Oxide scale, whose ionic conductivity is larger than its electronic one, generate an electro-motive force between a metal/scale and a scale/gas interfaces. When the scale is thin, an electrical potential gradient is large. The large electrical potential gradient may have a possibility to break scales. To confirm the possibility, high temperature oxidation of zirconium on initial stage was observed by an acoustic emission (AE) technique. AE signal was detected before the scale thickness less than 3 μm. And an electrical response on sputtered zirconium oxide thin film was observed. When the applied voltage over 2.00 V, the electrical current was scattered.

High-pressure and high-temperature piping in fossil power plants suffer from unexpected and rarely predictable failures. To prevent failures and ensure operational safety, a Quantitative Acoustic Emission (QAE) non-destructive inspection (NDI) method was developed for revealing, identifying, and assessing flaws in equipment operating under strong background noise. This method enables overall piping inspection during normal operation, locating suspected zones with developing low J-integral flaws, identifying flaw types and evaluating danger levels based on J-integral values, and detecting defective components prior to shutdown. Combining continuous and burst acoustic emission as an information tool, the QAE NDI revealed, identified, and assessed significant flaws like creep, micro-cracks, pore/inclusion systems, plastic deformation, and micro-cracking in over 50 operating high-energy piping systems. Findings were independently verified by various NDI techniques, including time of flight diffraction, focused array transducers, magnetic particles, ultrasonic testing, X-ray, replication, and metallurgical investigations.

Theoretical and experimental investigations, including fracture tests, acoustic emission (AE) studies, fractography, micro-sclerometric analyses, and spectral/chemical analyses of specimens, have established the possibility of revealing, recognizing in-service acquired, age-related, and prefabricated flaws based solely on AE data. Results show a linear dependence between AE and mechanical deformation power of steel specimens in original and creep stage 3a-3b conditions, decreasing fracture load and J1c value for aging steel, creep processes at stage 3a-3b having J-integral value below 0.05J1c, possibility of assessing and distinguishing different flaw development stages with ≥87% accuracy, revealing zones of tough and brittle fracture, and recognizing inclusions/pre-fabricated flaws and assessing individual/interacting flaws. Experiments confirmed the absence of the Kaiser effect under repeated loading of flawed specimens and demonstrated using AE for defect revelation. Analysis showed that creep-associated AE is mainly continuous, with repeated loading decreasing burst AE contribution during plastic deformation development.