy—along with a case study to demonstrate its use.

This case study details the noninvasive analysis of an 5000-year-old silver figurine from Iran, now in the collection of The Metropolitan Museum of Art. The The object of this study, a figure of a kneeling bull clothed in a robe with a stepped linear pattern and holding up a spouted vessel, is composed of 15 pieces of worked silver joined together with silver solder. The aim of the study is to apply noninvasive micro-xray fluorescence spectroscopy (μ-XRF) analysis to characterize the silver alloy compositions and compare the new data with previously obtained results from invasive chemical analyses of samples performed by thermal neutron activation.

A recent metallographic and historical analysis of two parts from the Buenos Aires to Pacific Railroad railway looked at possible manufacturing techniques of the parts in question. The information collected is useful for comparison with techniques and materials used at that time as well as with current techniques. The analysis questioned whether the material itself has varied or evolved from the metallurgical point of view, and confirmed the quality of raw material used to construct the historic railway line.

A scientific study of two copper coins from 1851 and 1853 reveals well-preserved symbols of a growing, newly independent Chile nation.

The benefits of trace elemental analysis to improve the performance and safety of lithium-ion batteries used in electric vehicles are explored.

A metallurgical study of a 10th century iron-base nail from the central-East coast of Tunisia reveals how early metallurgists without modern scientific knowledge created parts with engineered properties.

This article series explores the indispensable role of characterization in the development of cold spray coatings and illustrates some of the common processes used during coating development.

Integrated elemental analysis with color imaging lets researchers quickly and accurately answer compositional questions.

The rapid ability of next-generation EDS detectors to characterize beam sensitive materials is leading to breakthroughs in nanoparticle research.

Radio frequency inductively coupled plasma (RF-ICP) spraying is shown to be a promising method for producing oxidation-resistant W and W-Cr coatings on plasma-facing surfaces in fission and fusion reactors.

Advanced thermoelectric materials open new horizons for use in solid state power generation and refrigeration applications. This article describes a project that used state-of-the-art computational modeling and high-throughput experimentation to strategically screen the extensive material space and accelerate learning for materials development.

The use of coatings to enhance the performance of components is one of the most powerful tools in materials engineering. This article highlights some examples of how thermal spray technologies are used to enhance surface properties for selected applications and industries.

Among the structural materials developed in the 20th century, titanium and its alloys have played a leading role in improving component performance. This article discusses development of new production techniques, specifications, economic aspects, and applications that have enabled the current applications of titanium alloys.

In cold spray characterization, scanning electron microscopy is used to analyze feedstock powders for particle size, distribution, shape, and chemical composition prior to spraying. SEM is used extensively to characterize coating chemistry via energy-dispersive x-ray spectroscopy (EDS). Coating thickness and interface contour can be characterized in a manner that makes SEM an indispensable and versatile tool for evaluating coating integrity in the as-sprayed condition, as well as in developing an understanding of bonding to the substrate.

Affordable bulk production of a newly developed nanostructured bainitic steel is possible without using severe deformation or complex heat treatments. This article discusses the characteristics and significance of nanostructured bainite in terms of the transformation mechanism.