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creep stress
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Proceedings Papers
AM-EPRI2019, 2019 Joint EPRI – 123HiMAT International Conference on Advances in High-Temperature Materials, 1330-1339, October 21–24, 2019,
..., growth rate h, and initiation start time t 1 , and that stress and TF affect f, h and t 1 . We also proposed the method to estimate f, h and t 1 by measuring the change of the distribution of radius of voids during creep test. The creep test conditions are (1) test temperature of 650 C, maximum...
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Type IV creep damage is a problem in high-temperature steam piping made of high chromium steel at thermal power plants, and a method for evaluating the remaining life is required. In this study, we considered that void’s initiation and growth can be expressed by initiation rate f, growth rate h, and initiation start time t 1 , and that stress and TF affect f, h and t 1 . We also proposed the method to estimate f, h and t 1 by measuring the change of the distribution of radius of voids during creep test. The creep test conditions are (1) test temperature of 650 C, maximum principal stress σ 1 of 79.5MPa, and TF of 2.5 ~ 3.0, and (2) test temperature of 650C, maximum principal stress of 71.5MPa, and TF of 2.5 ~ 3.0. The influence of σ 1 to f, h and t 1 was quantified by comparing the result of test (1) and that of test (2).
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 458-465, October 11–14, 2016,
... Abstract In order to clarify the effect of stress and strain on microstructural changes during creep for T91 steel, creep interrupted tests were performed at 600°C for 10000h, 20000h, 30000h, 50000h and 70000h. The steel studied was T91 steel with high Ni content (0.28mass%) in the range...
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In order to clarify the effect of stress and strain on microstructural changes during creep for T91 steel, creep interrupted tests were performed at 600°C for 10000h, 20000h, 30000h, 50000h and 70000h. The steel studied was T91 steel with high Ni content (0.28mass%) in the range of specification. Changes of dislocation structure and precipitates distributions were observed for the grip and gauge portions of creep interrupted samples. The subgrain size gradually increased with increasing creep time up to 50000h in both the grip and gauge portions. However, the subgrain size abruptly increased after 50000h in the gauge portion as compared with the grip portion. Decrease in dislocation density inside subgrain was promoted in the gauge portion as compared with the grip portion. The size of M 23 C 6 gradually increased with increasing creep time up to 50000h in both the grip and gauge portions. The increase in M 23 C 6 size was accelerated after 50000h in the gauge portion as compared with the grip portion. The Z phase formation was promoted in the gauge portion as compared with the grip portion. The number density of all kinds of particles gradually decreased with increasing creep time in the gauge and grip potions. After 50000h, the number density rapidly decreased in the gauge portion as compared with the grip portion.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 622-631, October 11–14, 2016,
... Abstract Remaining-life assessment of high temperature components using the small punch (SP) creep testing technique necessitates the evaluation of SP load (F)/uniaxial stress (σ) conversion factor, F/σ, obtained by comparing the SP and uniaxial creep test results. In the present study, the SP...
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Remaining-life assessment of high temperature components using the small punch (SP) creep testing technique necessitates the evaluation of SP load (F)/uniaxial stress (σ) conversion factor, F/σ, obtained by comparing the SP and uniaxial creep test results. In the present study, the SP creep tests were carried out at 850°C on various Ni-base alloys having different reduction of area in the range of 0.05-0.67 to investigate the influence of creep ductility on the value of F/σ. The F/σ value was determined for each alloy by correlating SP creep rupture data with corresponding uniaxial creep ones. The experimental results revealed that the F/σ value was not well correlated with Vickers hardness, but it increased almost linearly with increasing reduction of area up to around 0.4. This result indicated that the SP creep rupture data could be converted to the uniaxial data if the creep ductility on a given material was available.
Proceedings Papers
AM-EPRI2004, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Fourth International Conference, 1101-1114, October 25–28, 2004,
... creep rate data'. When plotted on the basis of a Larson- Miller parameter (C=30), the calculated values compared well with actual long time rupture testing for exposed and re-heat treated specimens, and generally showed higher precision. The longest test time was about eighteen months for the stress...
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High precision stress relaxation tests (SRT) at temperatures between 550C and 700C were performed on serviced and reheat treated T91, 9%Cr steel. The service exposure was 116,000 hours at steam temperatures to 550C. Constant displacement rate (CDR) tests were also run at 600C on notched specimens for the two conditions. Specimens, heat treated after service, were stronger at the lower test temperatures in terms of both tensile strength and creep strength. This difference was reflected in the CDR results, which also suggested a lower fracture resistance in the heat treated condition. Thus, service exposure appears to have softened the alloy and enhanced its resistance to fracture, with no evidence of embrittling reactions. Based on the analysis of the SRT tests, projections were made of the times to 1% creep and the times to rupture as well as direct comparisons with minimum creep rate data'. When plotted on the basis of a Larson- Miller parameter (C=30), the calculated values compared well with actual long time rupture testing for exposed and re-heat treated specimens, and generally showed higher precision. The longest test time was about eighteen months for the stress rupture data compared with the use of one machine for a few weeks for the SRT data. The latter actually covered a far greater range of creep rates and projected lives. The SRT test is especially consistent at higher parameter values, i.e., higher temperatures and/or lower stresses. This method of accelerated testing is now being applied to a wide range of alloys for fossil power plants for composition and process optimization, design analysis, and life assessment.
Proceedings Papers
AM-EPRI2004, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Fourth International Conference, 1168-1182, October 25–28, 2004,
... Stress (MPa) 1.0E+00 1.0E-01 1.0E-02 10148 (593 C) 30176 (593 C) 30182 (593 C) 30383 (593 C) 30394 (593 C) 1.0E-03 1.0E-04 1.0E-05 100 120 140 160 180 200 220 Stress (MPa) Minimum Creep Rate hr) 1172 Creep Strain 5 Experimental Data Ellis (140 MPa, 500 C) 4 Ellis (140 MPa, 550 C) Ellis (140 MPa, 600 C) 3...
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Significant developments have been made in recent years in the description of creep as a damage process. Advanced martensitic steels that expend over half their lives in the tertiary creep stage have been the focus of attention since their use temperatures are being extended to higher temperatures. Data available for assessing the predictability of the damage models are somewhat scarce since long-time exposure testing has generally been for constant temperature and load conditions. In this work, data are reviewed from relatively long-time tests that involved temperature and stress changes. The prediction of several damage models are compared to material behavior. Most of the comparisons are for 9Cr-1Mo-V steel in the temperature range of 538 to 649 C and for times in the range of 10,000 to 80,000 hours.
Proceedings Papers
AM-EPRI2019, 2019 Joint EPRI – 123HiMAT International Conference on Advances in High-Temperature Materials, 1457-1468, October 21–24, 2019,
... Abstract A constitutive equation, with parameters derived from the interpolation of primary and steady state stages of constant load creep curves, has been utilized to estimate the stress relaxation behavior of the martensitic steel X20Cr13, alloy used in many high temperature applications...
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A constitutive equation, with parameters derived from the interpolation of primary and steady state stages of constant load creep curves, has been utilized to estimate the stress relaxation behavior of the martensitic steel X20Cr13, alloy used in many high temperature applications, including heavy duty gas turbines. Creep and stress relaxation tests have been performed at 350°C, close to the negligible creep temperature of the studied alloy for stresses of interest for engineering applications. The creep tests were carried out at stresses below and above the yield stress, whereas, for the relaxation stress tests, the imposed strain was in the range 0.2% to 1.2% with the purpose to have, at the beginning of the tests, the same initial stresses of the performed creep tests. After a stress relaxation period, lasting between 10 to 1000 hours, each specimen was generally reloaded at the initial stress and a new relaxation test, on the same specimen, was carried out. This “reloading procedure”, simulating the re-tightening of bolts, has been repeated several times. The proposed equation has shown to well predict the experimental creep and stress relaxation behavior of the steel under investigation.
Proceedings Papers
AM-EPRI2013, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Seventh International Conference, 607-614, October 22–25, 2013,
... Abstract In order to clarify the effect of stress state on microstructural changes during creep, the microstructure was observed in the central part of the cross section of the fine-grained heat-affected zone (FGHAZ) and in the surface region of the FGHAZ in Gr.92 steel welded joint. Creep...
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In order to clarify the effect of stress state on microstructural changes during creep, the microstructure was observed in the central part of the cross section of the fine-grained heat-affected zone (FGHAZ) and in the surface region of the FGHAZ in Gr.92 steel welded joint. Creep tests were performed under constant load in air at 650°C, using cross-weld specimens. The creep strength of welded joint was lower than that of base metal. Type IV fracture occurred in the long-term. Creep voids were detected in the FGHAZ after the fracture. Number of creep voids was higher in the central part of the cross section of the FGHAZ than in the surface region of the FGHAZ. It was checked the multiaxiality of stress during creep was higher in the central part of the cross section of the FGHAZ than in the surface region of the FGHAZ. The recovery of dislocation structure occurred after creep in the base metal and the FGHAZ. Mean subgrain size increased with increasing time to rupture. However, there was no difference of change of subgrain size during creep in the central part of the cross section of the FGHAZ and in the surface region of the FGHAZ. The growth of M 23 C 6 carbide and MX carbonitrides was observed during creep in the base metal and the FGHAZ. Laves phase precipitation occurred during creep. There was no difference of the change of mean diameter of MX carbonitrides in the central part of the cross section of the FGHAZ and in the surface region of the FGHAZ after creep. However, the growth rate of M 23 C 6 carbide in the FGHAZ was much higher in the central part of the cross section than in the surface region.
Proceedings Papers
AM-EPRI2024, Advances in Materials, Manufacturing, and Repair for Power Plants: Proceedings from the Tenth International Conference, 1207-1215, October 15–18, 2024,
... Abstract Creep-fatigue tests strain-controlled with different strain amplitudes and different hold times at 725 were done on nickel-based alloy 617 as a typical candidate material for turbine rotor of advanced ultra-supercritical power plant. Stress relaxes during the hold time when the strain...
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Creep-fatigue tests strain-controlled with different strain amplitudes and different hold times at 725 were done on nickel-based alloy 617 as a typical candidate material for turbine rotor of advanced ultra-supercritical power plant. Stress relaxes during the hold time when the strain remains at the tensile peak. The analysis of the stress relaxation during different strain hold times shows that the ratio of the relaxation stress and the maximum stresses has strong correlation with strain amplitude and hold time. The failure life also has a certain dependence on the relaxation stress ratio. The failure life decreases and the relaxation stress ratio increases as the strain amplitude increases. The failure life decreases and the relaxation stress ratio increases as the hold time increases. Therefore the stress relaxation ratio was used as an intermediate variable to obtain the corresponding relationship model by establishing the relationship between the relaxation stress ratio and the strain and the relationship between the relaxation stress ratio and the failure life. This model can be used to predict the creep-fatigue interaction life more simply and directly.
Proceedings Papers
AM-EPRI2019, 2019 Joint EPRI – 123HiMAT International Conference on Advances in High-Temperature Materials, 47-59, October 21–24, 2019,
... Abstract Creep strength of Grade 91 steels has been reviewed and allowable stress of the steels has been revised several times. Allowable stress regulated in ASME Boiler and Pressure Vessel Code of the steels with thickness of 3 inches and above was reduced in 1993, based on the re-evaluation...
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Creep strength of Grade 91 steels has been reviewed and allowable stress of the steels has been revised several times. Allowable stress regulated in ASME Boiler and Pressure Vessel Code of the steels with thickness of 3 inches and above was reduced in 1993, based on the re-evaluation with long-term creep rupture data collected from around the world. After steam leakage from long seam weld of hot reheat pipe made from Grade 122 steel in 2004, creep rupture strength of the creep strength enhanced ferritic (CSEF) steels has been reviewed by means of region splitting method in consideration of 50% of 0.2% offset yield stress (half yield) at the temperature, in the committee sponsored by the Ministry of Economy, Trade and Industry (METI) of Japanese Government. Allowable stresses in the Japanese technical standard of Grade 91 steels have been reduced in 2007 according to the above review. In 2010, additional long-term creep rupture data of the CSEF steels has been collected and the re-evaluation of creep rupture strength of the steels has been conducted by the committee supported by the Federation of Electric Power Companies of Japan, and reduction of allowable stress has been repeated in 2014. Regardless of the previous revision, additional reduction of the allowable stress of Grade 91 steels has been proposed by the review conducted in 2015 by the same committee as 2010. Further reduction of creep rupture strength of Grade 91 steels has been caused mainly by the additional creep rupture data of the low strength materials. A remaining of segregation of alloying elements has been revealed as one of the causes of lowered creep rupture strength. Improvement in creep strength may be expected by reducing segregation, since diffusional phenomena at the elevated temperatures is promoted by concentration gradient due to segregation which increases driving force of diffusion. It has been expected, consequently, that the creep strength and allowable stress of Grade 91 steels can be increased by proper process of fabrication to obtain a homogenized material free from undue segregation.
Proceedings Papers
AM-EPRI2013, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Seventh International Conference, 1292-1303, October 22–25, 2013,
... of threshold creep stress and effective internal creep stress. According to the experimental data of microstructure recovery, the effective internal stress decreased with creep deformation and consequently vanished. In such cases, creep strength is decided only by the threshold stress of creep. Integrating all...
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The Cr and W effect on the creep strength of ferritic steels were studied using the new strengthening hypothesis, precipitation strengthening mechanism, by examining the residual aligned precipitates consisting of W and Cr. In 2 mass% W-containing steel, the increase in Cr content up to 10 mass% resulted in the creep life extension. However, the Cr content higher than 11 mass% decreased the creep life. In 9 mass% Cr-containing steel, the increase in W content decreased the creep deformation rate with creep time. However, it also shortened the time to reach the minimum creep rate. Therefore, optimum Cr and W contents possibly resulted in the optimum alloy design. To understand the effect of W and Cr contents on creep strength, the precipitation strengthening hypothesis by the precipitates at the block boundary must be introduced. The residual aligned precipitation line is supposedly an effective obstacle for the dislocation motion at the interparticle space of the aligned precipitates. The new hypothesis will be activated after block boundary migration. It occurs during the acceleration creep period. On the basis of the hypothesis, creep strength was expressed as the summation of threshold creep stress and effective internal creep stress. According to the experimental data of microstructure recovery, the effective internal stress decreased with creep deformation and consequently vanished. In such cases, creep strength is decided only by the threshold stress of creep. Integrating all, we concluded that the creep deformation mechanism of ferritic creep-resistant steel possibly transits from the viscous dislocation gliding mode to the microstructure recovery driven type mode during the acceleration creep.
Proceedings Papers
AM-EPRI2013, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Seventh International Conference, 637-647, October 22–25, 2013,
...) of Gr. T91 steels creep-ruptured at 600 °C under the stress conditions of 160-80 MPa. The reduction of area at rupture (RA) was 55% for MGA, but 83% for MGC in the long-term condition (under the creep stress of 80 MPa), while RA was higher than 80 % for the two heats in the short-term conditions (under...
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Recovery of microstructure and void formation were investigated in creep-ruptured specimens of ASME Gr. T91 steels to understand the cause of loss of creep rupture ductility in the long-term creep condition and its heat-to-heat variation. The specimens studied were two heats (MGA, MGC) of Gr. T91 steels creep-ruptured at 600 °C under the stress conditions of 160-80 MPa. The reduction of area at rupture (RA) was 55% for MGA, but 83% for MGC in the long-term condition (under the creep stress of 80 MPa), while RA was higher than 80 % for the two heats in the short-term conditions (under the creep stresses above 100 MPa). In both heats, equiaxed grains were observed in the vicinity of ruptured surface in the long-term condition, indicating that recovery and recrystallization occurred extensively in the creep condition, while grains were elongated in the short-term conditions. In the uniformly deformed regions with a small area reduction in the long-term crept specimens, recovered and recrystallized grains were observed in the limited region close to high angle grain boundaries in MGA, while they were extended into grain interiors in MGC. In the long-term creep conditions two types of voids were observed: fine ones with a diameter below 1 μm and coarse ones with a diameter from 2 μm up to 50 μm. Fine creep voids were found to grow with necking in MGA while they neither nucleated nor grew with necking in MGC. Coarse creep voids increased in size and in number with necking in both heats and were larger and denser in MGA than in MGC.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 486-493, October 11–14, 2016,
...., chemical analysis using extracted residues, X-ray diffraction, and scanning transmission electron microscopy. Change ratio of the system free energy and creep stress showed the relationship with one master curve irrespective of creep conditions, indicating that the steel ruptures when the applied stress...
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In order to evaluate long term creep strength of modified 9Cr ferritic steels, the system free energy of creep ruptured specimens at both 650 and 700 °C is evaluated as the sum of chemical free energy, strain energy and surface energy, which are obtained by a series of experiments, i.e., chemical analysis using extracted residues, X-ray diffraction, and scanning transmission electron microscopy. Change ratio of the system free energy and creep stress showed the relationship with one master curve irrespective of creep conditions, indicating that the steel ruptures when the applied stress exceeds a limited stress depending on the microstructural state expressed by the change ratio of system free energy. Furthermore, it was found that dominant factor of the change ratio was the chemical free energy change. On the basis of these results, long term creep strength of the steel was evaluated at 700 °C, for example, 19MPa at 700 °C after 10 5 h. It is concluded that long term creep strength of modified 9Cr ferritic steels can be predicted by the system free energy concept using the ruptured specimens with various creep conditions.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 429-439, October 11–14, 2016,
... strength. All creep rupture test results for materials tempered within 10h exceeded the average creep strength of T91. Shorter tempering times such as 0.5h and 1h were clearly correlated with longer time to rupture at 600°C under 80MPa to 100MPa stress conditions. Reduction of area in creep-ruptured...
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The influence of holding time during tempering on the long-term creep rupture strength of mod.9Cr-1Mo steel was investigated in this study, so as to elucidate proper heat treatment for boiler applications. Tempering was conducted at 770°C for 0.5h, 1h, 3h, 10h and 100h for the test materials, after re-normalization at 1050°C for 1h in all cases. Creep rupture tests were conducted at 600°C, and ruptured specimens were investigated to better understand the microstructural changes, including changes in the number density of precipitates, in order to observe and discuss their creep strength. All creep rupture test results for materials tempered within 10h exceeded the average creep strength of T91. Shorter tempering times such as 0.5h and 1h were clearly correlated with longer time to rupture at 600°C under 80MPa to 100MPa stress conditions. Reduction of area in creep-ruptured specimens decreased principally with lowered creep stress. Materials tempered for 0.5h and 100h showed the lowest reduction of area at 90MPa and 100MPa respectively, and their reduction of area recovered at lower than those stress levels. These stresses, showing minimum reduction of area, met inflection stress in the creep rupture strength curve.
Proceedings Papers
AM-EPRI2013, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Seventh International Conference, 1441-1452, October 22–25, 2013,
... is the secondary stage creep strain at the intended service temperature and time, taking into account the coarsening rate of MX carbonitrides and its effect on the threshold stress for secondary creep. The creep stress to reach a maximal allowed creep strain (taken as 1%) at a given combination of service...
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This work concerns a study into the design of creep resistant precipitation hardened austenitic steels for fossil fuel power plants using an integrated thermodynamics based model in combination with a genetic algorithm optimization routine. The key optimization parameter is the secondary stage creep strain at the intended service temperature and time, taking into account the coarsening rate of MX carbonitrides and its effect on the threshold stress for secondary creep. The creep stress to reach a maximal allowed creep strain (taken as 1%) at a given combination of service temperature and time is formulated and maximized. The model was found to predict the behavior of commercial austenitic creep resistant steels rather accurately. Using the alloy optimization scheme three new steel compositions are presented yielding optimal creep strength for various intended service times up to 105 hours. According to the evaluation parameter employed, the newly defined compositions will outperform existing precipitate strengthened austenitic creep resistant steels.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 137-148, October 11–14, 2016,
.... As the result, it was found that the hardness was increased by not only precipitation due to thermal aging but also creep stress/strain, and there existed linear relationship between the applied stress and creep-induced hardness increase. Also the hardness scatter measured was increased along with the progress...
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The creep degradation/life assessment for high temperature critical component materials is absolutely needed to assure the long-term service operation and there is little experience with the service exposure of the high temperature components made of newly developed Ni-based alloys. In this study, therefore, the creep degradation assessment study on the Ni-based alloys, Alloy 617 and HR6W was conducted based on the hardness method, because the hardness measurement is a useful and simple technique for the materials characterization for any kind of high temperature-serviced steels and alloys. As the result, it was found that the hardness was increased by not only precipitation due to thermal aging but also creep stress/strain, and there existed linear relationship between the applied stress and creep-induced hardness increase. Also the hardness scatter measured was increased along with the progress of creep hardening and damage progressing in terms of creep life consumed. Those findings suggested that the creep life assessment of Ni-based alloys would be possible by means of hardness measurement. The paper also deals with the role and perspective development of non destructive damage detecting techniques, and life assessment issues on Ni-based alloys for A-USC power applications.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 74-89, October 11–14, 2016,
... (the critical inclusion size is directly linked to the creep stress) will act directly as nucleation sites. This paper compares results from traditional uniaxial laboratory creep testing with data obtained under multiaxial conditions. The need to understand and quantify how metallurgical and structural factors...
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Creep brittle behaviour in tempered martensitic, creep strength enhanced ferritic (CSEF) steels is linked to the formation of micro voids. Details of the number of voids formed, and the tendency for reductions in creep strain to fracture are different for the different CSEF steels. However, it appears that the susceptibility for void nucleation is related to the presence of trace elements and hard non-metallic inclusions in the base steel. A key factor in determining whether the inclusions present will nucleate voids is the particle size. Thus, only inclusions of a sufficient size (the critical inclusion size is directly linked to the creep stress) will act directly as nucleation sites. This paper compares results from traditional uniaxial laboratory creep testing with data obtained under multiaxial conditions. The need to understand and quantify how metallurgical and structural factors interact to influence creep damage and cracking is discussed and the significant benefits available through the use of high quality steel making and fabrication procedures are highlighted. Details of component behaviour are considered as part of well-engineered, Damage Tolerant, design methods.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 1018-1026, October 11–14, 2016,
... by specialized thermo(mechanical) treatment. The paper will outline the sensitivity of tensile, creep, stress relaxation and impact properties on processing and heat treatment. Furthermore an outlook on future development potentials will be derived. creep life creep properties heat treatment high...
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High chromium HiperFer (High performance ferritic) materials present a promising concept for the development of high temperature creep and corrosion resistant steels. The institute for Microstructure and Properties of Materials (IEK-2) at Forschungszentrum Jülich GmbH, Germany develops high strength, Laves phase forming, fully ferritic steels which feature excellent resistance to steam oxidation and better creep life than state of the art 9-12 Cr steels. Mechanical strength properties of these steels depend not only on chemical composition, but can be adapted to various applications by specialized thermo(mechanical) treatment. The paper will outline the sensitivity of tensile, creep, stress relaxation and impact properties on processing and heat treatment. Furthermore an outlook on future development potentials will be derived.
Proceedings Papers
AM-EPRI2013, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Seventh International Conference, 596-606, October 22–25, 2013,
... Abstract Contrary to expectations, long-term performance of creep stress enhanced ferritic steels (CSEF) falls short of predictions based on short-term data. This discrepancy is attributed to the formation and growth of creep voids, leading to reduced ductility. This study investigates cavities...
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Contrary to expectations, long-term performance of creep stress enhanced ferritic steels (CSEF) falls short of predictions based on short-term data. This discrepancy is attributed to the formation and growth of creep voids, leading to reduced ductility. This study investigates cavities in creep-tested P92 steel, revealing an association with large ceramic particles (1-2 μm) in standard samples. Three distinct particle compositions were identified: boron nitride (BN), manganese sulfide, and γ-Al 2 O 3 . Statistical analysis showed a strong correlation between BN particles and cavity formation. Using a 3D “slice and view” technique with a focused ion beam/field emission gun scanning electron microscope (FIB-FEGSEM), the study revealed irregular shapes for both cavities and associated particles. Furthermore, analysis of the head-gauge transition area (lower stress exposure) showed small cavities near BN particles, suggesting preferential nucleation on these hard, irregular features. These findings strongly support the hypothesis that BN particles play a key role in cavity nucleation, impacting the long-term performance of P92 steel.
Proceedings Papers
AM-EPRI2024, Advances in Materials, Manufacturing, and Repair for Power Plants: Proceedings from the Tenth International Conference, 123-134, October 15–18, 2024,
... Abstract The mechanical behavior of a cast form of an advanced austenitic stainless steel, CF8C-Plus, is compared with that of its wrought equivalent in terms of both tensile and creep-rupture properties and estimated allowable stress values for pressurized service at temperatures up to about...
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The mechanical behavior of a cast form of an advanced austenitic stainless steel, CF8C-Plus, is compared with that of its wrought equivalent in terms of both tensile and creep-rupture properties and estimated allowable stress values for pressurized service at temperatures up to about 850°C. A traditional Larson-Miller parametric model is used to analyze the creep-rupture data and to predict long-term lifetimes for comparison of the two alloy types. The cast CF8C-Plus exhibited lower yield and tensile strengths, but higher creep strength compared to its wrought counterpart. Two welding methods, shielded-metal-arc welding (SMAW) and gas-metal-arc welding, met the weld qualification acceptance criteria in ASME BPVC Section IX for the cast CF8C-Plus. However, for the wrought CF8C-Plus, while SMAW and gas-tungsten-arc welding passed the tensile acceptance criteria, they failed the side bend tests due to lack of fusion or weld metal discontinuities.
Proceedings Papers
AM-EPRI2016, Advances in Materials Technology for Fossil Power Plants: Proceedings from the Eighth International Conference, 161-168, October 11–14, 2016,
... for purpose of the transition joint by structural integrity assessment, additional mechanical test data, beyond the scope of ASME IX weld procedure qualification, was required. The range of mechanical testing included creep stress rupture testing (parent and cross weld), stress relaxation, cyclic stress...
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INCONEL 740H has been developed by Special Metals for use in Advanced Ultra Super Critical (A-USC) coal fired boilers. Its creep strength performance is currently amongst the ‘best in class’ of nickel based alloys, to meet the challenge of operating in typical A-USC steam temperatures of 700°C at 35 MPa pressure. Whilst the prime physical property of interest for INCONEL 740H has been creep strength, it exhibits other physical properties worthy of consideration in other applications. It has a thermal expansion co-efficient that lies between typical values for Creep Strength Enhanced Ferritic (CSEF) steels and austenitic stainless steels. This paper describes the validation work in support of the fabrication of a pipe transition joint that uses INCONEL 740H pipe, produced in accordance with ASME Boiler Code Case 2702, as a transition material to join P92 pipe to a 316H stainless steel header. The paper gives details of the material selection process, joint design and the verification process used for the joint.
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