This paper explores the low cycle fatigue (LCF) and creep-fatigue properties of a hot-forged, normalized, and tempered 9Cr-1Mo ferritic steel. This steel offers good performance in high-temperature applications (up to 873K) in power plants and reactors. The steel was forged into 70 mm diameter rods and then heat-treated with normalizing (1313K for 1 hour, air cooling) and tempering (1033K for 1 hour, air cooling). LCF tests were conducted at 300-873K with varying strain amplitudes and strain rates to understand the influence of both factors. Additionally, some specimens were aged at different temperatures for 10,000 hours before testing. Finally, creep-fatigue interaction tests were performed at 823K and 873K using tensile hold times ranging from 1 to 30 minutes.

A significant research and development effort is underway to support the qualification of Alloy 709 as a Class A construction material in the American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel Code, Section III, Division 5, High Temperature Reactors. This initiative includes a comprehensive Alloy 709 code qualification plan aimed at generating extensive material testing data crucial for compiling the code case data package. The data package is essential in establishing material-specific design parameters for Alloy 709 to be used as Section III, Division 5 Class A construction material for fast reactors, molten salt reactors and gas-cooled reactors. An ASME Section III, Division 5 material code case requires the evaluation of mechanical properties from a minimum of three commercial heats, covering anticipated compositional ranges. A key part of the data package involves fatigue and creep-fatigue testing at elevated temperatures, needed for developing the fatigue design curves and the damage envelope of the creep-fatigue interaction diagram (D-diagram). This paper summarizes the strain-controlled fatigue testing on three commercial heats of Alloy 709 at 760 and 816°C with strain ranges between 0.25% and 3%. The fatigue failure data are used to generate a preliminary fatigue design curve. Additionally, the creep-fatigue testing results at 816°C with tensile hold times of 10, 30, and 60 minutes are presented in support of developing the D-diagram for Alloy 709.

Creep-fatigue lives of nickel-based Alloy 617 and Alloy 740H were investigated to evaluate their applicability to advanced ultrasupercritical (A-USC) power plants. Strain controlled push-pull creep-fatigue tests were performed using solid bar specimen under triangular and trapezoidal waveforms at 700°C. The number of cycles to failure was experimentally obtained for both alloys and the applicability of three representative life prediction methods was studied.

Austenitic stainless steels have been used for boiler tubes in power plants. Since austenitic stainless steels are superior to ferritic steels in high temperature strength and steam oxidation resistance, austenitic stainless steel tubes are used in high temperature parts in boilers. Dissimilar welded joints of austenitic steel and ferritic steel are found in the transition regions between high and low temperature parts. In dissimilar welded parts, there is a large difference in the coefficient of thermal expansion between austenitic and ferritic steel, and thus, thermal stress and strain will occur when the temperature changes. Therefore, the dissimilar welded parts require high durability against the repetition of the thermal stresses. SUPER304H (18Cr-9Ni-3Cu-Nb-N) is an austenitic stainless steel that recently has been used for boiler tubes in power plants. In this study, thermal fatigue properties of a dissimilar welded part of SUPER304H were investigated by conducting thermal fatigue tests and finite element analyses. The test sample was a dissimilar welded tube of SUPER304H and T91 (9Cr-1Mo-V-Nb), which is a typical ferritic heat resistant boiler steel.

The fatigue crack propagation thresholds of SAW weld metal of 25Cr2Ni2MoV simulating product of fossil and nuclear power low pressure turbine rotor at different stress ratios are tested. There is a big dispersity of the test results, even at the same stress ratio. The double logarithm curves of the fatigue crack growth rate and stress intensity factor range are researched. The difference of critical points between stable propagation region and near-threshold region in different specimens is found to be an important cause to the dispersity. Their locations in the specimens can be determined by the method of backward inference. After the observation of the microstructures around the critical points, a good correspondence between the size of prior austenite grain and the maximum size of monotonic plastic zone on the crack tip is confirmed. The difference of the critical points at the same stress ratio is caused by the inhomogeneous microstructures. So the inhomogeneous microstructures in the multi-pass and multi-layer weld metal contribute to the dispersity of the experimental threshold values.

Future, flexible thermal energy conversion systems require new, demand-optimized high-performance materials. In order to provide a basis for the targeted development of fatigue-resistant, cost-effective steel grades, the microstructural damage to materials and the failure of conventional and novel steels were investigated in thermo-mechanical fatigue and fatigue crack propagation experiments. Based on the results, improved, ferritic “HiperFer” (High performance Ferrite) steels were designed, produced and characterized. A brief description of the current state of development is given.

This study presents a characterization of the microstructural evolutions taking place in a 9%Cr martensitic cast steel subjected to fatigue and creep-fatigue loading. Basis for this study of investigation is an extensive testing program performed on a sample heat of this type of steel by conducting a series of service-like high temperature creep-fatigue tests. The major goal here was to systematically vary specific effects in order to isolate and describe relevant damage contributing mechanisms. Furthermore, some of the tests have been interrupted at several percentages of damage to investigate not only the final microstructure but also their evolution. After performing those tests, the samples were examined using transmission electron microscopy (TEM) to characterize and quantify the microstructural evolutions. The size distribution of subgrains and the dislocation density were determined by using thin metal foils in TEM. A recovery process consisting of the coarsening of the subgrains and a decrease of the dislocation density was observed in different form. This coarsening is heterogeneous and depends on the applied temperature, strain amplitude and hold time. These microstructural observations are consistent with the very fast deterioration of creep properties due to cyclic loading.

Single crystal Ni-base superalloys are subjected to tension hold at high temperature in addition to cyclic loading during the operation of gas turbines. Various studies have investigated creep-fatigue crack propagation in superalloys under trapezoidal loadings and evaluated the life time based on parameters such as creep J-integral. However, it is still unclear how damage field and stress-strain condition change at the crack tip during hold time, and how it affects on fatigue crack propagation. In this study, the influence of the tension hold and accompanying creep at crack tip on subsequent fatigue crack propagation behavior was evaluated by introducing single tension holds into pure cyclic loadings. The series of the experiments revealed that because of the tension hold, material degradation and stress relaxation occurred simultaneously ahead of crack tip. In the region where material was degraded, the resistance against crack propagation was reduced, while in the region where stress was relaxed, the crack driving force was lowered.

9-12%Cr martensitic steels can be applied to the next highest temperature components such as boiler tracts, steam pipelines and turbines of advanced ultra-supercritical power plants with steam temperatures of 650°C. New 10%Cr martensitic steels with high B and low N contents can be a worthy candidate for use in production because it has superior creep resistance. At the same time, resistance to cyclic and dynamic loads is very important. In this work, we studied the low cycle fatigue (LCF) properties at room and elevated (500-650°C) temperatures and Charpy impact toughness at temperatures ranging from -196…100°C of advanced 10% Cr martensitic steel with high B and low N contents. The effect of new alloying scheme and corresponding peculiarities of M 23 C 6 carbides on the low cycle fatigue resistance and impact toughness of the 10%Cr martensitic steel is analyzed. It is revealed that fine and densely distributed carbides has no effect on the fatigue resistance except for the slight improvement of fatigue life at small strain amplitudes and shift the ductile-brittle transition temperature (DBTT) to higher but satisfactory value of +10°C as compared to other high-chromium martensitic steels.

Increasing demand for reliable design of all kinds of structures requires materials properties evaluated under the conditions as close to real service conditions as possible. Presently resolved project dealing with development of new turbine blades geometry requires better understanding of the material behavior under service conditions. Service conditions of turbine blades are cyclic loading at high temperatures under superheated steam conditions and complex mechanical loading. There are not commercially available testing systems providing such functionality and thus the system allowing samples testing under considered conditions was developed. The system allows cyclic loading at temperatures up to 650°C under superheated steam conditions. Typical blade steel is investigated here and experimental approach considering complex mechanical loading as well as thermal and corrosion is shown here. The results of high cycle fatigue tests in superheated steam corrosive environment are shown here.

This paper presents the creep and creep-fatigue crack growth behaviors of 30Cr1Mo1V turbine rotor steel which had been in service for 16 years. Two typical sections of the rotor, i.e. high and low temperature sections, are examined at 538°C, with crack initiation and propagation monitored by D.C. potential drop method in a compact tension (CT) specimen. The material of the high temperature section has the lower resistance to creep and creep-fatigue crack growths than the low temperature section. The creep crack initiation (CCI) time decreases with the increase of initial stress intensity factor. The creep-fatigue crack growth (CFCG) is dominated by the cycle-dependent fatigue process when the hold time at the maximum load is shorter, but it becomes dominated by the time-dependent creep process when the hold time becomes longer. The high temperature section shows a larger influence of time-dependent creep behavior on CFCG than the low temperature section.

Creep rupture strength is the principal material property prioritized in designing power generation plants against the steady-state stress due to internal pressure. Increasingly plants must cycle so there is a possibility of life reduction due to creep-fatigue interaction. Grade 92 steel is one of the creep strength enhanced ferritic (CSEF) steels which has superior creep strength compared to other CSEFs. It is expected to be widely used in coal-fired ultra-super critical plants as well as in LNG-fired combined cycle plants. However, at present there is insufficient information regarding the creep-fatigue behavior of this material. A joint study has been conducted to understand the behavior of this steel under creep-fatigue condition and see how accurate the failure life can be estimated. Three kinds of base materials as well as two kinds of welded joints have been tested under strain-controlled cyclic loading with or without hold times as well as under constant load creep condition. Continued decrease in the number of cycles to failure was observed with the extension of hold time in all the base metals and cross-weld specimens. It was found that the modified ductility exhaustion approach based on inelastic strain, as well as its extension employing the inelastic strain energy density, made reasonably accurate predictions of failure lives under a wide range of test conditions. Temperature- and rate-dependencies of fracture limits in terms of inelastic strain and energy density were able to be uniquely expressed using simple thermal activation energy parameters.

The creep-fatigue properties of modified 9Cr-1Mo (grade 91) steel have been investigated for the purpose of design in cyclic service. In this paper test results from creep-fatigue (CF) and low cycle fatigue (LCF) on grade 91 steel are reported. The tests performed on the high precision pneumatic loading system (HIPS) are in the temperature range of 550-600ºC, total strain range of 0.7-0.9% and with hold periods in both tension and compression. Curves of cyclic softening and stress relaxation are presented. The CF test results and results obtained from literature are also analysed using methods described in the assessment and design codes of RCC-MRx, R5 and ASME NH as well as by the recently developed Φ-model. It is shown that the number of cycles to failure for CF data can be accurately predicted by the simple Φ-model. The practicality in using the life fraction rule for presenting the combined damage is discussed and recommendations for alternative approaches are made.

Creep-fatigue crack formation (endurance) and crack growth rate data are necessary inputs for assessing the structural integrity and for estimating the design life of high temperature components in power generation and aircraft engine industries. Ensuring consistency in the reported test data, as well as an understanding of the inherent scatter and its source in the data, are both necessary for assuring quality and limitations of the analyses that rely on the data. In 2008, the American Society for Testing and Materials (ASTM) under the umbrella of its subcommittees E08.05 on Cyclic Deformation and Crack Formation and E08.06 on Crack Growth, and the sponsorship of Electric Power Research Institute (EPRI) through its international experts’ working group on creep-fatigue embarked on the task of developing separate standard test methods for creep-fatigue crack formation and creep-fatigue crack growth. The first standard entitled, “E-2714-09: Standard Test Method for Creep-fatigue Testing” was developed in 2009 and was followed up with a round-robin consisting of 13 laboratories around the world for testing the newly developed standard. This paper discusses the results of this round-robin concluded in 2012 using the widely used P91 steel that led to the formulation of the Precision and Bias statement contained in the version of the ASTM standard E2714 that was successfully balloted in the year 2013.

A research program has been initiated to develop the first predictive methodology for corrosion fatigue life in steam turbine blades, addressing a critical gap in current understanding despite extensive research into corrosion pitting and fatigue failure. The study focuses initially on dual-certified 403/410 12% Cr stainless steel, utilizing a newly developed test facility capable of conducting high-cycle fatigue tests in simulated steam environments at 90°C with controlled corrosive conditions. This testing platform enables the investigation of various steady and cyclic stress conditions, establishing a foundation for future testing of other blade steels and the development of comprehensive blade life estimation techniques.

The creep-fatigue properties of steam turbine materials such as the 1%CrMoV steel traditionally adopted for steam inlet temperatures up to ~565°C, the newer advanced 9-11%Cr steels for applications up to ~600°C, and the nickel based Alloy 617 for potential use to >700°C are reviewed, in particular with reference to their cyclic/hold test crack initiation endurances. The results of cyclic/hold creep-fatigue tests are commonly employed to establish the damage summation diagrams used to form the basis of a number of creep-fatigue assessment procedures, and it is demonstrated that care should be exercised in the way such diagrams are interpreted to compare the creep-fatigue resistances of different alloy types. The form of such damage diagrams is dependent, not only on the analytical procedures used to define the respective fatigue and creep damage fractions, but also on both the deformation and damage interaction mechanisms displayed by the material.

To enhance power plant efficiency, global projects aim to increase operating temperatures to 700 °C (1292 °F) and beyond, surpassing the capabilities of conventional ferritic and austenitic steel alloys and necessitating the use of nickel-based alloys like Alloy 617. This study evaluated the fatigue and creep-fatigue performance of Alloy 617, including both parent metal and welds, at 650 °C (1202 °F). Tests were conducted on virgin material, service-aged samples (up to 25,000 hours), and material over-aged at 800 °C (1472 °F) for 1,000 hours. Results indicated that service aging only slightly reduced the pure fatigue properties of Alloy 617, but significantly decreased its life under creep-fatigue conditions. The creep-fatigue life of ex-service welds was reduced to less than one-third of that of virgin parent metal. The data suggests that the introduction of a tensile hold period impacts Alloy 617's life more than Alloy 263 but less than Alloy 740, potentially linked to the cyclic strength of the alloys. The reduction in life for Alloy 617 is notably greater than that observed in conventional ferritic alloys.

Grade 92 steel, a creep strength-enhanced ferritic (CSEF) steel, is used in supercritical steam fossil power plants for boilers and piping systems. While its creep strength is crucial, understanding the interaction between creep and fatigue damage is also vital for assessing component integrity under cyclic loading. Despite existing studies on its creep-fatigue behavior, additional data under creep-dominant conditions relevant to plant evaluations are needed. Girth welds, critical to piping system integrity, are particularly important in this context. EPRI and CRIEPI initiated a project to develop a comprehensive database on the creep-fatigue behavior of Grade 92 steel's base metal and welded joints and to establish a suitable life estimation procedure. Key findings include: (i) a thick pipe with submerged arc welding (SAW) was manufactured for testing; (ii) base metal and cross-weld specimens showed similar behavior under short-term creep and cyclic loading; (iii) these specimens had lower creep strengths than average literature values for this steel class in the short time regime, with differences decreasing as stress decreased; and (iv) the fatigue and creep-fatigue behavior of these specimens were similar to those of Grade 91 and 122 steels, with common characteristics in creep-fatigue failure prediction models across the three CSEF steels.

For the safe life prediction of components under high cycle fatigue loading at high temperature, such as gas turbine blades and turbocharger components, the behavior of initial defects, which are physically short cracks below the long crack threshold ΔK is of crucial importance. The evolution of different crack closure mechanisms (such as plasticity, roughness and oxide induced crack closure) can lead to crack arrest by a reduction of the effective crack tip loading. To visualize the crack growth behavior of such cracks, cyclic crack resistance curves (cyclic R-curves) are used. The experimental determination of cyclic R-curves is challenging, especially under high temperature conditions due to a lack of optical accessibility. The formation of very short cracks in high strength materials makes it even more complicated to reliably determine these data. Within this study the crack growth behavior of physically short fatigue cracks in three different material states of the nickel alloy IN718 (wrought, cast and PBF-LB/M - processed) is experimentally determined at 650 °C. Based on a load increase procedure applied on Single Edge Notched (SEN) specimens with a compression pre-cracking procedure in advance, crack propagation of physically short cracks is measured with alternating current potential drop systems in air and under vacuum conditions. These examinations are carried out for three different load ratios (R = -1, 0 and 0.5) to investigate the amount of certain crack closure mechanisms active under different loading conditions. Moreover, the formation of a plastic wake along the crack flanks is determined by a finite element simulation. The results determined in air and under vacuum conditions are used to describe the impact of oxide induced crack closure on the behavior of physically short cracks. This allows the evaluation of the behavior of both near-surface and internal defects that are not accessible to the atmosphere.

High-performance Ferritic (HiperFer) steels represent a promising materials innovation for next-generation thermal energy conversion systems, particularly in cyclically operating applications like concentrating solar thermal plants and heat storage power plants (Carnot batteries), where current market adoption is hindered by the lack of cost-effective, high-performance materials. HiperFer steels demonstrate superior fatigue resistance, creep strength, and corrosion resistance compared to conventional ferritic-martensitic 9-12 Cr steels and some austenitic stainless steels, making them potentially transformative for future energy technologies. This paper examines the microstructural mechanisms underlying HiperFer’s enhanced fatigue resistance in both short and long crack propagation, while also presenting current findings on salt corrosion properties and exploring potential alloying improvements for fusion reactor applications, highlighting the broad technical relevance of these innovative materials.